#------------------------------------------------------------------------------ #$Date: 2023-01-18 01:54:34 +0200 (Wed, 18 Jan 2023) $ #$Revision: 280404 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/71/21/7712140.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7712140 loop_ _publ_author_name 'Osawa, Masahisa' 'Soma, Sakie' 'Kobayashi, Hiroyuki' 'Tanaka, Yuya' 'Hoshino, Mikio' _publ_section_title ; Near-white light emission from single crystals of cationic dinuclear gold(I) complexes with bridged diphosphine ligands. ; _journal_name_full 'Dalton transactions (Cambridge, England : 2003)' _journal_paper_doi 10.1039/d2dt03785h _journal_year 2023 _chemical_formula_moiety 'C46 H54 Au2 N2 P2, 2(B F4), H2 O' _chemical_formula_sum 'C46 H56 Au2 B2 F8 N2 O P2' _chemical_formula_weight 1282.42 _space_group_crystal_system orthorhombic _space_group_IT_number 43 _space_group_name_Hall 'F 2 -2d' _space_group_name_H-M_alt 'F d d 2' _atom_sites_solution_hydrogens mixed _audit_creation_date 2020-09-15 _audit_creation_method ; Olex2 1.2 (compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2022-11-19 deposited with the CCDC. 2022-12-26 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 28.1116(8) _cell_length_b 23.6525(7) _cell_length_c 14.2329(5) _cell_measurement_reflns_used 12087 _cell_measurement_temperature 93(2) _cell_measurement_theta_max 74.8540 _cell_measurement_theta_min 3.6730 _cell_volume 9463.6(5) _computing_cell_refinement 'CrysAlisPro 1.171.40.68a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.68a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.68a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 93(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.972 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 13.00 116.00 0.50 0.05 -- 42.05 77.00 30.00 206 2 \w 32.00 138.00 0.50 0.15 -- 106.13 -84.00 48.00 212 3 \w 33.00 112.00 0.50 0.15 -- 106.13-125.00 -90.00 158 4 \w 32.00 73.00 0.50 0.15 -- 106.13 -61.00-150.00 82 5 \w 32.00 73.00 0.50 0.15 -- 106.13 -61.00-120.00 82 6 \w 20.00 72.00 0.50 0.05 -- 42.05 57.00 150.00 104 7 \w -24.00 39.00 0.50 0.05 -- -42.05 19.00 90.00 126 8 \w -24.00 39.00 0.50 0.05 -- -42.05 19.00 150.00 126 9 \w -69.00 -28.00 0.50 0.15 -- -102.00 61.00 120.00 82 10 \w -69.00 -28.00 0.50 0.15 -- -102.00 61.00-120.00 82 11 \w -108.00 -26.00 0.50 0.15 -- -102.00 110.00-107.00 164 12 \w -88.00 -2.00 0.50 0.05 -- -42.05 110.00-107.00 172 13 \w -175.00 -79.00 0.50 0.15 -- -102.00 -41.00-120.00 192 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0152412000 _diffrn_orient_matrix_UB_12 -0.0244864000 _diffrn_orient_matrix_UB_13 0.0956543000 _diffrn_orient_matrix_UB_21 0.0456934000 _diffrn_orient_matrix_UB_22 0.0235478000 _diffrn_orient_matrix_UB_23 0.0451248000 _diffrn_orient_matrix_UB_31 -0.0261068000 _diffrn_orient_matrix_UB_32 0.0555660000 _diffrn_orient_matrix_UB_33 0.0232054000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0268 _diffrn_reflns_av_unetI/netI 0.0230 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.972 _diffrn_reflns_limit_h_max 34 _diffrn_reflns_limit_h_min -34 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 11981 _diffrn_reflns_point_group_measured_fraction_full 0.924 _diffrn_reflns_point_group_measured_fraction_max 0.874 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 74.828 _diffrn_reflns_theta_min 3.951 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 12.718 _exptl_absorpt_correction_T_max 0.101 _exptl_absorpt_correction_T_min 0.090 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.68a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.800 _exptl_crystal_description irregular _exptl_crystal_F_000 4992 _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.18 _refine_diff_density_max 1.068 _refine_diff_density_min -1.062 _refine_diff_density_rms 0.122 _refine_ls_abs_structure_details ; Flack x determined using 1744 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.009(8) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.073 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 294 _refine_ls_number_reflns 4860 _refine_ls_number_restraints 424 _refine_ls_restrained_S_all 1.047 _refine_ls_R_factor_all 0.0239 _refine_ls_R_factor_gt 0.0238 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0388P)^2^+77.5245P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0616 _refine_ls_wR_factor_ref 0.0617 _reflns_Friedel_coverage 0.727 _reflns_Friedel_fraction_full 0.842 _reflns_Friedel_fraction_max 0.768 _reflns_number_gt 4242 _reflns_number_total 4860 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL exp_762_a.res in Fdd2 olex2_20200904_osawa_sample1.res created by SHELXL-2018/3 at 12:14:33 on 15-Sep-2020 REM Old TITL exp_762 in Fdd2 REM SHELXT solution in Fdd2: R1 0.064, Rweak 0.031, Alpha 0.016 REM 3.269 for 118 systematic absences, Orientation as input REM Flack x = 0.170 ( 0.005 ) from 1774 Parsons' quotients REM Formula found by SHELXT: C40 N11 O10 I2 CELL 1.54184 28.1116 23.6525 14.2329 90 90 90 ZERR 8 0.0008 0.0007 0.0005 0 0 0 LATT -4 SYMM -X,-Y,+Z SYMM 0.25+X,0.25-Y,0.25+Z SYMM 0.25-X,0.25+Y,0.25+Z SFAC C H Au B F N O P UNIT 368 448 16 16 64 16 8 16 DFIX 0.84 0.0001 O1 H1 DELU Au1 P1 N1 C1 C13 C7 C22 C2 C6 C14 C12 C8 C23 C3 C16 C5 C15 C11 C19 C9 = C4 C17 C18 C10 C21 C20 B1 F1 F4 F3 F2 O1 SIMU 0.04 0.08 1.7 P1 Au1 N1 C1 C13 C7 C22 C2 C6 C14 C12 C8 C23 C3 C16 C5 = C15 C11 C19 C9 C4 C17 C18 C10 C21 C20 B1 F1 F4 F3 F2 O1 ISOR 0.005 0.01 P1 Au1 N1 C1 C13 C7 C22 C2 C6 C14 C12 C8 C23 C3 C16 C5 C15 = C11 C19 C9 C4 C17 C18 C10 C21 C20 F1 B1 F4 F3 F2 O1 L.S. 10 PLAN 99 SIZE 0.25 0.2 0.18 TEMP -180(2) MORE -1 CONF fmap 2 acta REM REM REM WGHT 0.038800 77.524498 FVAR 0.08813 AU1 3 0.701581 0.278874 0.442376 11.00000 0.00886 0.01211 = 0.01209 -0.00065 0.00191 -0.00037 P1 8 0.734966 0.322919 0.318851 11.00000 0.00674 0.00981 = 0.01145 -0.00025 -0.00012 0.00209 F1 5 0.705329 0.428708 0.809158 11.00000 0.08897 0.03152 = 0.03871 0.00929 -0.02814 0.00071 F4 5 0.721712 0.396775 0.956984 11.00000 0.09495 0.02984 = 0.02835 -0.00285 -0.01828 0.01438 F3 5 0.682476 0.340566 0.854975 11.00000 0.05391 0.04623 = 0.06598 0.01902 -0.03616 -0.01985 N1 6 0.670429 0.245129 0.558081 11.00000 0.01537 0.02040 = 0.02673 0.00271 0.01051 0.00457 F2 5 0.759213 0.359021 0.832704 11.00000 0.05767 0.05644 = 0.06939 0.00215 0.00426 0.00458 C21 1 0.765487 0.383740 0.590495 11.00000 0.01654 0.02078 = 0.01588 -0.00503 0.00284 -0.00234 AFIX 137 H21A 2 0.760129 0.342802 0.589702 11.00000 -1.50000 H21B 2 0.740723 0.402032 0.628235 11.00000 -1.50000 H21C 2 0.796746 0.391746 0.617921 11.00000 -1.50000 AFIX 0 C12 1 0.832786 0.330247 0.292575 11.00000 0.01333 0.01393 = 0.01478 0.00175 0.00448 0.00013 AFIX 43 H12 2 0.827086 0.309318 0.236729 11.00000 -1.20000 AFIX 0 C19 1 0.763725 0.406464 0.490571 11.00000 0.01016 0.01525 = 0.01857 -0.00630 -0.00185 -0.00341 AFIX 13 H19 2 0.732356 0.395558 0.462835 11.00000 -1.20000 AFIX 0 C2 1 0.650822 0.376695 0.258627 11.00000 0.01528 0.01981 = 0.01328 -0.00410 -0.00264 0.00408 C14 1 0.737425 0.306359 0.128152 11.00000 0.02141 0.01301 = 0.01096 0.00074 0.00061 0.00150 AFIX 43 H14 2 0.728328 0.345041 0.127662 11.00000 -1.20000 AFIX 0 C9 1 0.849603 0.393782 0.452683 11.00000 0.00962 0.01877 = 0.01963 0.00248 -0.00374 -0.00163 AFIX 43 H9 2 0.855881 0.415678 0.507249 11.00000 -1.20000 AFIX 0 C10 1 0.887550 0.374720 0.398859 11.00000 0.00609 0.02251 = 0.02509 0.00246 0.00128 -0.00069 AFIX 43 H10 2 0.919188 0.383617 0.417074 11.00000 -1.20000 AFIX 0 C6 1 0.722542 0.434869 0.265072 11.00000 0.02114 0.01571 = 0.01118 0.00059 0.00055 0.00180 AFIX 43 H6 2 0.755633 0.438151 0.277465 11.00000 -1.20000 AFIX 0 O1 7 0.750000 0.250000 0.735490 10.50000 0.09260 0.06821 = 0.06162 0.00000 0.00000 -0.00759 C1 1 0.699584 0.382973 0.277198 11.00000 0.01347 0.01467 = 0.01205 -0.00098 -0.00255 0.00374 C15 1 0.744292 0.278506 0.042608 11.00000 0.02835 0.02323 = 0.01630 0.00286 0.00352 0.00845 AFIX 43 H15 2 0.741168 0.298460 -0.014989 11.00000 -1.20000 AFIX 0 C8 1 0.802535 0.381726 0.428987 11.00000 0.01185 0.01071 = 0.01675 0.00170 -0.00227 -0.00250 C11 1 0.879591 0.342878 0.318935 11.00000 0.01062 0.02046 = 0.02525 0.00317 0.00480 -0.00011 AFIX 43 H11 2 0.905580 0.329714 0.282307 11.00000 -1.20000 AFIX 0 C13 1 0.743518 0.279107 0.214189 11.00000 0.00958 0.01523 = 0.01219 -0.00037 0.00030 0.00180 C7 1 0.794206 0.348121 0.347624 11.00000 0.01189 0.01088 = 0.01682 0.00355 0.00103 0.00017 C17 1 0.604210 0.302483 0.171594 11.00000 0.02295 0.03836 = 0.02397 -0.01316 -0.00548 -0.00097 AFIX 137 H17A 2 0.580464 0.330160 0.150959 11.00000 -1.50000 H17B 2 0.589184 0.265287 0.177856 11.00000 -1.50000 H17C 2 0.629885 0.300385 0.125147 11.00000 -1.50000 AFIX 0 C3 1 0.625877 0.424620 0.227901 11.00000 0.02154 0.02725 = 0.01912 -0.00378 -0.00661 0.00869 AFIX 43 H3 2 0.592892 0.421593 0.214286 11.00000 -1.20000 AFIX 0 C5 1 0.696847 0.481697 0.234828 11.00000 0.02734 0.01751 = 0.01379 0.00050 -0.00279 0.00508 AFIX 43 H5 2 0.712404 0.516998 0.226488 11.00000 -1.20000 AFIX 0 C4 1 0.648721 0.476923 0.216903 11.00000 0.03304 0.02747 = 0.01907 -0.00377 -0.00465 0.01450 AFIX 43 H4 2 0.631097 0.509061 0.197129 11.00000 -1.20000 AFIX 0 C16 1 0.624665 0.320627 0.266575 11.00000 0.01183 0.02128 = 0.01826 -0.00498 -0.00137 0.00135 AFIX 13 H16 2 0.648539 0.291445 0.285582 11.00000 -1.20000 AFIX 0 C23 1 0.641316 0.202637 0.715249 11.00000 0.05285 0.04715 = 0.03090 0.01940 0.02247 0.01919 AFIX 137 H23A 2 0.607649 0.192392 0.709831 11.00000 -1.50000 H23B 2 0.645263 0.230533 0.765559 11.00000 -1.50000 H23C 2 0.660030 0.168811 0.729906 11.00000 -1.50000 AFIX 0 C18 1 0.586710 0.322612 0.343088 11.00000 0.02129 0.03635 = 0.02591 -0.01030 0.00037 -0.00449 AFIX 137 H18A 2 0.601537 0.332451 0.403222 11.00000 -1.50000 H18B 2 0.571411 0.285514 0.348287 11.00000 -1.50000 H18C 2 0.562797 0.351147 0.326915 11.00000 -1.50000 AFIX 0 C20 1 0.766679 0.471089 0.490911 11.00000 0.02108 0.01822 = 0.02750 -0.00568 -0.00479 0.00575 AFIX 137 H20A 2 0.740006 0.486574 0.527013 11.00000 -1.50000 H20B 2 0.765190 0.485140 0.426203 11.00000 -1.50000 H20C 2 0.796731 0.482926 0.519734 11.00000 -1.50000 AFIX 0 C22 1 0.657486 0.226403 0.627753 11.00000 0.02821 0.02481 = 0.02670 0.00051 0.01115 0.00829 B1 4 0.716717 0.381962 0.862899 11.00000 0.03847 0.02961 = 0.02674 0.00583 -0.01012 0.00128 H1 2 0.739507 0.278072 0.765111 11.00000 1.84142 HKLF 4 REM exp_762_a.res in Fdd2 REM wR2 = 0.0617, GooF = S = 1.073, Restrained GooF = 1.047 for all data REM R1 = 0.0238 for 4242 Fo > 4sig(Fo) and 0.0239 for all 4860 data REM 294 parameters refined using 424 restraints END WGHT 0.0388 77.4973 REM Highest difference peak 1.068, deepest hole -1.062, 1-sigma level 0.122 Q1 1 0.7499 0.2762 0.4420 11.00000 0.05 1.07 Q2 1 0.6542 0.2780 0.4462 11.00000 0.05 1.00 Q3 1 0.7009 0.2749 0.3516 11.00000 0.05 0.93 Q4 1 0.7013 0.2767 0.5359 11.00000 0.05 0.89 Q5 1 0.7341 0.2804 0.3108 11.00000 0.05 0.63 Q6 1 0.7376 0.2766 0.5697 11.00000 0.05 0.57 Q7 1 0.6682 0.2782 0.3191 11.00000 0.05 0.56 Q8 1 0.6998 0.3984 0.4461 11.00000 0.05 0.53 Q9 1 0.6685 0.2809 0.5712 11.00000 0.05 0.51 Q10 1 0.7003 0.3189 0.4735 11.00000 0.05 0.50 Q11 1 0.8541 0.4092 0.6899 11.00000 0.05 0.45 Q12 1 0.6350 0.3479 0.2540 11.00000 0.05 0.41 Q13 1 0.7544 0.4684 0.1899 11.00000 0.05 0.40 Q14 1 0.6927 0.2300 0.4362 11.00000 0.05 0.37 Q15 1 0.6993 0.3158 0.4139 11.00000 0.05 0.36 Q16 1 0.6735 0.4288 0.8453 11.00000 0.05 0.35 Q17 1 0.5754 0.1773 0.7968 11.00000 0.05 0.34 Q18 1 0.6643 0.3424 0.3879 11.00000 0.05 0.33 Q19 1 0.6999 0.2389 0.4104 11.00000 0.05 0.33 Q20 1 0.6891 0.3198 0.2912 11.00000 0.05 0.32 Q21 1 0.6480 0.2217 0.5828 11.00000 0.05 0.32 Q22 1 0.6885 0.2521 0.2859 11.00000 0.05 0.31 Q23 1 0.7350 0.2926 0.7109 11.00000 0.05 0.31 Q24 1 0.7958 0.3787 0.2065 11.00000 0.05 0.30 Q25 1 0.7350 0.4706 0.6501 11.00000 0.05 0.30 Q26 1 0.6371 0.1672 0.6927 11.00000 0.05 0.29 Q27 1 0.6887 0.2711 0.1714 11.00000 0.05 0.29 Q28 1 0.8871 0.2692 0.3207 11.00000 0.05 0.29 Q29 1 0.6949 0.3082 0.6024 11.00000 0.05 0.29 Q30 1 0.7988 0.3643 0.6126 11.00000 0.05 0.29 Q31 1 0.7187 0.5618 0.3122 11.00000 0.05 0.29 Q32 1 0.6605 0.2205 0.4736 11.00000 0.05 0.29 Q33 1 0.7927 0.3283 0.5673 11.00000 0.05 0.29 Q34 1 0.6937 0.2845 0.2327 11.00000 0.05 0.28 Q35 1 0.8068 0.3603 0.8517 11.00000 0.05 0.28 Q36 1 0.6471 0.5488 0.1534 11.00000 0.05 0.28 Q37 1 0.6101 0.3232 0.3037 11.00000 0.05 0.28 Q38 1 0.7624 0.5171 0.2350 11.00000 0.05 0.28 Q39 1 0.6185 0.5402 0.1924 11.00000 0.05 0.28 Q40 1 0.7458 0.2789 0.7896 11.00000 0.05 0.28 Q41 1 0.7478 0.3230 -0.0481 11.00000 0.05 0.27 Q42 1 0.6841 0.3373 0.9347 11.00000 0.05 0.27 Q43 1 0.7500 0.2500 0.5287 10.50000 0.05 0.27 Q44 1 0.7429 0.2723 -0.0539 11.00000 0.05 0.27 Q45 1 0.8516 0.2799 0.3074 11.00000 0.05 0.27 Q46 1 0.7426 0.5381 0.1949 11.00000 0.05 0.27 Q47 1 0.6904 0.3803 0.9781 11.00000 0.05 0.27 Q48 1 0.5600 0.4710 0.1879 11.00000 0.05 0.27 Q49 1 0.6482 0.2702 0.6281 11.00000 0.05 0.27 Q50 1 0.7248 0.2907 0.7721 11.00000 0.05 0.27 Q51 1 0.7359 0.5239 0.2671 11.00000 0.05 0.27 Q52 1 0.6464 0.5386 0.2276 11.00000 0.05 0.26 Q53 1 0.7231 0.3535 0.9483 11.00000 0.05 0.26 Q54 1 0.5408 0.3193 0.3192 11.00000 0.05 0.26 Q55 1 0.6174 0.4074 0.1164 11.00000 0.05 0.26 Q56 1 0.6583 0.1134 0.7871 11.00000 0.05 0.26 Q57 1 0.5951 0.2211 0.6302 11.00000 0.05 0.26 Q58 1 0.7295 0.2864 0.1688 11.00000 0.05 0.26 Q59 1 0.7401 0.3358 0.4096 11.00000 0.05 0.26 Q60 1 0.7787 0.3579 0.2087 11.00000 0.05 0.26 Q61 1 0.5885 0.4646 0.1387 11.00000 0.05 0.25 Q62 1 0.7257 0.4441 0.2300 11.00000 0.05 0.25 Q63 1 0.6252 0.2875 0.4879 11.00000 0.05 0.25 Q64 1 0.6328 0.4524 0.2247 11.00000 0.05 0.25 Q65 1 0.9101 0.4164 0.4440 11.00000 0.05 0.25 Q66 1 0.6258 0.3174 0.4417 11.00000 0.05 0.25 Q67 1 0.6009 0.2191 0.8171 11.00000 0.05 0.25 Q68 1 0.7407 0.4434 0.3058 11.00000 0.05 0.25 Q69 1 0.6765 0.5289 0.2652 11.00000 0.05 0.25 Q70 1 0.5879 0.3644 0.2074 11.00000 0.05 0.25 Q71 1 0.9352 0.4104 0.4025 11.00000 0.05 0.25 Q72 1 0.8639 0.4385 0.4086 11.00000 0.05 0.25 Q73 1 0.6994 0.4346 0.7234 11.00000 0.05 0.24 Q74 1 0.7046 0.4386 0.7019 11.00000 0.05 0.24 Q75 1 0.7311 0.4505 0.3245 11.00000 0.05 0.24 Q76 1 0.7854 0.3250 0.3182 11.00000 0.05 0.24 Q77 1 0.7771 0.2958 0.5106 11.00000 0.05 0.24 Q78 1 0.8291 0.3534 0.2117 11.00000 0.05 0.24 Q79 1 0.7060 0.3522 0.1053 11.00000 0.05 0.24 Q80 1 0.7093 0.3741 0.0987 11.00000 0.05 0.24 Q81 1 0.6975 0.2719 0.1025 11.00000 0.05 0.24 Q82 1 0.6123 0.5014 0.1935 11.00000 0.05 0.24 Q83 1 0.6996 0.1240 0.7310 11.00000 0.05 0.24 Q84 1 0.7069 0.4984 0.1486 11.00000 0.05 0.24 Q85 1 0.5597 0.2006 0.7437 11.00000 0.05 0.24 Q86 1 0.5943 0.2787 0.4748 11.00000 0.05 0.24 Q87 1 0.5901 0.3532 0.3620 11.00000 0.05 0.24 Q88 1 0.7005 0.3297 0.7765 11.00000 0.05 0.23 Q89 1 0.5392 0.2407 0.4486 11.00000 0.05 0.23 Q90 1 0.6751 0.2637 0.7122 11.00000 0.05 0.23 Q91 1 0.6995 0.3453 0.7759 11.00000 0.05 0.23 Q92 1 0.6932 0.3170 0.7827 11.00000 0.05 0.23 Q93 1 0.6308 0.3057 0.3075 11.00000 0.05 0.23 Q94 1 0.7993 0.3662 0.5381 11.00000 0.05 0.23 Q95 1 0.6409 0.4417 0.1089 11.00000 0.05 0.23 Q96 1 0.6295 0.4483 0.1948 11.00000 0.05 0.23 Q97 1 0.7344 0.3199 0.8258 11.00000 0.05 0.23 Q98 1 0.6955 0.4827 0.8383 11.00000 0.05 0.23 Q99 1 0.6027 0.3111 0.1014 11.00000 0.05 0.23 REM The information below was added by Olex2. REM REM R1 = 0.0238 for 4242 Fo > 4sig(Fo) and 0.0239 for all 12297 data REM n/a parameters refined using n/a restraints REM Highest difference peak 1.07, deepest hole -1.06 REM Mean Shift 0, Max Shift 0.004. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0239 REM R1_gt = 0.0238 REM wR_ref = 0.0617 REM GOOF = 1.073 REM Shift_max = 0.004 REM Shift_mean = 0 REM Reflections_all = 12297 REM Reflections_gt = 4242 REM Parameters = n/a REM Hole = -1.06 REM Peak = 1.07 REM Flack = -0.009(8) ; _cod_data_source_file d2dt03785h2.cif _cod_data_source_block olex2_20200904_osawa_sample1 _cod_database_code 7712140 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.208 _shelx_estimated_absorpt_t_min 0.143 _diffrn_oxdiff_digest_frames ; 015373b225078a919f397dc6d6d662ea6100087e77c ; _diffrn_oxdiff_digest_hkl ; 0141021d70e426dcea981a06ca20649187b679 ; _reflns_odcompleteness_completeness 99.91 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances O1-H1 0.84 with sigma of 0.0001 3. Rigid bond restraints Au1, P1, N1, C1, C13, C7, C22, C2, C6, C14, C12, C8, C23, C3, C16, C5, C15, C11, C19, C9, C4, C17, C18, C10, C21, C20, B1, F1, F4, F3, F2, O1 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 4. Uiso/Uaniso restraints and constraints P1 \\sim Au1 \\sim N1 \\sim C1 \\sim C13 \\sim C7 \\sim C22 \\sim C2 \\sim C6 \\sim C14 \\sim C12 \\sim C8 \\sim C23 \\sim C3 \\sim C16 \\sim C5 \\sim C15 \\sim C11 \\sim C19 \\sim C9 \\sim C4 \\sim C17 \\sim C18 \\sim C10 \\sim C21 \\sim C20 \\sim B1 \\sim F1 \\sim F4 \\sim F3 \\sim F2 \\sim O1: within 1.7A with sigma of 0.04 and sigma for terminal atoms of 0.08 Uanis(P1) \\sim Ueq, Uanis(Au1) \\sim Ueq, Uanis(N1) \\sim Ueq, Uanis(C1) \\sim Ueq, Uanis(C13) \\sim Ueq, Uanis(C7) \\sim Ueq, Uanis(C22) \\sim Ueq, Uanis(C2) \\sim Ueq, Uanis(C6) \\sim Ueq, Uanis(C14) \\sim Ueq, Uanis(C12) \\sim Ueq, Uanis(C8) \\sim Ueq, Uanis(C23) \\sim Ueq, Uanis(C3) \\sim Ueq, Uanis(C16) \\sim Ueq, Uanis(C5) \\sim Ueq, Uanis(C15) \\sim Ueq, Uanis(C11) \\sim Ueq, Uanis(C19) \\sim Ueq, Uanis(C9) \\sim Ueq, Uanis(C4) \\sim Ueq, Uanis(C17) \\sim Ueq, Uanis(C18) \\sim Ueq, Uanis(C10) \\sim Ueq, Uanis(C21) \\sim Ueq, Uanis(C20) \\sim Ueq, Uanis(F1) \\sim Ueq, Uanis(B1) \\sim Ueq, Uanis(F4) \\sim Ueq, Uanis(F3) \\sim Ueq, Uanis(F2) \\sim Ueq, Uanis(O1) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01 5.a Ternary CH refined with riding coordinates: C19(H19), C16(H16) 5.b Aromatic/amide H refined with riding coordinates: C12(H12), C14(H14), C9(H9), C10(H10), C6(H6), C15(H15), C11(H11), C3(H3), C5(H5), C4(H4) 5.c Idealised Me refined as rotating group: C21(H21A,H21B,H21C), C17(H17A,H17B,H17C), C23(H23A,H23B,H23C), C18(H18A,H18B, H18C), C20(H20A,H20B,H20C) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.232 _oxdiff_exptl_absorpt_empirical_full_min 0.606 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au1 Au 0.70158(2) 0.27887(2) 0.4424(9) 0.01102(8) Uani 1 1 d . U . . . P1 P 0.73497(5) 0.32292(6) 0.3189(9) 0.0093(3) Uani 1 1 d . U . . . F1 F 0.7053(2) 0.4287(2) 0.8092(10) 0.0531(17) Uani 1 1 d . U . . . F4 F 0.7217(3) 0.3968(2) 0.9570(10) 0.0510(16) Uani 1 1 d . U . . . F3 F 0.6825(2) 0.3406(3) 0.8550(10) 0.0554(18) Uani 1 1 d . U . . . N1 N 0.6704(2) 0.2451(3) 0.5581(10) 0.0208(13) Uani 1 1 d . U . . . F2 F 0.7592(3) 0.3590(3) 0.8327(11) 0.0612(17) Uani 1 1 d . U . . . C21 C 0.7655(3) 0.3837(3) 0.5905(10) 0.0177(14) Uani 1 1 d . U . . . H21A H 0.760129 0.342802 0.589702 0.027 Uiso 1 1 calc GR . . . . H21B H 0.740723 0.402032 0.628235 0.027 Uiso 1 1 calc GR . . . . H21C H 0.796746 0.391746 0.617921 0.027 Uiso 1 1 calc GR . . . . C12 C 0.8328(2) 0.3302(3) 0.2926(10) 0.0140(13) Uani 1 1 d . U . . . H12 H 0.827086 0.309318 0.236729 0.017 Uiso 1 1 calc R . . . . C19 C 0.7637(2) 0.4065(3) 0.4906(10) 0.0147(13) Uani 1 1 d . U . . . H19 H 0.732356 0.395558 0.462835 0.018 Uiso 1 1 calc R . . . . C2 C 0.6508(2) 0.3767(3) 0.2586(11) 0.0161(14) Uani 1 1 d . U . . . C14 C 0.7374(2) 0.3064(3) 0.1282(10) 0.0151(13) Uani 1 1 d . U . . . H14 H 0.728328 0.345041 0.127662 0.018 Uiso 1 1 calc R . . . . C9 C 0.8496(2) 0.3938(3) 0.4527(11) 0.0160(13) Uani 1 1 d . U . . . H9 H 0.855881 0.415678 0.507249 0.019 Uiso 1 1 calc R . . . . C10 C 0.8876(2) 0.3747(3) 0.3989(10) 0.0179(15) Uani 1 1 d . U . . . H10 H 0.919188 0.383617 0.417074 0.021 Uiso 1 1 calc R . . . . C6 C 0.7225(3) 0.4349(3) 0.2651(10) 0.0160(13) Uani 1 1 d . U . . . H6 H 0.755633 0.438151 0.277465 0.019 Uiso 1 1 calc R . . . . O1 O 0.750000 0.250000 0.73549(2) 0.074(4) Uani 1 2 d DS TU P . . C1 C 0.6996(2) 0.3830(3) 0.2772(10) 0.0134(13) Uani 1 1 d . U . . . C15 C 0.7443(3) 0.2785(3) 0.0426(11) 0.0226(16) Uani 1 1 d . U . . . H15 H 0.741168 0.298460 -0.014989 0.027 Uiso 1 1 calc R . . . . C8 C 0.8025(2) 0.3817(2) 0.4290(11) 0.0131(13) Uani 1 1 d . U . . . C11 C 0.8796(2) 0.3429(3) 0.3189(11) 0.0188(13) Uani 1 1 d . U . . . H11 H 0.905580 0.329714 0.282307 0.023 Uiso 1 1 calc R . . . . C13 C 0.7435(2) 0.2791(3) 0.2142(10) 0.0123(13) Uani 1 1 d . U . . . C7 C 0.7942(2) 0.3481(3) 0.3476(10) 0.0132(13) Uani 1 1 d . U . . . C17 C 0.6042(3) 0.3025(4) 0.1716(11) 0.0284(18) Uani 1 1 d . U . . . H17A H 0.580464 0.330160 0.150959 0.043 Uiso 1 1 calc GR . . . . H17B H 0.589184 0.265287 0.177856 0.043 Uiso 1 1 calc GR . . . . H17C H 0.629885 0.300385 0.125147 0.043 Uiso 1 1 calc GR . . . . C3 C 0.6259(3) 0.4246(3) 0.2279(11) 0.0226(15) Uani 1 1 d . U . . . H3 H 0.592892 0.421593 0.214286 0.027 Uiso 1 1 calc R . . . . C5 C 0.6968(3) 0.4817(3) 0.2348(11) 0.0195(14) Uani 1 1 d . U . . . H5 H 0.712404 0.516998 0.226488 0.023 Uiso 1 1 calc R . . . . C4 C 0.6487(3) 0.4769(3) 0.2169(11) 0.0265(18) Uani 1 1 d . U . . . H4 H 0.631097 0.509061 0.197129 0.032 Uiso 1 1 calc R . . . . C16 C 0.6247(2) 0.3206(3) 0.2666(11) 0.0171(14) Uani 1 1 d . U . . . H16 H 0.648539 0.291445 0.285582 0.021 Uiso 1 1 calc R . . . . C23 C 0.6413(4) 0.2026(4) 0.7152(11) 0.044(3) Uani 1 1 d . U . . . H23A H 0.607649 0.192392 0.709831 0.065 Uiso 1 1 calc GR . . . . H23B H 0.645263 0.230533 0.765559 0.065 Uiso 1 1 calc GR . . . . H23C H 0.660030 0.168811 0.729906 0.065 Uiso 1 1 calc GR . . . . C18 C 0.5867(3) 0.3226(4) 0.3431(11) 0.0278(17) Uani 1 1 d . U . . . H18A H 0.601537 0.332451 0.403222 0.042 Uiso 1 1 calc GR . . . . H18B H 0.571411 0.285514 0.348287 0.042 Uiso 1 1 calc GR . . . . H18C H 0.562797 0.351147 0.326915 0.042 Uiso 1 1 calc GR . . . . C20 C 0.7667(3) 0.4711(3) 0.4909(11) 0.0223(16) Uani 1 1 d . U . . . H20A H 0.740006 0.486574 0.527013 0.033 Uiso 1 1 calc GR . . . . H20B H 0.765190 0.485140 0.426203 0.033 Uiso 1 1 calc GR . . . . H20C H 0.796731 0.482926 0.519734 0.033 Uiso 1 1 calc GR . . . . C22 C 0.6575(3) 0.2264(3) 0.6278(11) 0.0266(17) Uani 1 1 d . U . . . B1 B 0.7167(4) 0.3820(4) 0.8629(12) 0.032(2) Uani 1 1 d . U . . . H1 H 0.7395(4) 0.2781(2) 0.7651(6) 1.8(19) Uiso 1 1 d D . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Au1 0.00886(11) 0.01211(12) 0.01209(13) -0.00065(11) 0.00191(10) -0.00037(8) P1 0.0067(6) 0.0098(6) 0.0115(8) -0.0003(6) -0.0001(6) 0.0021(6) F1 0.089(5) 0.032(3) 0.039(3) 0.009(2) -0.028(3) 0.001(3) F4 0.095(4) 0.030(2) 0.028(3) -0.003(2) -0.018(3) 0.014(3) F3 0.054(3) 0.046(3) 0.066(4) 0.019(3) -0.036(3) -0.020(3) N1 0.015(3) 0.020(3) 0.027(3) 0.003(2) 0.011(2) 0.005(2) F2 0.058(4) 0.056(4) 0.069(5) 0.002(3) 0.004(4) 0.005(3) C21 0.017(3) 0.021(3) 0.016(4) -0.005(3) 0.003(3) -0.002(3) C12 0.013(3) 0.014(3) 0.015(3) 0.002(2) 0.004(2) 0.000(2) C19 0.010(3) 0.015(3) 0.019(3) -0.006(2) -0.002(2) -0.003(2) C2 0.015(3) 0.020(3) 0.013(3) -0.004(2) -0.003(2) 0.004(2) C14 0.021(3) 0.013(3) 0.011(3) 0.001(2) 0.001(3) 0.001(2) C9 0.010(2) 0.019(3) 0.020(3) 0.002(3) -0.004(3) -0.002(2) C10 0.006(3) 0.023(3) 0.025(3) 0.002(3) 0.001(2) -0.001(2) C6 0.021(3) 0.016(3) 0.011(3) 0.001(2) 0.001(3) 0.002(2) O1 0.093(9) 0.068(7) 0.062(7) 0.000 0.000 -0.008(7) C1 0.013(3) 0.015(3) 0.012(3) -0.001(2) -0.003(2) 0.004(2) C15 0.028(3) 0.023(3) 0.016(3) 0.003(3) 0.004(3) 0.008(3) C8 0.012(2) 0.011(2) 0.017(4) 0.002(2) -0.002(2) -0.003(2) C11 0.011(3) 0.020(3) 0.025(3) 0.003(3) 0.005(3) 0.000(2) C13 0.010(2) 0.015(3) 0.012(3) 0.000(2) 0.000(2) 0.002(2) C7 0.012(3) 0.011(3) 0.017(3) 0.004(2) 0.001(2) 0.000(2) C17 0.023(3) 0.038(4) 0.024(4) -0.013(3) -0.005(3) -0.001(3) C3 0.022(3) 0.027(3) 0.019(3) -0.004(3) -0.007(3) 0.009(3) C5 0.027(3) 0.018(3) 0.014(3) 0.001(3) -0.003(3) 0.005(3) C4 0.033(3) 0.027(3) 0.019(4) -0.004(3) -0.005(3) 0.014(3) C16 0.012(3) 0.021(3) 0.018(3) -0.005(3) -0.001(2) 0.001(2) C23 0.053(5) 0.047(5) 0.031(6) 0.019(4) 0.022(4) 0.019(4) C18 0.021(3) 0.036(4) 0.026(4) -0.010(3) 0.000(3) -0.004(3) C20 0.021(3) 0.018(3) 0.027(4) -0.006(3) -0.005(3) 0.006(3) C22 0.028(4) 0.025(3) 0.027(4) 0.001(3) 0.011(3) 0.008(3) B1 0.038(4) 0.030(4) 0.027(4) 0.006(3) -0.010(4) 0.001(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -4.4197 7.2980 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag P1 Au1 Au1 80.49(4) . 14_655 ? N1 Au1 Au1 102.09(17) . 14_655 ? N1 Au1 P1 175.57(18) . . ? C1 P1 Au1 112.7(2) . . ? C13 P1 Au1 115.4(2) . . ? C13 P1 C1 104.3(3) . . ? C7 P1 Au1 111.0(2) . . ? C7 P1 C1 108.4(3) . . ? C7 P1 C13 104.4(3) . . ? C22 N1 Au1 172.8(7) . . ? C11 C12 C7 120.8(7) . . ? C21 C19 C20 110.4(6) . . ? C8 C19 C21 112.4(6) . . ? C8 C19 C20 110.4(6) . . ? C1 C2 C16 123.4(6) . . ? C3 C2 C1 117.5(7) . . ? C3 C2 C16 119.1(6) . . ? C13 C14 C15 122.0(6) . . ? C10 C9 C8 121.9(7) . . ? C11 C10 C9 120.4(6) . . ? C5 C6 C1 119.9(7) . . ? C2 C1 P1 120.6(5) . . ? C6 C1 P1 118.0(5) . . ? C6 C1 C2 121.4(6) . . ? C15 C15 C14 119.4(4) 14_655 . ? C9 C8 C19 117.6(6) . . ? C9 C8 C7 117.8(6) . . ? C7 C8 C19 124.5(6) . . ? C10 C11 C12 119.3(7) . . ? C14 C13 P1 115.9(5) . . ? C14 C13 C13 118.6(4) . 14_655 ? C13 C13 P1 125.5(2) 14_655 . ? C12 C7 P1 119.0(5) . . ? C12 C7 C8 119.7(6) . . ? C8 C7 P1 121.2(5) . . ? C4 C3 C2 121.2(7) . . ? C4 C5 C6 120.1(7) . . ? C5 C4 C3 120.0(7) . . ? C2 C16 C17 111.1(6) . . ? C2 C16 C18 111.4(6) . . ? C18 C16 C17 112.1(6) . . ? N1 C22 C23 179.8(11) . . ? F1 B1 F4 110.8(8) . . ? F3 B1 F1 111.2(8) . . ? F3 B1 F4 109.2(9) . . ? F3 B1 F2 107.4(8) . . ? F2 B1 F1 110.0(9) . . ? F2 B1 F4 108.1(8) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Au1 Au1 3.0456(4) 14_655 ? Au1 P1 2.2488(17) . ? Au1 N1 2.029(6) . ? P1 C1 1.833(7) . ? P1 C13 1.830(7) . ? P1 C7 1.816(7) . ? F1 B1 1.382(11) . ? F4 B1 1.391(13) . ? F3 B1 1.378(12) . ? N1 C22 1.145(11) . ? F2 B1 1.381(13) . ? C21 C19 1.521(10) . ? C12 C11 1.400(10) . ? C12 C7 1.403(9) . ? C19 C8 1.517(9) . ? C19 C20 1.531(9) . ? C2 C1 1.404(9) . ? C2 C3 1.403(10) . ? C2 C16 1.521(10) . ? C14 C15 1.398(10) . ? C14 C13 1.394(9) . ? C9 C10 1.389(10) . ? C9 C8 1.395(8) . ? C10 C11 1.382(11) . ? C6 C1 1.398(10) . ? C6 C5 1.391(10) . ? C15 C15 1.386(14) 14_655 ? C8 C7 1.424(10) . ? C13 C13 1.424(12) 14_655 ? C17 C16 1.530(10) . ? C3 C4 1.403(12) . ? C5 C4 1.381(11) . ? C16 C18 1.525(10) . ? C23 C22 1.440(12) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Au1 P1 C1 C2 -50.5(6) . . . . ? Au1 P1 C1 C6 129.2(5) . . . . ? Au1 P1 C13 C14 144.6(5) . . . . ? Au1 P1 C13 C13 -36.6(9) . . . 14_655 ? Au1 P1 C7 C12 123.1(5) . . . . ? Au1 P1 C7 C8 -51.8(6) . . . . ? C21 C19 C8 C9 -63.8(8) . . . . ? C21 C19 C8 C7 117.6(7) . . . . ? C19 C8 C7 P1 -9.0(9) . . . . ? C19 C8 C7 C12 176.2(6) . . . . ? C2 C3 C4 C5 1.2(12) . . . . ? C9 C10 C11 C12 0.3(11) . . . . ? C9 C8 C7 P1 172.4(5) . . . . ? C9 C8 C7 C12 -2.4(10) . . . . ? C10 C9 C8 C19 -177.8(6) . . . . ? C10 C9 C8 C7 0.9(10) . . . . ? C6 C5 C4 C3 -0.9(12) . . . . ? C1 P1 C13 C14 20.4(6) . . . . ? C1 P1 C13 C13 -160.8(8) . . . 14_655 ? C1 P1 C7 C12 -112.6(6) . . . . ? C1 P1 C7 C8 72.5(6) . . . . ? C1 C2 C3 C4 -0.5(11) . . . . ? C1 C2 C16 C17 -117.9(8) . . . . ? C1 C2 C16 C18 116.3(8) . . . . ? C1 C6 C5 C4 0.1(11) . . . . ? C15 C14 C13 P1 178.0(6) . . . . ? C15 C14 C13 C13 -0.9(12) . . . 14_655 ? C8 C9 C10 C11 0.2(11) . . . . ? C11 C12 C7 P1 -172.0(5) . . . . ? C11 C12 C7 C8 2.9(10) . . . . ? C13 P1 C1 C2 75.4(6) . . . . ? C13 P1 C1 C6 -104.9(6) . . . . ? C13 P1 C7 C12 -1.9(6) . . . . ? C13 P1 C7 C8 -176.7(5) . . . . ? C13 C14 C15 C15 2.6(14) . . . 14_655 ? C7 P1 C1 C2 -173.8(6) . . . . ? C7 P1 C1 C6 5.9(7) . . . . ? C7 P1 C13 C14 -93.3(6) . . . . ? C7 P1 C13 C13 85.5(8) . . . 14_655 ? C7 C12 C11 C10 -1.8(11) . . . . ? C3 C2 C1 P1 179.3(6) . . . . ? C3 C2 C1 C6 -0.4(11) . . . . ? C3 C2 C16 C17 59.6(9) . . . . ? C3 C2 C16 C18 -66.1(9) . . . . ? C5 C6 C1 P1 -179.1(6) . . . . ? C5 C6 C1 C2 0.6(11) . . . . ? C16 C2 C1 P1 -3.1(10) . . . . ? C16 C2 C1 C6 177.2(7) . . . . ? C16 C2 C3 C4 -178.2(7) . . . . ? C20 C19 C8 C9 59.8(8) . . . . ? C20 C19 C8 C7 -118.8(7) . . . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 -12 2526.16 82.49 0 0 -10 54.76 11.88 0 0 -8 8201.28 122.98 0 0 -6 4.92 3.78 0 0 -4 3688.39 56.24 0 0 2 3.45 1.24 0 0 4 5299.94 55.02 0 0 6 11.38 4.37 0 0 8 9630.75 127.8 0 0 10 4.06 3.43 0 0 10 16.11 7.55 0 0 12 2431.03 51.04 0 0 14 8.46 3.93 0 0 16 1828.11 32.27 0 2 -12 0.7 4.72 0 -2 -12 3.1 5.8 0 2 -10 5648.86 112.32 0 -2 -10 5422.36 115.25 0 -2 -8 31.12 8.45 0 2 -8 6.22 4.91 0 2 -6 4558.89 75.96 0 2 -4 6.66 3.2 0 -2 -4 4.53 3.43 0 2 -2 4765.73 40.62 0 2 -2 4854.11 29.23 0 2 0 20.85 1.92 0 -2 2 4498.62 40.24 0 2 2 5018.01 31.15 0 -2 4 8.51 2.88 0 -2 6 4759.55 72.57 0 -2 8 0.47 3.5 0 -2 10 4964.4 67.57 0 2 10 4953.62 68.56 0 -2 10 4930.02 109.25 0 2 12 10.51 4.61 0 -2 12 8.16 4.15 0 -2 14 1448.17 36.09 0 2 16 5.7 2.82 0 -2 16 5.52 2.64 0 -4 -12 1269.26 62.11 0 4 -10 61 12.19 0 4 -8 2485.56 66.27 0 4 -6 11.04 4.62 0 -4 -6 2.96 4.63 0 -4 -4 6664.19 83.44 0 4 -4 7128.48 75.69 0 -4 -2 2.61 2.88 0 4 -2 7.09 1.99 0 4 0 391.07 11.67 0 4 0 396.68 7.95 0 4 2 14.29 2.18 0 4 2 15.85 2.34 0 -4 2 15.86 3.45 0 4 4 8187.52 68.88 0 -4 4 7972.99 79.8 0 4 6 3.37 3.11 0 -4 6 9.23 4.41 0 4 8 2301.23 63.3 0 -4 8 2035.75 59.61 0 4 10 6.25 5.97 0 4 10 5.55 3.68 0 -4 10 5.78 3.32 0 4 12 1491.88 40.15 0 -4 12 1470.36 38.49 0 4 14 10.34 3.98 0 -4 14 4.49 3.55 0 4 16 729.46 19.69 0 -4 16 716.01 18.76 0 -6 -10 898.67 51.47 0 6 -10 1016.01 44.76 0 -6 -8 6.74 5.39 0 6 -8 9.23 5.19 0 -6 -6 3720.53 78.93 0 6 -6 4017.7 71.62 0 -6 -4 143.61 13.05 0 6 -4 2.09 1.95 0 6 -2 5001.2 52.09 0 -6 -2 4839.43 59.4 0 6 0 8.94 1.65 0 -6 0 14.49 2.66 0 6 2 5874.76 44.51 0 -6 2 5949.83 57.71 0 6 2 5990.45 60.26 0 6 4 0.33 1.33 0 6 6 3656.87 62.95 0 6 8 7.72 4.52 0 6 10 1075.19 33.06 0 -6 10 999.39 29.04 0 6 10 1081.99 52.69 0 -6 12 6.74 3.5 0 6 12 7.41 4.07 0 6 14 638.02 23.38 0 -6 14 599.63 21.22 0 6 16 4.62 2 0 -6 16 2.25 1.67 0 -8 -10 2.51 5.19 0 -8 -8 57.54 12.34 0 -8 -6 13.04 6.45 0 8 -6 5.37 2.71 0 -8 -4 912.13 33.79 0 -8 -2 6.05 2.82 0 -8 0 241.33 11.62 0 8 0 244.7 13.65 0 8 0 229 8.62 0 -8 0 264.57 10.88 0 8 2 11.37 2.11 0 8 2 7.08 1.96 0 -8 2 8.74 2.96 0 8 4 830.35 23.49 0 8 6 5.65 3.38 0 8 8 36.25 4.76 0 8 8 30.92 8.25 0 8 10 2.89 4.48 0 8 10 4.68 2.83 0 -8 12 226.23 13.46 0 8 12 252.73 16.24 0 -8 14 4.76 2.55 0 8 14 7.02 3.36 0 8 16 12.84 3.65 0 -8 16 4.74 1.53 0 10 -10 126.25 7.94 0 -10 -10 127.37 20.78 0 10 -8 2.68 2.96 0 -10 -8 9.72 6.37 0 10 -8 16.8 3.11 0 -10 -6 1093.48 46.27 0 -10 -4 7.7 4.24 0 -10 -2 861.37 27.03 0 -10 0 1.89 2.01 0 -10 0 4.17 1.8 0 10 2 1005.13 19.68 0 10 2 1059.85 23.12 0 10 4 2.06 2.04 0 10 6 1058.93 36.45 0 10 8 3 2.32 0 10 8 6.63 4.39 0 10 10 136.37 10.59 0 10 10 167.93 13.37 0 10 10 160.93 21.45 0 10 12 11.19 4.18 0 -10 12 6.02 2.65 0 10 14 190.73 14 0 10 16 6.72 2.95 0 -12 -10 2.5 5.64 0 12 -10 2.47 1.93 0 12 -8 551.75 17.24 0 -12 -8 553.39 38.73 0 12 -8 539.3 20.86 0 -12 -6 8.59 5.33 0 12 -6 10.79 2.59 0 -12 -4 4623.08 81.27 0 -12 -2 15.88 4.2 0 12 -2 5.74 2.3 0 12 0 1054.24 23.45 0 -12 0 1203.66 34.31 0 12 2 11.47 2.85 0 -12 2 4.85 3.41 0 12 4 4177.18 59.31 0 12 6 3.93 3.37 0 12 6 2.16 1.96 0 12 8 494.18 32.89 0 12 8 494.22 18.93 0 12 10 9.69 3.75 0 12 12 1421.01 39.78 0 12 14 2.5 3.78 0 12 16 345.68 12.4 0 14 -10 1961.59 33.03 0 14 -8 15.53 3.65 0 -14 -8 18.91 8.62 0 14 -8 0.23 4.03 0 14 -6 1670.2 30.88 0 -14 -6 1667.25 57.53 0 14 -6 1658.21 36.52 0 14 -4 1.75 1.97 0 14 -4 13.84 3.13 0 14 -2 1795.79 37.05 0 -14 -2 2207.71 54.27 0 14 0 8.1 2.56 0 -14 0 9.38 4.22 0 14 2 1838.5 35.88 0 -14 2 1980.79 51.9 0 14 4 13.9 3.08 0 14 6 1462.72 31.04 0 14 6 1520.22 35.9 0 14 8 7.2 4.06 0 14 10 1778.92 39.6 0 14 10 1577.8 41.72 0 14 12 38.53 7 0 14 14 1064.72 29.44 0 16 -10 6.88 2.65 0 16 -8 2690.18 41.62 0 16 -8 2585.67 47.33 0 16 -6 14.64 5.65 0 16 -6 7.41 3.05 0 16 -4 4707.23 63.42 0 -16 -4 4775.11 93.51 0 16 -4 4772.36 54.47 0 16 -2 4.19 4.13 0 -16 -2 1.86 2.89 0 16 -2 13.59 3.3 0 16 -2 16.38 3.66 0 16 0 3392.37 46.89 0 -16 0 3679.16 76.66 0 16 2 5.23 3.21 0 -16 2 2.3 2.99 0 16 4 4867.81 55.23 0 16 4 4843.78 63.5 0 16 6 2.87 2.58 0 16 6 12.68 4.51 0 16 8 3085.66 51.31 0 16 8 2882.36 55.38 0 16 10 3.9 4.13 0 16 12 1846.72 42.95 0 16 14 2.61 2.98 0 18 -10 2256.57 34.04 0 18 -8 12.02 3.41 0 18 -8 1.86 4.73 0 18 -6 4044.1 62.22 0 18 -6 4049.4 52.96 0 18 -4 0.26 5.71 0 18 -4 7.81 3.11 0 18 -2 4597.43 64.3 0 -18 -2 4825.74 99.26 0 18 0 57.62 7.76 0 -18 0 12.21 5.89 0 18 2 4615.09 65.22 0 -18 2 4419.37 95.52 0 18 2 4429.11 53.8 0 18 4 0.53 3.6 0 18 4 24.86 4.79 0 18 6 4072.41 65.25 0 18 6 4184.23 59.51 0 18 8 4.72 4.13 0 18 8 7.79 3.87 0 18 10 2173.49 47.69 0 18 10 2174.37 43.25 0 18 12 2.25 3.45 0 18 14 1420.55 24.31 0 20 -8 2015.96 40.15 0 20 -6 3.54 5.31 0 20 -4 1248.56 36.21 0 -20 -4 1090.16 49.96 0 20 -2 29.02 7.99 0 -20 -2 5.78 5.25 0 20 0 4352.54 66.61 0 -20 0 4680.36 103.52 0 20 2 6.2 3.03 0 20 2 30.09 6.55 0 20 4 1559.26 36.7 0 20 4 1444.28 39.27 0 20 6 24.34 5.24 0 20 6 3.43 4.04 0 20 8 1847.18 40.72 0 20 8 1674.96 41.5 0 20 10 4.1 4.04 0 20 12 739.76 21.5 0 22 -8 2.14 3.33 0 22 -6 885.01 27.81 0 22 -4 11.17 6.18 0 22 -2 1216.78 36.42 0 22 0 9.04 7.17 0 22 2 1360.06 33.62 0 22 2 1280.87 37.49 0 22 4 5.27 3.52 0 22 4 7.13 4.6 0 22 6 1097.31 31.7 0 22 6 971.17 31.7 0 22 8 4.81 3.46 0 22 8 7.27 4.17 0 22 10 662.49 21.77 0 24 -8 198.6 10.2 0 24 -6 3.31 4.08 0 24 -4 430.14 19.76 0 24 -2 21.54 8.33 0 24 0 451.67 22.63 0 24 2 9.71 6.57 0 24 4 388.14 20.27 0 24 6 6.81 3.63 0 24 6 7.54 4.28 0 24 8 250.03 13.37 0 24 10 3.19 2.69 0 26 -6 7.98 3.27 0 26 -4 3.3 3.93 0 26 -2 34.91 7.39 0 26 0 4.32 6.37 0 26 2 28.98 7.89 0 26 4 4.82 5.23 0 26 6 9.31 4.59 0 26 8 2.06 3.09 0 28 -4 32.3 4.14 0 28 -2 0.68 3.19 0 28 0 409.72 15.74 0 28 2 6.7 4.41 0 28 4 68.6 6.79 -1 1 -11 1604.79 63.91 -1 -1 -11 1585.54 64.73 1 1 -11 1501.58 60.67 1 -1 -11 1444.04 60.87 1 -1 -9 2639.69 74.89 -1 -1 -9 2627.77 74.05 1 1 -9 2585.61 72.23 -1 1 -9 2589.86 73.98 1 -1 -7 4786.11 87.71 1 1 -7 4773.53 84.99 -1 -1 -7 4685.63 88.09 -1 1 -5 3192.57 57.75 1 1 -5 3289.36 58.55 -1 1 -3 1123.74 9.61 -1 1 -3 1106.83 25.87 1 1 -3 1097.28 25.7 -1 -1 -3 1087.19 26.46 -1 -1 -1 4639.52 32.16 -1 1 -1 4619.52 22.68 1 -1 1 4414.41 22.22 -1 1 1 4315.65 23.17 1 -1 3 1000.97 19.83 1 1 3 1025.08 19.64 -1 -1 3 1017.07 23.56 -1 1 3 1075.7 10.35 -1 -1 5 3408.6 55.51 1 -1 5 3283.79 49.94 1 1 5 3366.87 50.39 1 -1 7 4782.33 79.5 -1 -1 7 4638.37 81.05 1 1 7 4813.75 78.37 1 1 9 2434.46 70.54 -1 -1 9 2234.01 68.77 1 -1 9 2449.42 70.02 -1 -1 9 2226.19 42.41 1 -1 9 2287.62 42.54 1 -1 11 1301.59 59.61 1 1 11 1227.36 58.84 1 -1 11 1300.45 36.27 -1 -1 11 1336.61 36.59 -1 -1 13 876.65 29.72 1 -1 13 887.85 30.46 1 -1 15 1001.35 27.61 -1 -1 15 988.33 27.14 1 -1 17 868.8 18.04 -1 -1 17 894.2 18.11 -1 -3 -11 1229.53 58.8 1 -3 -11 1261.73 58.73 -1 3 -11 1299.94 56.77 1 3 -11 1302.37 55.17 1 -3 -9 2458.4 75.17 1 3 -9 2556.6 70.17 1 3 -7 2967.57 66.42 -1 3 -7 2962.09 68.13 -1 3 -5 650.5 26.59 -1 -3 -5 642.98 27.19 1 -3 -5 661.75 28.74 1 3 -5 700.86 26.37 1 3 -3 4674.51 49.71 -1 -3 -3 4797.96 57.57 1 -3 -3 4806.67 63.74 -1 3 -1 2903.69 23.68 -1 3 -1 2894.28 27 -1 -3 -1 2876.08 29.5 1 -3 1 2904.75 26.03 -1 -3 1 3111.1 30.27 -1 3 1 2844.71 19.42 1 3 1 2789.35 22.58 -1 3 3 4627.14 44.12 1 3 3 4790.72 43.67 1 -3 3 4570.59 46.93 -1 -3 3 4514.75 54.3 -1 3 3 4842.95 37.38 1 3 5 720.96 23.22 -1 3 5 719.96 23.8 -1 -3 5 680.18 26.02 1 -3 5 697.39 24.59 -1 -3 7 3059.99 66.56 -1 3 7 3223.78 66.94 1 -3 7 3266.66 66.72 1 3 7 2969.41 61.32 1 -3 9 2122.14 40.53 -1 -3 9 2130.5 40.62 1 3 9 2154.02 42.06 -1 3 9 2098.28 41.93 1 -3 9 2124.07 65.52 1 3 9 2210.13 67.43 -1 3 9 2276.35 69.73 -1 3 11 1122.06 33.99 -1 -3 11 1183.38 33.78 1 -3 11 1143.58 34.14 1 3 11 1129.65 34.73 1 3 11 1183.01 57.99 -1 3 11 1187.98 58.72 1 -3 13 1221.64 34.85 1 3 13 1135.63 34.72 -1 -3 13 1205.82 33.79 -1 3 13 1194.79 34.64 1 3 15 989.25 27.29 -1 -3 15 985.72 26.41 -1 3 15 1009.58 27.21 1 -3 15 968.47 26.41 1 -3 17 494.21 13.01 -1 -3 17 522.25 13.24 1 3 17 506.84 13.58 -1 3 17 519.58 13.57 -1 5 -11 1189.61 51.89 -1 5 -9 822.67 40.96 -1 -5 -9 766.9 43.77 1 5 -9 888.17 41.02 1 -5 -9 748.48 42.9 1 5 -7 440.99 25.53 -1 5 -7 413.37 26.26 1 -5 -7 421.63 28.82 -1 -5 -7 354.8 25.29 -1 -5 -5 2016.11 50.35 1 5 -5 2116.51 45.84 1 -5 -5 1977.4 53.06 -1 5 -5 2115.79 49.58 -1 5 -3 3249.4 36.89 1 -5 -3 3092.14 55.31 -1 5 -3 2976.89 39.54 -1 -5 -3 3163.59 49.55 1 5 -3 3363.34 39.49 -1 5 -1 827.56 18.8 -1 -5 -1 805.86 17.46 1 5 1 692.32 13.42 -1 5 1 649.11 9.68 -1 5 1 718.97 11.56 1 -5 1 786.7 16.96 -1 -5 1 766.2 18.14 -1 5 3 3410.27 38.14 1 5 3 3671.55 39.79 -1 5 3 3705.1 42.51 1 -5 3 3475.63 47.17 1 -5 5 1834.88 42.63 -1 5 5 1801.43 38.46 1 5 5 1854.4 38.34 -1 5 7 682.77 31.13 1 -5 7 651.44 30.84 1 5 7 645.18 29.19 1 5 9 872.65 42.93 -1 5 9 895.04 44.34 1 5 9 766.34 21.02 1 5 9 799.15 26.44 -1 -5 9 782.11 24.45 1 -5 9 794.73 24.69 -1 5 9 821.28 26.85 1 5 11 1113.18 56.67 -1 5 11 1114.65 57.28 -1 5 11 1163.94 34.76 1 5 11 1108.69 34.62 1 -5 11 1074.97 32.12 -1 -5 11 1114.12 32.21 -1 -5 13 683.13 24.59 1 -5 13 658.87 24.59 1 5 13 642.46 25.66 -1 5 13 684.12 26.11 -1 -5 15 196.38 11.25 1 5 15 199.38 12.13 1 -5 15 189.51 11.19 -1 5 15 201.31 12.04 -1 5 17 250.57 8.78 1 -5 17 239.58 8.25 1 5 17 252.34 8.9 -1 -5 17 249.58 8.34 1 -7 -11 247.35 28.36 -1 -7 -11 303.65 31.08 -1 7 -9 230.14 9.95 -1 -7 -9 258.4 26.64 1 -7 -9 236.88 25.72 -1 7 -9 271.81 21.92 -1 -7 -7 595.4 33.94 1 7 -7 704.93 30 1 -7 -7 635.31 37.05 -1 7 -7 640.86 30.3 1 7 -5 1165.33 30.2 -1 -7 -5 1174.28 40.05 1 -7 -5 1163.26 43.04 -1 7 -3 638.51 19.86 -1 -7 -3 601.61 22.84 1 -7 -3 601.13 25.99 -1 7 -1 2918.6 42.22 1 -7 -1 2915.19 48.02 -1 7 1 3267.41 29.16 -1 -7 1 3389.6 43.72 1 -7 1 3356.17 41.68 -1 7 3 587.04 16.35 1 7 3 633.15 17.96 1 7 3 631.08 17.34 -1 7 3 660.51 21.66 1 -7 3 607.11 21.96 -1 -7 3 641.51 23.72 -1 7 5 871.51 27.62 1 7 5 921.28 27.76 1 7 7 627.18 29.34 -1 7 7 625.74 30.47 1 7 9 313.02 26.25 -1 7 9 301.26 26.32 -1 7 9 299.37 16.72 1 7 9 291.38 16.76 1 -7 9 264.83 14.12 -1 -7 9 321.98 15.27 1 7 9 289.91 13.4 -1 7 9 277.32 13.51 1 7 11 325.3 31.08 -1 7 11 286.83 29.28 1 7 11 316.68 18.91 1 -7 11 313.07 16.64 -1 -7 11 302.47 15.86 -1 7 11 377.29 19.85 -1 -7 13 178.47 11.95 -1 7 13 184.26 13.47 1 7 13 185.59 13.78 1 -7 13 167.9 11.9 1 7 15 154.43 10.12 -1 7 15 160.5 10.16 1 -7 15 161.76 9.42 -1 -7 15 159.5 9.21 1 7 17 141.34 7.68 -1 -9 -11 208.41 26.32 1 -9 -11 212.72 26.59 1 -9 -9 251.04 27.1 -1 -9 -9 232 25.86 1 9 -9 210.12 9.76 -1 9 -9 212.78 10.11 -1 -9 -7 149.75 17.9 1 -9 -7 167.39 20.06 1 -9 -5 330.69 23.94 -1 -9 -5 314.18 21.44 1 -9 -3 379.6 21.57 -1 -9 -3 351.29 18.22 -1 9 -1 70.1 7.75 -1 9 -1 73.12 5.23 -1 -9 -1 79.92 6.33 1 -9 -1 77.03 8.24 1 9 -1 81.87 6.46 -1 9 1 31.24 2.49 1 9 1 29.7 3.72 -1 9 1 31.1 3.36 -1 -9 1 31.69 4.98 1 -9 1 42.68 5.59 1 9 3 391.42 15.13 -1 9 3 358.74 13.61 1 9 3 385.84 14.38 -1 -9 3 403.44 19.93 1 -9 3 392.81 19.36 1 9 5 441.76 20.15 -1 9 5 447.32 20.63 1 9 7 141.89 14.55 -1 9 7 145.42 15.54 1 9 7 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46.45 8 8 8 66.39 10.78 -8 8 8 53.1 6.43 -8 -8 8 40.26 4.92 8 8 8 77.69 6.69 8 8 8 45.18 6.2 8 -8 8 58.12 6.17 8 8 10 1744.4 63.84 8 8 10 1813.36 43.46 8 -8 10 1804.24 38.54 -8 -8 10 1833.19 34.05 8 8 10 1817.7 35.4 8 8 12 16.81 5.69 8 -8 12 17.04 4.88 -8 8 12 16.06 4.6 -8 -8 12 13.31 3.63 8 8 14 728.23 23.7 8 8 14 725.98 24.13 8 -8 14 719.1 21.65 8 8 16 65.99 5.17 -8 8 16 83.71 5.84 -8 10 -14 98.3 8.76 -8 10 -12 1470.6 28.11 -8 10 -10 142.96 9.6 -8 -10 -10 156.4 20.89 8 -10 -10 108.91 19.6 -8 -10 -8 957.3 44.47 8 -10 -8 855.01 52.28 -8 10 -8 895.67 25.34 -8 -10 -6 294.31 20.55 8 -10 -6 283.56 28.61 -8 10 -6 278.41 16.62 -8 -10 -4 3615.49 60.61 8 -10 -4 3465.62 94.23 -8 10 -4 3519.78 61.94 -8 10 -2 316.8 19.06 8 10 -2 313.89 18.89 -8 -10 -2 328.35 18.71 8 10 0 578.52 23.93 -8 10 0 598.21 26.83 8 10 2 243.93 15.66 -8 10 2 213.57 16.56 8 10 4 3436.57 62.36 -8 10 4 3396.83 66.65 8 10 6 289.22 19.95 -8 10 6 288.87 19.42 8 10 6 294.42 12.04 8 10 8 938.56 41.38 8 10 8 974.77 24.69 8 10 8 1027.31 30.73 8 10 10 106.58 16.35 8 10 10 115.8 12.01 8 10 10 115.59 9.44 -8 10 10 127.09 10.69 8 -10 12 1601.85 35.67 8 10 12 1660.25 42.33 -8 10 12 1450.83 41.36 8 10 12 1519.42 37.25 8 10 14 105.69 8.92 -8 10 14 122.7 10.54 -8 12 -14 534.6 17.72 -8 12 -12 357.23 18.63 -8 12 -12 333.24 13.23 -8 12 -10 458.67 22.67 -8 12 -10 467.06 17.37 -8 12 -8 647.13 27.12 -8 12 -8 723.88 23.62 -8 -12 -8 725.9 38.56 8 -12 -8 717 49.06 -8 12 -8 779.8 22.48 -8 12 -6 1433.59 32.41 -8 -12 -6 1477.18 46.25 8 -12 -6 1401.76 66.4 -8 12 -6 1455.21 29.23 -8 12 -4 1037.11 36.81 -8 -12 -4 1140.9 40.23 8 -12 -4 1080.58 56.51 -8 12 -4 1009.53 23.68 -8 12 -2 846.85 34.32 8 12 -2 840.55 32.58 -8 12 0 689.15 31.44 8 12 0 665.2 27.89 -8 -12 2 1043.68 37.5 -8 12 2 1087.93 41.03 8 12 2 1028.3 34.97 -8 12 4 1250.97 44.78 8 12 4 1206.47 39.56 8 12 4 1178.33 37.74 -8 12 6 1340.17 30.19 8 12 6 1296.17 27.37 -8 12 6 1305.6 45.56 8 12 6 1496.82 31.83 -8 12 6 1289.8 33.1 8 12 6 1213.12 42.74 -8 12 6 1485.09 36.34 8 12 8 736.61 22.71 8 12 8 686.66 36.98 -8 12 8 685.6 26.89 8 12 10 432.94 20.17 -8 12 10 370.26 21.28 8 12 10 385.94 17.62 8 12 12 299.61 16.47 -8 12 12 271.14 17.96 8 12 14 380.61 15.6 -8 12 14 474.53 19.03 -8 14 -12 214.77 10.2 -8 14 -12 222.23 13.43 -8 14 -10 908.72 30.94 -8 14 -10 854.86 23.44 -8 14 -8 605.38 26.17 8 14 -8 643.68 21.67 -8 14 -8 601.78 22.28 -8 14 -8 627.86 20.7 8 14 -6 1838.69 36.19 -8 14 -6 1719.38 37.79 -8 14 -6 1563.32 41.79 -8 -14 -6 1710.32 57.14 8 -14 -6 1651.69 73.69 -8 14 -4 436.66 15.14 -8 14 -4 426.76 16.22 8 14 -4 462.6 27.55 -8 14 -4 405.57 20.56 8 14 -4 434.24 17.17 -8 14 -4 412.72 18.76 8 -14 -4 412.04 35.76 -8 14 -4 428.65 25.86 -8 14 -2 2009.16 56.95 8 -14 -2 2042.28 76.62 -8 14 -2 1992.3 33.37 -8 14 -2 2119.5 33.88 -8 -14 0 748.64 33.56 -8 14 0 703.38 19.94 8 14 0 689.31 30.91 -8 14 0 706.82 34.66 -8 -14 2 2072.83 57.53 -8 14 2 2091.49 35.65 -8 14 2 1989.71 59.78 8 14 2 2062.72 53.64 8 14 4 413.39 24.97 8 14 4 393.35 23.15 -8 14 4 431.12 15.74 -8 14 4 482.08 17.92 8 14 4 508.04 18.45 -8 14 4 452.07 19.28 -8 14 4 425.59 28.77 -8 14 6 1891.59 37.73 8 14 6 1931.37 36.05 -8 14 6 1891.88 43.01 -8 14 6 1933.3 34.67 8 14 6 1799.26 55.17 8 14 8 564.59 22.45 -8 14 8 505.23 24.29 8 14 8 526.84 34.12 8 14 8 544.11 20.7 8 14 10 813.4 26.12 8 14 10 855.37 28.38 8 14 12 217.73 13.56 -8 14 12 200.92 15.13 8 14 14 668.04 18.29 -8 14 14 813.11 22 -8 16 -12 1110.85 25.78 -8 16 -12 1077.52 21.3 -8 16 -10 133.88 9.22 -8 16 -10 137.41 11.34 -8 16 -8 1122.49 27.71 -8 16 -8 1086.68 34.05 8 16 -8 1106.76 27.85 -8 16 -8 1047.73 29.94 -8 16 -6 146.21 13.1 8 16 -6 174.79 18.43 8 16 -6 184.03 12 -8 16 -6 146.19 12.09 8 16 -4 1899.81 58.33 8 16 -4 1810.7 36.42 -8 16 -4 1828.42 41.03 -8 16 -4 1835.98 33.03 -8 16 -4 1857.8 35.49 -8 16 -2 439.37 16.82 -8 16 -2 431.46 16.7 8 16 -2 470.06 27.72 -8 -16 -2 453.28 29.2 8 16 -2 431.31 17.28 -8 16 -2 429.36 19.76 -8 16 -2 437.47 29.2 -8 16 -2 418.1 20.71 -8 16 0 1964.23 63.41 -8 16 0 1925.34 32.82 8 16 0 2002.16 56.33 -8 16 0 2137.77 38.02 -8 -16 0 2058.08 60.08 8 16 0 2070.74 37.06 -8 16 0 2111.08 42.18 -8 16 0 2106.52 44.67 -8 16 2 424.49 19.97 8 16 2 394.8 24.97 -8 16 2 418.94 17.35 -8 -16 2 358.25 26.02 8 16 2 429.59 17.33 -8 16 2 431.91 19.51 -8 16 2 396.64 29.57 -8 16 4 1693.35 41.18 8 16 4 1784.67 36.99 -8 16 4 1607.5 39.16 -8 16 4 1685.5 35.26 8 16 4 1504.31 50.44 8 16 6 218.43 13.85 -8 16 6 177.8 14.04 -8 16 6 204.48 12.11 8 16 6 201.86 12.5 8 16 8 1093.16 30.31 -8 16 8 1043.39 35.47 8 16 10 139.61 11.04 8 16 10 139.65 11.43 -8 16 10 131.24 12.9 8 16 12 1028.82 26.96 -8 16 12 975.61 30.15 -8 18 -12 54.78 4.49 -8 18 -10 1082.87 27.35 -8 18 -10 1073.57 24.2 -8 18 -8 7.78 3.22 8 18 -8 13.84 3.8 -8 18 -8 7.99 3.92 -8 18 -8 8.65 3.87 -8 18 -6 1581.11 33.93 -8 18 -6 1544.27 37.67 8 18 -6 1617.15 34.29 -8 18 -6 1522.63 29.25 -8 18 -6 1555.14 40.75 -8 18 -4 540.8 20.04 8 18 -4 517.59 30.85 -8 -18 -4 521.85 34.02 8 18 -4 529.2 20.57 -8 18 -4 523.67 23.27 -8 18 -4 519.22 18.77 -8 18 -4 498.82 23.69 -8 18 -2 1946.66 37.28 8 18 -2 2041.89 60.77 -8 -18 -2 1949.55 64.33 8 18 -2 1871.94 38.13 -8 18 -2 1903.06 43.66 -8 18 -2 1814.17 44.71 -8 18 -2 2011.81 38.34 -8 18 0 44.37 6.24 8 18 0 36.44 8.5 -8 18 0 39.26 5.36 -8 -18 0 48.1 10.43 8 18 0 40.98 6.78 -8 18 0 51.72 8.55 -8 18 0 45.71 7.37 8 18 2 1678.29 54.68 8 18 2 1870.13 38.32 -8 18 2 1815.61 42.06 -8 -18 2 1729.73 61.36 -8 18 2 1872.49 44.2 -8 18 2 1906.05 39.35 -8 18 4 552.79 24.69 -8 18 4 567.86 21.93 8 18 4 574.57 22.12 -8 18 4 523.62 23.66 -8 18 6 1854.6 38.12 8 18 6 1759.91 39.6 8 18 8 14.4 4.22 8 18 8 18.98 4.81 -8 18 8 14.37 5.39 8 18 10 1050.43 28.75 8 18 10 1051.92 28.97 8 18 12 56.52 5.85 -8 18 12 66 7.17 -8 20 -10 117.88 7.38 -8 20 -8 875.97 23.01 8 20 -8 816.19 21.5 -8 20 -8 807.64 23.81 -8 20 -8 824.79 24.14 -8 20 -6 299.67 14.57 -8 20 -6 309.58 16.76 8 20 -6 289.56 14.33 -8 20 -6 296.04 16.52 8 20 -4 1658.75 36.07 -8 20 -4 1603.59 40.36 -8 20 -4 1715.68 35.68 -8 20 -4 1626.36 40.91 -8 20 -4 1669.33 34.51 -8 20 -2 350.68 20.31 8 20 -2 370.27 18.17 -8 20 -2 367.77 16.61 -8 20 -2 401.44 17.96 -8 20 -2 373.59 20.38 -8 20 0 949.44 28.57 -8 20 0 865.94 30.96 8 20 0 892.81 27.63 -8 20 0 861.38 30.59 -8 20 2 353.62 19.96 -8 20 2 362.01 18.34 8 20 2 329.05 17.37 -8 20 2 331.87 19.32 -8 20 4 1701.44 39.26 8 20 4 1641.7 37.91 -8 20 4 1589.38 42.55 8 20 4 1656.32 38.62 8 20 6 313.1 16.87 -8 20 6 320.04 19.49 8 20 8 812.72 26.32 8 20 8 768.36 24.97 -8 20 8 724.49 27.92 8 20 10 142.74 10.08 8 20 10 136.74 9.57 -8 20 10 145.51 11.52 -8 22 -6 579.43 18.76 8 22 -6 557.84 18.29 -8 22 -6 518.4 19.89 -8 22 -6 564.5 19.59 -8 22 -4 188.42 11.51 8 22 -4 191.12 12.3 -8 22 -4 186.98 13.96 -8 22 -4 186.26 12.7 -8 22 -2 500.49 20.13 8 22 -2 472.41 20.14 -8 22 -2 469.99 23.01 -8 22 -2 443.28 20.86 -8 22 0 568.46 22.29 -8 22 0 499.4 22.93 -8 22 0 479.92 23.59 8 22 0 521.11 21.47 8 22 2 581.46 22.73 -8 22 2 658.68 24.64 -8 22 2 566.05 25.57 8 22 2 610.17 23.38 -8 22 2 566.62 24.81 8 22 4 145.31 11.8 -8 22 4 125.89 12.49 8 22 4 153.64 11.94 8 22 6 506.95 19.88 -8 22 6 479.2 22.38 8 22 8 576.03 19.4 -8 22 8 543.24 22.14 8 22 10 273.26 10.87 -8 22 10 270.41 12.89 8 24 -6 583.36 16.18 -8 24 -6 549.49 17.47 -8 24 -4 194.54 12.48 8 24 -4 196.72 11.11 -8 24 -2 859.68 25.17 8 24 -2 870.59 24.78 -8 24 -2 870.41 28.05 -8 24 0 91.23 9.06 8 24 0 91.29 9.62 -8 24 0 87.8 11.29 8 24 0 104.88 8.73 -8 24 2 784.24 26.69 8 24 2 831.73 25.58 8 24 2 761.33 24.38 -8 24 2 736.27 27.55 8 24 4 202.4 12.9 8 24 4 182.97 12.2 -8 24 4 167.44 13.92 -8 24 6 590.57 22.84 8 24 6 615.39 19.82 -8 24 8 88.37 8.4 8 24 8 79.88 6.58 8 24 8 86.78 7.28 8 26 -4 591.48 15.29 -8 26 -4 563.84 16.82 -8 26 -2 75.61 7.9 8 26 -2 77.92 6.83 8 26 0 1201.14 26.17 -8 26 0 1117.03 29.01 -8 26 2 77.26 9.33 8 26 2 80.11 7.88 8 26 4 621.87 17.98 -8 26 4 620.14 21.32 8 26 4 615.65 18.46 8 26 6 30.12 4.24 -8 26 6 31.47 5.59 8 26 6 31.12 4.18 8 28 0 22.74 3.14 -9 -1 -11 2126.23 79.15 9 -1 -11 1956.75 71.95 9 1 -11 2059.85 69.32 -9 1 -11 2209.8 83.12 -9 1 -9 1946.94 70.32 9 1 -9 2028.88 66.7 9 -1 -9 2014.83 69.68 -9 -1 -7 1611.1 54.92 9 -1 -7 1730.6 60.35 9 1 -7 1757.62 57.81 -9 -1 -5 2310.74 55.38 -9 -1 -5 2333.84 41.81 -9 -1 -3 3418.34 57.11 -9 1 -3 3257.01 58.83 -9 -1 -1 4746.51 41.45 -9 1 -1 4469.26 60.15 9 1 1 4542.56 47.29 9 -1 1 4457.62 41.89 -9 1 3 3585.77 57.58 9 -1 3 3632.92 44.79 9 1 3 3713.86 47.42 -9 -1 5 2277.86 46.91 -9 1 5 2234.45 45.42 9 1 5 2198.42 42.69 9 -1 5 2203.32 42.23 9 -1 7 1510.29 42.32 9 1 7 1515.01 42.64 9 1 9 1872.33 57.83 9 -1 9 1933.33 58.98 9 -1 9 1869.99 36.03 -9 -1 9 1777.36 34.96 9 1 11 1807.58 67.51 9 -1 11 1890.68 70.55 -9 -1 11 1913.28 39.34 9 -1 11 1885.38 42.23 -9 -1 13 1068.64 29.47 9 -1 13 1020.52 32.7 9 -1 15 632.41 22.15 -9 3 -17 325.57 10.28 9 -3 -11 957.04 52.34 -9 3 -11 1088.93 58.81 9 3 -9 1058.87 45.18 -9 -3 -9 1054.97 50.3 -9 3 -9 1071.77 54.54 9 -3 -9 1014.72 52.13 -9 -3 -7 1168.11 45.36 9 -3 -7 1284.22 55.08 9 3 -7 1175.26 44.39 -9 3 -7 1153.19 50.49 -9 3 -5 2664.99 44.92 9 3 -5 2570.44 60.6 -9 3 -5 2569.99 65.26 -9 3 -3 2319.4 43.01 -9 -3 -3 2399.54 46.13 9 -3 -1 2487.08 27.54 -9 -3 -1 2509.16 34.7 -9 3 -1 2425.92 44.84 -9 -3 1 2412.59 40.31 9 3 1 2445.72 37.76 9 -3 1 2415.73 27.61 9 -3 3 2596.46 37.28 9 3 3 2639.06 41.96 -9 3 3 2554.21 49.37 9 -3 5 2715.73 46.7 9 3 5 2786.77 50.02 -9 3 5 2847.51 52.4 9 -3 7 1384.36 41.61 9 3 7 1278.01 39.72 9 -3 9 1055.16 44.6 -9 3 9 1022.01 27.28 -9 -3 9 1025.35 26.12 9 3 9 1003.04 42.68 9 -3 9 975.33 26.09 9 3 9 1050.68 27.62 9 3 11 841.78 45.75 9 -3 11 934.93 50.01 9 3 11 853.77 29.02 9 -3 11 859.64 28.35 -9 3 11 865.82 27.34 -9 -3 11 884.02 26.3 9 -3 13 756.16 27.85 9 3 13 791.25 29.38 -9 3 13 830.53 26.11 -9 -3 13 780.92 24.69 9 -3 15 660.42 21.8 9 3 15 648.83 22.55 9 -5 -11 643.75 44.59 -9 -5 -11 650.91 44.7 -9 5 -11 728.14 47.47 -9 -5 -9 966.48 48.34 9 -5 -9 917.65 51.83 -9 5 -9 886.37 50.92 -9 -5 -7 2092.12 60.29 9 5 -7 2251.03 55.44 -9 5 -7 2148.87 71.06 -9 5 -5 976.18 27.51 9 5 -5 1009.59 33.19 -9 -5 -5 969.19 34.51 -9 5 -5 980.39 41.28 -9 5 -3 903 28.31 -9 -5 -3 851.76 26.98 9 5 -1 2805.3 46.95 9 -5 -1 2761.4 18.95 -9 -5 -1 2958.93 43.28 -9 5 -1 2893.25 51.73 -9 -5 1 3057.19 47.53 9 5 1 3197.7 47.3 -9 5 3 916.96 31.05 9 5 3 878.67 26.61 9 -5 3 863.52 20.61 -9 5 5 954.08 30.58 9 5 5 884.21 29.85 9 -5 5 900.27 27.13 9 -5 7 1967.26 51.09 -9 5 9 930.73 26.35 -9 -5 9 889.41 23.76 9 5 9 888.21 26.33 9 -5 9 905.34 25.12 9 -5 11 642.04 42.31 -9 5 11 682.42 24.21 -9 -5 11 638.81 21.69 9 5 11 625.34 25.29 9 -5 11 643.01 24.24 -9 5 13 398.08 17.97 -9 -5 13 378.74 16.62 9 -5 13 366.8 18.96 9 5 13 362.86 20.01 9 -5 15 622.98 19.81 9 5 15 644.52 21.32 -9 7 -13 162.28 8.86 9 -7 -11 281.72 30.29 -9 -7 -11 305.49 30.68 -9 7 -9 799.32 46.45 -9 -7 -9 838.37 45.16 -9 7 -7 543.98 35.13 -9 -7 -7 576.37 31.6 9 -7 -7 643.43 42.35 -9 7 -5 374.49 18.28 -9 -7 -5 391.28 22.06 9 7 -3 141.02 8.89 -9 7 -3 167.42 12.78 -9 -7 -1 1456.68 34.17 -9 -7 -1 1502.97 28.45 -9 -7 1 1242.2 32.82 9 -7 3 173.25 8.91 -9 7 3 213.96 15.53 -9 -7 3 208.05 15.9 9 -7 5 270.83 15.42 9 7 5 281.71 17.47 -9 7 5 302.45 18.52 9 -7 7 502.09 27.43 9 7 7 448.01 25.24 -9 7 9 764.82 24.67 -9 -7 9 740.82 21.3 9 7 9 735.22 38.03 9 7 9 796.83 26.07 9 -7 9 747.1 23.15 9 7 9 777.07 21.55 9 -7 11 259.44 15.53 9 7 11 269.48 17.28 9 7 11 272.71 13.99 -9 7 11 288.38 16 -9 -7 11 264.97 13.5 9 -7 13 144.31 11.46 9 7 13 149.29 12.82 9 7 15 173.17 10.06 9 7 15 166.59 10.17 9 -7 15 168.73 9.43 -9 9 -15 117.3 8.38 -9 9 -13 230.75 10.38 -9 9 -11 410.34 15.92 -9 -9 -9 379.99 30.33 9 -9 -9 371.93 34.93 9 -9 -7 256.33 28.31 -9 -9 -7 282.91 22.23 -9 -9 -5 874.16 32.83 9 -9 -5 887.56 49.23 -9 9 -5 885.79 30.02 -9 -9 -3 859.75 30.12 -9 -9 -3 858.52 27.06 -9 9 -3 846.78 30.94 -9 -9 -1 14.19 4.2 9 9 -1 17.94 4.74 -9 9 -1 13.84 4.57 9 9 1 63.44 8.18 -9 -9 1 62.18 8.11 -9 9 3 859.73 33.3 9 9 3 850.14 30.79 -9 9 5 860.66 33.11 9 9 5 839.87 32.37 9 9 5 823.57 31.56 -9 9 7 287 13.67 9 9 7 309.42 21.96 9 9 7 332.82 13.18 9 9 7 319.74 14.86 -9 9 9 290.31 15.58 -9 -9 9 280.72 12.99 9 9 9 248.69 23.13 9 -9 9 295.24 14.81 9 9 9 282.81 16.76 9 9 9 284.5 13.84 9 9 11 402.67 21.74 9 -9 11 382.53 18.42 9 9 11 376.93 16.88 -9 9 11 411.62 19.2 9 9 13 259.19 14.64 -9 9 13 291.12 17.38 9 9 13 256.28 15.88 9 -9 13 269.88 14.24 9 9 15 94.18 7.07 -9 9 15 123.4 8.43 -9 11 -15 229.45 9.99 -9 11 -13 359.43 12.5 -9 11 -13 398.37 18.75 -9 11 -11 671.21 20.42 -9 -11 -9 280.99 25.78 9 -11 -9 244.59 28.93 -9 11 -9 290.65 13.79 -9 -11 -7 600.41 32.13 9 -11 -7 599.89 44.21 -9 11 -7 591.52 20.6 -9 11 -5 1027.95 35.42 9 -11 -5 1021.46 55.81 -9 -11 -5 1051.35 36.05 9 11 -3 1201.27 40.6 -9 11 -3 1196.52 38.92 -9 -11 -3 1199.46 39.51 -9 11 -1 243.05 18.05 -9 -11 -1 226.54 16.48 9 11 -1 229.15 16.62 9 11 1 202.91 15.54 -9 11 3 1071.15 39.85 9 11 3 1053.81 36.44 -9 11 5 1047.37 40.06 9 11 5 1049.75 38.72 9 11 5 1007.79 36.53 9 11 7 654.89 33.4 9 11 7 667.76 20.03 -9 11 7 632.72 23.84 9 11 9 210.43 21.98 9 11 9 232.78 13.15 -9 11 9 202.29 15.21 9 11 9 248.7 14.49 9 11 11 679.15 24.83 9 11 11 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10 14 -4 2104.59 37.32 -10 14 -4 1923.94 39.32 -10 14 -4 1838.03 55.33 10 -14 -4 1830.68 81.79 10 14 -2 28.69 7.35 -10 14 -2 29.52 4.46 -10 14 -2 70.48 6.5 -10 -14 -2 26.42 7.04 -10 14 -2 27.31 5.61 -10 14 -2 65.07 10.99 -10 14 0 3485.49 45.74 -10 14 0 3507.21 81.01 -10 -14 2 48.8 9.68 -10 14 2 49.52 5.85 -10 14 2 45.72 9.92 10 14 2 40.84 8.43 10 14 4 1903.32 54.44 10 14 4 1912.09 57.02 -10 14 4 2220.39 44.83 -10 14 4 2092.61 38.08 10 14 4 2253.57 38.23 -10 14 4 2077.82 41.58 -10 14 4 1919.38 62.79 -10 14 6 98.25 14.64 -10 14 6 96.32 8.07 10 14 6 100.27 8.64 10 14 6 111.9 9.44 -10 14 6 99.16 10.19 -10 14 6 116.98 11.2 10 14 6 83.84 12.85 -10 14 8 2372.7 52.4 10 14 8 2575.08 45.41 10 14 10 17.25 4.79 -10 14 10 6.47 4.54 10 14 10 16.4 4.43 -10 14 12 955.72 30.18 10 14 12 905.49 25.39 -10 16 -12 21.78 3.36 -10 16 -12 19.26 3.98 -10 16 -10 2534.31 49.17 -10 16 -10 2492.03 38.71 10 16 -8 86.15 7.92 -10 16 -8 81.58 8.43 -10 16 -8 91.67 8.33 -10 16 -8 77.8 10 -10 16 -6 2633.71 57.61 10 16 -6 2968.69 76.99 -10 -16 -6 2697.07 76.71 10 16 -6 2899.68 44.76 -10 16 -6 2733.05 48.15 -10 16 -6 2816.86 45.07 10 16 -4 24.93 7.48 -10 -16 -4 34.03 8.85 -10 16 -4 18.97 5.69 10 16 -4 35.67 5.92 -10 16 -4 38.15 7.13 -10 16 -4 45.66 5.72 -10 16 -4 29.66 5 -10 16 -4 37.1 9.16 -10 16 -2 2924.66 57.24 10 16 -2 3163.73 75.87 10 16 -2 2969.39 44.91 -10 16 -2 2911.07 50.69 -10 16 -2 2886.04 43.78 -10 16 -2 3138.73 46.87 -10 16 -2 2820.18 75.49 -10 16 0 214.58 21.42 -10 16 0 207.13 10.85 10 16 0 200.04 18.92 -10 16 0 232.06 13.06 -10 -16 0 202.58 19.62 10 16 0 219.84 12.24 -10 16 0 226.4 14.38 -10 16 0 233.94 15.59 -10 16 2 3036.42 54.82 10 16 2 2828.05 70.86 -10 16 2 3115.83 49.67 -10 -16 2 2729.21 73.27 10 16 2 2971.18 44.63 -10 16 2 2875.86 49.66 -10 16 2 2827.02 80.29 -10 16 4 28.75 5.29 -10 16 4 19.92 7.9 10 16 4 39.12 5.78 -10 16 4 28.59 6.02 10 16 4 20.17 7.12 -10 16 6 2865.72 45.72 10 16 6 2759.52 46.74 -10 16 6 2974.75 57.18 10 16 6 2982.03 49.2 -10 16 6 2639.07 53.48 10 16 8 84.61 8.74 10 16 8 103.81 9.7 -10 16 8 92.38 11.04 10 16 10 2445.81 44.06 10 16 10 2530.74 44.77 10 16 12 18.14 3.83 -10 16 12 17.88 4.71 -10 18 -12 1701.67 25.04 -10 18 -12 1620.27 22.63 -10 18 -10 30.02 5.14 -10 18 -10 25 4.21 -10 18 -8 1905.87 43.57 10 18 -8 1853.99 32.78 -10 18 -8 1853.62 36.61 -10 18 -6 57.76 6.82 -10 18 -6 67.38 6.28 -10 18 -6 60.08 8.78 10 18 -6 61.92 7.12 -10 18 -6 54.53 7.82 -10 18 -4 2957.74 46.72 10 18 -4 2955.6 46.68 -10 18 -4 2815.46 51.84 -10 18 -4 2841.54 44.14 -10 18 -2 193.94 12 10 18 -2 213.85 20.88 -10 -18 -2 187.54 20.4 10 18 -2 210.4 13.16 -10 18 -2 192.01 14.69 -10 18 -2 186.96 15.18 -10 18 -2 198.92 12.33 -10 18 0 3005.37 48.55 -10 18 0 2796.08 41.35 10 18 0 3061.16 77.65 -10 -18 0 2911.58 78.25 -10 18 0 2844.08 52.02 10 18 0 2961.34 46.45 -10 18 0 2943.3 85.45 -10 18 0 2974.23 58.12 10 18 2 176.74 19.05 10 18 2 205.93 12.69 -10 18 2 224.64 15.02 -10 -18 2 182.61 20.78 -10 18 2 192.81 14.88 -10 18 2 207.92 13.35 -10 18 4 3027.82 58.1 -10 18 4 3073.4 51.29 10 18 4 2988.09 49.05 10 18 6 70.13 8.06 -10 18 6 57.22 8.58 -10 18 6 71.15 7.73 10 18 6 66.55 7.94 10 18 8 1964.1 39.7 10 18 8 1901.51 40.23 -10 18 10 17.57 5.16 10 18 10 21.89 4.6 10 18 10 25.26 5.06 10 18 12 1314.83 22.61 -10 20 -10 1248.63 22.88 -10 20 -8 4.1 2.8 -10 20 -6 2266.36 39.2 -10 20 -6 2227.42 46.56 10 20 -6 2166.78 36.35 -10 20 -6 2153.82 40.94 10 20 -4 89.98 8.82 -10 20 -4 71.97 9.33 -10 20 -4 76.63 7.72 -10 20 -4 68.19 9.13 -10 20 -4 65.03 7.2 10 20 -2 2553.22 44.59 -10 20 -2 2367.35 49.24 -10 20 -2 2573.25 44.86 -10 20 -2 2491.94 42.46 -10 20 -2 2290.42 51.87 -10 20 0 4.18 3.81 -10 20 0 4.78 3.67 10 20 0 6.78 5.46 -10 20 0 7.13 7.07 -10 20 2 2473.46 53.65 -10 20 2 2635.26 48.33 10 20 2 2507.96 45.08 -10 20 2 2472.47 50.83 -10 20 4 83.09 9.05 10 20 4 85.74 8.75 -10 20 4 91.56 10.37 -10 20 4 78.27 10 10 20 4 85.19 9.12 10 20 6 2206.59 41.83 -10 20 6 2004.5 46.88 10 20 8 11.65 4.02 -10 20 8 9.85 4.73 10 20 8 3.5 3.1 10 20 10 1218.29 24.9 10 20 10 1293.76 28.5 -10 22 -6 7.63 3.06 -10 22 -6 8.49 3.31 10 22 -6 6.09 2.95 -10 22 -6 3.41 3.46 10 22 -4 1377.84 29.46 -10 22 -4 1269.67 32.22 -10 22 -4 1391.85 30.2 -10 22 -4 1316.75 34.67 -10 22 -4 1348.93 30.09 -10 22 -2 106.4 10.87 10 22 -2 110.83 9.76 -10 22 -2 106.71 11.23 -10 22 -2 112.09 9.69 -10 22 0 378.69 20.51 10 22 0 416.73 18.49 -10 22 0 408.54 21.11 -10 22 0 446.07 19.7 10 22 2 90.26 9.43 -10 22 2 86.12 11.23 -10 22 2 88.79 9.38 10 22 2 92.12 9.26 -10 22 2 81.25 9.91 -10 22 4 1330.38 37.39 10 22 4 1358.61 32.23 10 22 4 1444.02 35.42 -10 22 4 1374.06 39.03 10 22 6 10.51 4.57 -10 22 6 14.96 5.69 10 22 8 607.39 18.16 -10 22 8 600.45 21.76 10 22 8 651.58 21.22 10 24 -6 178.56 7.87 -10 24 -4 13.23 3.45 10 24 -4 17.08 3.81 -10 24 -4 17.99 4.66 -10 24 -2 184.63 12.08 10 24 -2 180.76 10.7 -10 24 -2 182.77 12.5 -10 24 0 140.9 11.34 10 24 0 128.55 10.04 -10 24 0 129.21 11.99 10 24 0 134.76 9.55 -10 24 2 150.51 12.11 10 24 2 148.73 10.55 10 24 2 143.94 10.47 -10 24 2 147.03 12.87 10 24 4 22.84 5.39 -10 24 4 19.8 6.95 10 24 4 18.82 4.55 10 24 6 199.11 11.68 10 24 6 176.72 9.73 10 26 -4 18.24 2.6 10 26 -2 58.89 5.08 10 26 0 78.63 6.33 10 26 2 45.63 5.03 10 26 2 49.64 5.3 10 26 4 17.9 3.46 10 26 4 19.07 3.64 -11 1 -11 2519.06 91.36 11 -1 -11 2232.78 76.53 -11 -1 -11 2449.86 88.18 11 1 -11 2181.87 71.1 11 1 -9 1406.92 56.63 11 -1 -9 1443.22 61.15 -11 1 -9 1361.39 62.03 -11 -1 -7 2376.91 68.47 11 1 -7 2606.22 73.28 11 -1 -7 2620.01 78.17 -11 -1 -5 2581.09 50.64 -11 1 -5 2534.82 49.47 -11 1 -5 2601.86 65.83 -11 -1 -5 2590.87 62.43 -11 1 -3 4686.77 69.15 -11 -1 -3 4755.16 45.29 -11 1 -3 4731.39 73.6 11 -1 -1 1715.97 30.45 11 1 -1 1720.37 33.58 -11 1 -1 1618.31 42.15 -11 -1 -1 1710.77 28.82 11 1 1 1721.12 32.73 11 -1 1 1658.83 29.29 -11 1 3 4641.86 75.24 11 -1 3 4504.72 54.85 11 1 3 4459.58 57.89 -11 -1 5 2555.84 56.96 -11 1 5 2566.16 56.42 11 1 5 2486.95 48.76 11 -1 5 2569.73 47.96 11 -1 7 1943.67 31.12 -11 -1 7 2034.21 34.17 11 1 7 2111.11 52.09 11 -1 7 2109.08 52.08 11 -1 9 1229.84 29.76 11 1 9 1259.35 48.15 11 -1 9 1241.14 48.07 -11 -1 9 1221.44 28.8 11 1 11 1962.08 70.19 11 -1 11 2061.76 72.96 -11 -1 11 2153.06 40.98 11 -1 11 2091.49 44.53 -11 -1 13 1053.22 28.63 11 -1 13 996.17 31.88 11 -1 15 539.63 20.25 -11 3 -11 1034.35 58.25 11 -3 -11 894.47 51.47 -11 -3 -11 1079.58 57.7 -11 3 -9 1284.79 62.49 -11 -3 -9 1316.1 56.65 11 3 -9 1314.14 51.39 11 -3 -9 1336.36 61.56 -11 3 -7 1972.48 69.3 -11 -3 -7 1891.46 58.66 11 -3 -7 2146.03 74.39 11 3 -7 2050.26 60.46 -11 3 -5 1170.84 34.02 -11 3 -5 1120.47 45.17 -11 -3 -5 1105.21 39.33 11 3 -5 1213.2 44.65 -11 3 -3 2211.26 47.48 -11 -3 -3 2191.32 36.76 11 -3 -1 4303.25 42.28 11 3 -1 4281.37 58.19 -11 3 -1 4207.18 67.1 -11 -3 1 4499.27 62.01 11 -3 1 4631.08 43.83 -11 3 3 2473.23 55.03 11 3 3 2512.91 45.38 -11 3 5 1295.8 40.18 11 -3 5 1183.76 32.37 11 3 5 1209.45 35.29 -11 3 7 1984.22 34.53 -11 -3 7 2098.58 34.3 11 3 7 2034.19 52.17 11 -3 7 2171.28 53.48 11 -3 7 1978.86 31.38 11 3 7 1906.28 31.7 11 -3 9 1448.65 52.94 -11 3 9 1371.81 31.62 -11 -3 9 1368.34 30.18 11 3 9 1278.37 48.89 11 3 9 1296.27 31.43 11 -3 9 1336.99 30.92 11 -3 11 1097.17 54.67 11 3 11 979.3 31.32 11 -3 11 995.52 30.7 -11 3 11 1010.29 29.04 -11 -3 11 1045.81 28.35 11 3 13 747.29 28.23 11 -3 13 766.55 27.53 11 3 15 885.39 25.79 11 -3 15 846.83 24.16 -11 5 -11 843.84 50.88 -11 5 -9 726.98 47.38 -11 -5 -9 756.84 42.68 11 -5 -9 808.06 49.69 -11 5 -7 587.94 38.8 -11 -5 -7 591.21 32.6 11 5 -7 611.63 29.74 11 -5 -7 617.56 41.49 -11 5 -5 1929.36 43.86 -11 -5 -5 1878.35 50.22 -11 -5 -3 1084.68 29.53 -11 5 -3 1095.49 34.99 -11 -5 -3 1168.23 35.57 11 5 -1 355 17.87 -11 -5 -1 347.29 16.11 -11 5 -1 375.13 20.96 -11 -5 1 299.3 16.07 11 5 1 318.04 16.55 11 -5 3 1193.85 26.99 11 5 3 1216.57 34.05 -11 5 3 1254.66 40.25 11 5 5 1914.55 46.65 11 5 5 1871.58 45.97 11 -5 5 1905.05 41.34 -11 5 5 1913.33 48.82 11 -5 7 586.14 28.89 11 5 7 527.37 27.66 -11 5 7 497.69 17.83 -11 -5 7 547.31 17.67 11 5 7 516.97 17.06 11 -5 7 524.83 16.29 11 5 9 724.83 37.63 11 -5 9 778.34 40.58 -11 5 9 750.9 24.06 -11 -5 9 723.62 21.97 11 5 9 737.19 24.28 11 -5 9 747.58 23.11 -11 5 11 663.86 23.9 -11 -5 11 622.94 21.4 11 5 11 617.89 25.38 11 -5 11 621.24 23.82 11 -5 13 579.61 23.38 11 5 13 540.55 23.94 11 -5 15 254.03 12.45 11 5 15 262.21 13.39 -11 7 -15 156.88 10.07 -11 7 -13 111.84 7.5 -11 -7 -9 364.33 29.62 -11 -7 -7 268.26 21.87 11 -7 -7 316.89 31 -11 7 -5 124.14 11.6 -11 -7 -5 83.66 10.7 -11 -7 -3 529.29 22.85 -11 7 -3 538.95 25.13 -11 -7 -3 546.86 24.31 11 7 -1 1003.28 32.09 -11 7 -1 1012.22 35.02 -11 -7 -1 1054.13 31.22 11 7 1 980.98 31.53 -11 -7 1 895.87 29.51 11 7 3 489.82 23.15 -11 7 3 553.28 27.24 -11 7 5 163.1 14.83 11 7 5 142.21 13.6 11 7 5 151.33 13.95 11 7 7 268.89 20.65 11 7 7 247.24 10.86 11 7 7 249.83 12.48 11 -7 7 261.63 11.82 11 7 9 312.21 25.34 -11 7 9 328.11 16.41 -11 -7 9 328.32 14.58 11 7 9 316.47 16.67 11 -7 9 313.1 15.18 11 7 11 71.52 9.32 11 -7 11 75.67 8.62 11 -7 13 127.66 10.66 11 7 13 129.84 11.86 11 7 15 129.04 8.6 11 -7 15 127.58 7.93 -11 9 -15 28.89 4.38 -11 9 -13 76.14 6.15 -11 -9 -9 84.62 14.45 11 -9 -9 64.97 15.53 -11 -9 -7 100.25 13.41 11 -9 -7 90.03 18.02 -11 -9 -5 389.38 22.62 -11 9 -5 411.98 22.27 -11 -9 -3 403.36 20.41 -11 9 -3 372.64 21.83 -11 -9 -3 402.82 22.12 -11 9 -1 457.98 24.56 -11 -9 -1 528.54 24.26 -11 -9 1 427.08 22.15 -11 9 3 435.48 25.56 -11 -9 3 399.32 24.2 -11 9 5 427.68 25.5 11 9 5 468.92 25.42 11 9 7 117.25 14.36 11 9 7 136.14 8.72 11 9 7 124.63 9.52 11 9 9 52.05 11.18 11 9 9 58.89 6.74 11 9 9 63.78 6.76 11 9 9 53.64 7.69 11 -9 9 56.52 6.78 11 9 11 209.7 13.07 -11 9 11 189.88 14.66 11 9 11 194.26 12.02 11 9 11 207.61 15.67 11 -9 11 189.04 13.09 11 9 13 78.05 7.64 -11 9 13 88.07 9.04 11 -9 13 82.08 8.01 11 9 13 76.97 8.81 -11 11 -15 330.43 11.5 -11 11 -13 86.15 6.28 -11 11 -13 96.07 9.45 -11 11 -11 78.46 7.37 -11 11 -11 88.41 10.62 -11 11 -9 415.72 23.35 -11 -11 -9 416.84 30.35 11 -11 -9 407.91 38.1 -11 11 -7 844.98 24.17 -11 -11 -7 846.23 38.15 11 -11 -7 834.62 54.5 11 -11 -5 157.85 23.62 -11 -11 -5 155.05 15.72 -11 11 -5 147.43 8.21 -11 11 -5 153.23 14.62 -11 -11 -3 155.77 15.05 11 11 -3 186 16.66 -11 11 -3 162.95 15.47 -11 11 -3 165.12 9.03 -11 11 -1 744.6 33.62 11 11 -1 739.57 31.98 -11 -11 -1 762.79 32.15 11 11 1 721.47 31.42 -11 -11 1 716.96 30.84 -11 11 3 182.88 17.68 -11 11 3 181.91 10.25 -11 -11 3 192.91 17.93 11 11 3 212.58 17.5 -11 11 5 150.39 16.31 -11 11 5 151.56 9.4 -11 11 5 184.84 12.1 11 11 5 162.61 16.28 11 11 5 149.4 15.35 -11 11 7 823.1 27.52 11 11 7 843.38 23.16 11 11 9 340.36 19.1 11 11 9 333.47 15.79 11 11 9 364.66 17.1 -11 11 9 325.48 19.08 11 11 11 98.11 10.84 11 11 11 100.8 8.93 11 11 11 114.43 9.83 -11 11 11 108.25 11.4 11 11 13 121.62 9 -11 11 13 123.88 10.24 -11 13 -15 233.97 7.53 -11 13 -13 412.43 16.97 -11 13 -13 361.76 11.85 -11 13 -11 583.97 25.27 -11 13 -11 598.04 19.14 -11 13 -9 674.77 29.47 -11 13 -9 712.35 22.5 -11 13 -7 1190.15 39.71 -11 13 -7 1345.04 31.87 11 -13 -7 1251.33 68.44 -11 -13 -7 1304.96 50.42 -11 13 -5 683.42 18.87 -11 13 -5 658.06 20.8 11 13 -5 752.23 37.9 -11 -13 -5 667.17 34.89 -11 13 -5 645.3 22.03 -11 13 -5 596.31 26.99 -11 13 -5 650.37 31.88 11 -13 -5 645.12 49.46 -11 -13 -3 1209.26 44.9 -11 13 -3 1176.97 25.39 -11 13 -3 1099.14 25.94 -11 13 -3 1159.66 44.61 11 13 -3 1261.29 46.13 -11 -13 -1 1754.99 52.92 -11 13 -1 1620.44 30.59 -11 13 -1 1645 53.28 11 13 -1 1716.93 51.79 -11 -13 1 1751.8 52.62 -11 13 1 1723.38 32.32 -11 13 3 1167.09 27.38 -11 13 3 1162.73 48.14 11 13 3 1185.93 43.74 11 13 5 712.18 36 11 13 5 605.26 31.98 -11 13 5 810.43 27.18 -11 13 5 695.94 21.45 -11 13 5 766.91 25.38 -11 13 5 696.75 36.87 -11 13 7 1378.79 37.58 11 13 7 1301.81 51.07 11 13 7 1419.25 31.93 11 13 9 560.43 21.38 11 13 9 614.21 22.63 -11 13 9 558.45 25.53 11 13 11 522.82 19.96 11 13 11 575.94 21.29 -11 13 11 538.73 24.24 11 13 13 385.08 14.43 -11 15 -13 614.8 17.54 -11 15 -13 587.91 13.61 -11 15 -11 1027.4 30.43 -11 15 -11 973.18 23.14 -11 15 -9 1187.49 37.54 -11 15 -9 1178.77 28.28 -11 15 -7 1054.17 28.94 -11 15 -7 1017.7 36.56 -11 15 -5 668.22 19.78 -11 15 -5 643.42 21.35 -11 15 -5 563.98 27.18 11 15 -5 669.18 36.32 -11 -15 -5 623.02 35.76 -11 15 -5 605.19 22.65 11 15 -5 671.93 21.46 -11 15 -5 594.73 32.64 11 -15 -5 494.3 44.42 -11 15 -3 1882.39 34.53 -11 15 -3 1827.29 34.99 -11 15 -3 1671.66 33.21 -11 15 -3 1777.54 45.64 11 15 -3 2038.79 61.62 -11 -15 -3 1866.78 59.49 -11 15 -3 1686.66 37.93 -11 15 -3 1775.92 57.9 11 -15 -3 1510.68 77.89 -11 15 -1 1829.97 43.5 -11 -15 -1 1805.9 57.15 -11 15 -1 1763.21 37.34 -11 15 -1 1749.39 59.24 -11 15 -1 1845.35 34.66 -11 15 -1 1721.79 32 11 15 1 1958.84 58.79 -11 15 1 1866.04 38.04 -11 15 3 1850.21 42.11 11 15 3 1544.65 50.3 11 15 3 1677.47 56.04 -11 15 3 1755.08 36.07 -11 -15 3 1499.14 56.22 -11 15 3 1746.2 37.99 -11 15 3 1652.82 60.82 11 15 5 709.28 35.94 -11 15 5 873.53 29.75 -11 15 5 805.76 27.71 -11 15 5 755.77 41.77 -11 15 5 820.02 24.77 -11 15 7 1094.98 34.45 11 15 7 1099.04 29.61 -11 15 9 1154.08 36.44 11 15 9 1199.12 31.63 11 15 11 929.25 25.33 -11 15 11 960.7 30.58 11 15 11 875.87 25.22 -11 17 -13 828.69 15.66 -11 17 -11 717.48 18.34 -11 17 -11 765.19 22.77 -11 17 -9 1607.59 31.83 -11 17 -9 1594.78 39.84 11 17 -7 1614.5 31.86 -11 17 -7 1574.73 34.94 -11 17 -7 1584.32 33.55 -11 17 -7 1563.04 43.75 -11 17 -5 356.81 17.9 11 17 -5 386.59 16.46 -11 17 -5 390.14 22.46 -11 17 -5 364.66 16.49 -11 17 -5 369.44 15.24 -11 17 -3 1355.38 30.7 -11 17 -3 1372.54 31.69 11 17 -3 1363.27 52.26 -11 -17 -3 1276.46 52.42 11 17 -3 1371.63 31.15 -11 17 -3 1279.81 34.59 -11 17 -3 1299.47 52.92 -11 17 -3 1227.86 39.11 -11 17 -1 1808.36 37.13 -11 17 -1 1521.06 31.62 11 17 -1 1765.98 58.98 11 17 -1 1627.9 33.68 -11 17 -1 1553.24 37.75 -11 17 -1 1618.16 60.37 -11 17 -1 1638.26 43.59 -11 17 1 1797.8 40.51 -11 17 1 1936.16 45.77 11 17 1 1952.54 62.21 -11 17 3 1351.64 58.68 -11 17 3 1387.17 33.83 11 17 3 1403.69 31.85 -11 17 3 1297.17 35.01 11 17 3 1268.71 50.46 11 17 5 470.8 19.76 -11 17 5 496.97 20.15 11 17 5 486.07 19.51 -11 17 5 450.6 21.71 11 17 7 1492.02 34.25 11 17 7 1435.3 34.95 11 17 9 1496.53 33.32 11 17 9 1463.54 34.77 11 17 11 717.42 19.72 11 17 11 749.74 22.15 -11 19 -11 857.32 17.6 -11 19 -9 651.55 18.9 -11 19 -9 659.54 22.31 -11 19 -9 629.64 19.8 -11 19 -7 965.86 25.25 -11 19 -7 960.12 31.15 11 19 -7 951.35 22.94 -11 19 -7 905.87 25.12 11 19 -5 1543.87 31.68 -11 19 -5 1458.17 35 -11 19 -5 1555.5 33.53 -11 19 -5 1469.94 41.62 -11 19 -5 1466.05 30.75 11 19 -3 1802.16 35.95 -11 19 -3 1667.01 39.8 -11 19 -3 1756.83 36.35 -11 19 -3 1748.18 36.01 11 19 -1 922.38 26.53 -11 19 -1 874.48 29.72 -11 19 -1 860.4 24.08 -11 19 -1 903.23 27 -11 19 -1 891.77 33.21 -11 19 1 910.74 32.84 -11 19 1 903.04 30.07 11 19 1 983.43 27.42 -11 19 3 1829.27 46.21 -11 19 3 1953.17 41.53 11 19 3 1855.48 37.98 11 19 5 1581.05 37.04 -11 19 5 1574.66 36.47 11 19 5 1559.48 34.85 11 19 7 846.04 25.38 -11 19 7 772.53 28.89 11 19 7 825.25 26.84 11 19 9 579.24 19.23 -11 19 9 540.61 22.4 11 19 9 589.71 21.15 -11 21 -9 440.67 14.56 -11 21 -7 696.86 19.82 -11 21 -7 693.12 22.95 -11 21 -7 627.05 18.81 11 21 -5 899.55 22.7 -11 21 -5 905.98 24.55 -11 21 -5 888.68 29.43 -11 21 -5 838.17 22.58 11 21 -3 994.83 25.96 -11 21 -3 957.03 29.36 -11 21 -3 1020.21 26.7 -11 21 -3 998.66 27.27 -11 21 -3 957.88 32.77 -11 21 -1 456.63 23.22 11 21 -1 502.19 19.82 -11 21 -1 463.65 22.06 -11 21 1 558.43 25.84 11 21 1 593.74 21.56 -11 21 1 552.53 24.19 -11 21 3 1131.77 31.94 11 21 3 1150.11 31.82 -11 21 3 1050.84 34.89 11 21 3 1080.91 28.87 11 21 5 753.89 23.68 -11 21 5 733.25 27.56 11 21 7 587.97 21.67 11 21 7 559.92 18.88 -11 21 7 537.01 22.44 11 21 9 450.84 16.87 11 23 -5 89.93 6.57 -11 23 -5 84.45 7.36 -11 23 -5 103.69 8.6 -11 23 -3 194.67 11.76 -11 23 -3 161.97 11.53 11 23 -3 180.43 10.31 -11 23 -3 175.58 12.46 -11 23 -1 304.52 15.45 -11 23 -1 289 17.03 11 23 -1 298.77 14.16 -11 23 -1 297.47 16.67 -11 23 1 337.5 18.93 11 23 1 350.56 15.95 -11 23 1 334.6 18.64 11 23 1 396.16 17.46 11 23 3 221.66 12.63 -11 23 3 217.95 15.42 -11 23 3 250.28 14.69 -11 23 3 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1035.2 31.59 -22 12 -2 1039.39 32.73 -22 12 -2 984.32 29 -22 12 0 228.59 14.93 -22 12 0 221.56 13.96 -22 12 0 203.2 13.14 -22 12 0 203.3 14.43 -22 12 2 1012.57 31.57 -22 12 2 948.16 27.28 -22 12 2 954.7 30.44 -22 12 4 463.96 20.87 -22 12 4 494.85 21.39 -22 12 4 448.1 18.03 -22 12 6 630.92 20.82 -22 14 -10 191.1 8.3 -22 14 -10 190.34 10.3 -22 14 -8 1466.5 31.7 -22 14 -8 1426.8 35.61 -22 14 -6 144.8 10.16 -22 14 -6 117.08 9.96 -22 14 -6 113.02 10.18 -22 14 -6 124.28 11.79 -22 14 -4 905.89 24.96 -22 14 -4 906.79 25.22 -22 14 -4 899.28 30.02 -22 14 -4 882.13 27.71 -22 14 -4 941.15 32.05 -22 14 -2 182.71 12.41 -22 14 -2 180.55 13.77 -22 14 -2 177.06 12.42 -22 14 -2 166.14 13.21 -22 14 0 2201.88 44.56 -22 14 0 2182.19 44.59 -22 14 0 2147.97 41.97 -22 14 0 2111.06 46.09 -22 14 2 161.99 11.74 -22 14 2 143.85 11.9 -22 14 2 153.37 12.27 -22 14 4 821.81 24.71 -22 14 4 905.23 27.94 22 14 6 82.82 7.08 -22 14 6 82.94 7.51 -22 16 -10 1398.82 22.46 -22 16 -8 110.08 6.96 -22 16 -8 120.44 8.32 -22 16 -8 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-8 879.75 21.69 -26 -4 -8 867.59 20.75 -26 4 -6 15.7 3.45 -26 -4 -6 10.53 3.11 -26 4 -6 9.59 3.28 -26 -4 -6 9.84 3.17 -26 4 -4 972.19 28.84 -26 4 -4 984.61 27.05 -26 -4 -4 1026.59 25.79 -26 4 -4 951.22 29.13 -26 4 -2 2.91 3.32 -26 4 -2 5.45 2.92 -26 -4 -2 11.14 3.34 -26 4 -2 7.05 3.84 -26 -4 0 1928.1 35.92 -26 4 0 1887.17 40.88 -26 4 0 1906.12 40.14 -26 -4 2 12.07 3.44 -26 4 2 6.36 3.7 -26 4 2 7.76 4.62 -26 4 4 1039.85 29.47 -26 4 4 1161.19 33.85 -26 4 6 9.32 3.16 26 4 6 11.39 4.02 26 -4 6 9.56 3.64 -26 -4 6 13.73 3.64 26 4 8 858.05 25.6 26 -4 8 912.27 26.88 26 4 10 6.17 2.95 26 -4 10 7 3.21 -26 6 -10 1897.59 26.7 -26 6 -8 47.78 5.37 -26 6 -6 1558.29 32.41 -26 6 -4 97.12 9.12 -26 6 -4 96.74 8.87 -26 6 -4 106.04 10.11 -26 6 -2 2352.57 48.67 -26 6 -2 2229.11 43.11 -26 6 -2 2278.03 45.73 -26 6 0 48.59 8.13 -26 6 0 32.03 5.9 -26 6 0 37.61 6.07 -26 6 2 2258.26 50.55 -26 6 2 2090.39 42.98 -26 6 4 110.17 9.9 26 6 4 106.05 9.45 26 -6 4 115.96 10.28 -26 6 4 96.26 9.82 26 6 6 1530.41 34 26 -6 6 1582.54 35.67 -26 6 6 1615.9 31.58 -26 -6 6 1517.15 30.36 26 6 8 45.65 6.07 26 -6 8 51.24 6.62 26 6 10 1577.62 29.3 26 -6 10 1704.4 31.8 -26 8 -10 19.84 2.98 -26 8 -10 17.89 3.23 -26 8 -10 18.44 2.94 -26 8 -8 1958.19 37.06 -26 8 -8 1975.76 32.84 -26 8 -6 82.04 8.67 -26 8 -6 82.36 7.66 -26 8 -4 2195.31 40.55 -26 8 -4 2204.96 41.2 -26 8 -4 2130.26 44.29 -26 8 -2 17.9 4.63 -26 8 -2 5.36 3.55 -26 8 0 3293.94 59.26 -26 8 0 3010.32 53.06 -26 8 2 5.76 4.25 26 8 4 2358.5 41.19 26 -8 4 2314.88 42.32 26 8 6 93.08 8.26 26 -8 6 88.21 8.31 26 8 8 1903.95 33.99 26 -8 8 2094.21 36.96 -26 10 -10 1134.92 18.92 -26 10 -10 1117.04 19.49 -26 10 -8 5.08 2.29 -26 10 -8 6.3 2.57 -26 10 -8 3.86 2.09 -26 10 -6 1922.15 39.81 -26 10 -6 1919.75 35.57 -26 10 -6 1822.68 33.08 -26 10 -4 1.47 3.13 -26 10 -4 5.16 2.43 -26 10 -4 3.84 2.88 -26 10 -2 2240.78 44.08 -26 10 -2 2189.22 45.47 -26 10 0 83.28 9.45 -26 10 0 77.95 8.89 26 10 2 2347.77 38.59 -26 10 2 2335.26 47.97 -26 10 2 2223.78 44.37 -26 10 4 17.31 4.68 26 10 4 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