Crystallography Open Database

Information card for entry 7714158

Preview

Coordinates	7714158.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H30.7 Cl Fe N2 O0.35 P Pd
Calculated formula	C23 H30.707 Cl Fe N2 O0.3535 P Pd
Title of publication	Synthesis and reactivity of Pd(II) imidoyl complexes obtained by insertion of isocyanoferrocene into the Pd-C bonds of orthopalladated precursors
Authors of publication	Franc, Michal; Vosahlo, Petr; Schulz, Jiří; Cisarova, Ivana; Štěpnička, Petr
Journal of publication	Dalton Transactions
Year of publication	2023
a	10.3488 ± 0.0005 Å
b	13.782 ± 0.0007 Å
c	17.1619 ± 0.0009 Å
α	101.004 ± 0.002°
β	95.44 ± 0.002°
γ	96.566 ± 0.002°
Cell volume	2369.9 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0225
Residual factor for significantly intense reflections	0.0208
Weighted residual factors for significantly intense reflections	0.05
Weighted residual factors for all reflections included in the refinement	0.051
Goodness-of-fit parameter for all reflections included in the refinement	1.078
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
286838 (current)	2023-10-07	cif/ Adding structures of 7714153, 7714154, 7714155, 7714156, 7714157, 7714158, 7714159, 7714160, 7714161, 7714162 via cif-deposit CGI script.	7714158.cif