Crystallography Open Database

Information card for entry 7712126

Preview

Coordinates	7712126.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H32 B F20 Mg N3
Calculated formula	C37 H32 B F20 Mg N3
Title of publication	Reactivity of a quasi-four-coordinate butylmagnesium cation.
Authors of publication	Ankur, ?; Sharma, Deepti; Andrews, Alex P.; Venugopal, Ajay
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	52
Journal issue	6
Pages of publication	1533 - 1537
a	14.9256 ± 0.0014 Å
b	20.6814 ± 0.0018 Å
c	13.6544 ± 0.0012 Å
α	90°
β	109.49 ± 0.003°
γ	90°
Cell volume	3973.4 ± 0.6 Å³
Cell temperature	140 ± 2 K
Ambient diffraction temperature	140 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0786
Residual factor for significantly intense reflections	0.0426
Weighted residual factors for significantly intense reflections	0.1062
Weighted residual factors for all reflections included in the refinement	0.1321
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283307 (current)	2023-05-05	cif/ Updating files of 7712126, 7712127, 7712128, 7712129, 7712130 Original log message: Adding full bibliography for 7712126--7712130.cif.	7712126.cif
280353	2023-01-17	cif/ Adding structures of 7712126, 7712127, 7712128, 7712129, 7712130 via cif-deposit CGI script.	7712126.cif