Crystallography Open Database

Information card for entry 7712252

Preview

Coordinates	7712252.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H60 Ge3 N3 O3 P7
Calculated formula	C39 H60 Ge3 N3 O3 P7
Title of publication	Reactivity of tetrel functionalized heptapnictogen clusters towards heteroallenes.
Authors of publication	Jobbins, William D.; van IJzendoorn, Bono; Vitorica-Yrezabal, Inigo J; Whitehead, George F. S.; Mehta, Meera
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	52
Journal issue	8
Pages of publication	2384 - 2391
a	14.6729 ± 0.0002 Å
b	20.5725 ± 0.0003 Å
c	15.8849 ± 0.0002 Å
α	90°
β	94.247 ± 0.001°
γ	90°
Cell volume	4781.82 ± 0.11 Å³
Cell temperature	100 ± 0.3 K
Ambient diffraction temperature	100 ± 0.3 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0489
Residual factor for significantly intense reflections	0.0475
Weighted residual factors for significantly intense reflections	0.1086
Weighted residual factors for all reflections included in the refinement	0.1094
Goodness-of-fit parameter for all reflections included in the refinement	1.181
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283235 (current)	2023-05-05	cif/ Updating files of 7712250, 7712251, 7712252, 7712253, 7712254 Original log message: Adding full bibliography for 7712250--7712254.cif.	7712252.cif
280717	2023-02-01	cif/ Adding structures of 7712250, 7712251, 7712252, 7712253, 7712254 via cif-deposit CGI script.	7712252.cif