Crystallography Open Database

Information card for entry 7712089

7712088 << 7712089 >> 7712090

Preview

Coordinates	7712089.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H48 Cl O3 V
Calculated formula	C35 H48 Cl O3 V
Title of publication	Synthesis and molecular structural studies of racemic chiral-at-vanadium(V) complexes using an unsymmetric achiral phenolic bidentate ligand.
Authors of publication	Nagata, Koichi; Hino, Ayako; Ube, Hitoshi; Sato, Hiroyasu; Shionoya, Mitsuhiko
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	52
Journal issue	11
Pages of publication	3295 - 3299
a	10.4288 ± 0.0002 Å
b	27.1835 ± 0.0004 Å
c	11.229 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	3183.32 ± 0.1 Å³
Cell temperature	123.15 K
Ambient diffraction temperature	123.15 K
Number of distinct elements	5
Space group number	26
Hermann-Mauguin space group symbol	P m c 21
Hall space group symbol	P 2c -2
Residual factor for all reflections	0.0775
Residual factor for significantly intense reflections	0.0712
Weighted residual factors for significantly intense reflections	0.2037
Weighted residual factors for all reflections included in the refinement	0.2112
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283329 (current)	2023-05-05	cif/ Updating files of 7712089, 7712090 Original log message: Adding full bibliography for 7712089--7712090.cif.	7712089.cif
280289	2023-01-12	cif/ Adding structures of 7712089, 7712090 via cif-deposit CGI script.	7712089.cif