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Information card for entry 7712213
Preview
| Coordinates | 7712213.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C46 H45 F6 N O6 P4 Pb S2 |
|---|---|
| Calculated formula | C46 H45 F6 N O6 P4 Pb S2 |
| SMILES | [Pb]12([P](c3ccccc3)(c3ccccc3)CC[P]1(CC[P]2(c1ccccc1)c1ccccc1)CC[P](c1ccccc1)c1ccccc1)(OS(=O)(=O)C(F)(F)F)OS(=O)(=O)C(F)(F)F.N#CC |
| Title of publication | Synthesis, spectroscopic and structural properties of Sn(II) and Pb(II) triflate complexes with soft phosphine and arsine coordination. |
| Authors of publication | Cairns, Kelsey R.; King, Rhys P.; Bannister, Robert D.; Levason, William; Reid, Gillian |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2023 |
| Journal volume | 52 |
| Journal issue | 8 |
| Pages of publication | 2293 - 2308 |
| a | 16.3354 ± 0.0005 Å |
| b | 14.2959 ± 0.0003 Å |
| c | 21.6774 ± 0.0005 Å |
| α | 90° |
| β | 102.94 ± 0.002° |
| γ | 90° |
| Cell volume | 4933.8 ± 0.2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.047 |
| Residual factor for significantly intense reflections | 0.0314 |
| Weighted residual factors for significantly intense reflections | 0.0515 |
| Weighted residual factors for all reflections included in the refinement | 0.0546 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Diffraction radiation X-ray symbol | K-L~3~ |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 283245 (current) | 2023-05-05 | cif/ Updating files of 7712208, 7712209, 7712210, 7712211, 7712212, 7712213, 7712214, 7712215, 7712216, 7712217, 7712218, 7712219 Original log message: Adding full bibliography for 7712208--7712219.cif. |
7712213.cif |
| 280681 | 2023-01-31 | cif/ Adding structures of 7712208, 7712209, 7712210, 7712211, 7712212, 7712213, 7712214, 7712215, 7712216, 7712217, 7712218, 7712219 via cif-deposit CGI script. |
7712213.cif |
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Users of the data should acknowledge the original authors of the
structural data.