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Information card for entry 7712135
Preview
| Coordinates | 7712135.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C76 H64 Cl2 N4 O2 P4 Rh2 |
|---|---|
| Calculated formula | C76 H64 Cl2 N4 O2 P4 Rh2 |
| Title of publication | C-H activation in bimetallic rhodium complexes to afford N-heterocyclic carbene pincer complexes. |
| Authors of publication | Watson, Lachlan J.; Hill, Anthony F. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2023 |
| Journal volume | 52 |
| Journal issue | 7 |
| Pages of publication | 2164 - 2174 |
| a | 11.403 ± 0.002 Å |
| b | 12.569 ± 0.003 Å |
| c | 12.798 ± 0.003 Å |
| α | 108.38 ± 0.03° |
| β | 106.46 ± 0.03° |
| γ | 93.84 ± 0.03° |
| Cell volume | 1644.5 ± 0.8 Å3 |
| Cell temperature | 100 ± 0.2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0719 |
| Residual factor for significantly intense reflections | 0.0521 |
| Weighted residual factors for significantly intense reflections | 0.1411 |
| Weighted residual factors for all reflections included in the refinement | 0.1575 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.053 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | Synchrotron |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 283324 (current) | 2023-05-05 | cif/ Updating files of 7712131, 7712132, 7712133, 7712134, 7712135, 7712136, 7712137 Original log message: Adding full bibliography for 7712131--7712137.cif. |
7712135.cif |
| 280354 | 2023-01-17 | cif/ Adding structures of 7712131, 7712132, 7712133, 7712134, 7712135, 7712136, 7712137 via cif-deposit CGI script. |
7712135.cif |
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Users of the data should acknowledge the original authors of the
structural data.