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Information card for entry 7714195
Preview
| Coordinates | 7714195.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H50 B Br Cl2 N3 P |
|---|---|
| Calculated formula | C24 H50 B Br Cl2 N3 P |
| Title of publication | Phosphinoborenium cations stabilized by N-heterocyclic carbenes: synthesis, structure, and reactivity |
| Authors of publication | Kaniewska-Laskowska, Kinga; Ordyszewska, Anna; Wojnowski, Tomasz; Halenka, Hanna; Czapla, Marcin; Chojnacki, Jarosław; Grubba, Rafał |
| Journal of publication | Dalton Transactions |
| Year of publication | 2023 |
| a | 17.2597 ± 0.0004 Å |
| b | 10.7727 ± 0.0002 Å |
| c | 18.5283 ± 0.0005 Å |
| α | 90° |
| β | 113.564 ± 0.002° |
| γ | 90° |
| Cell volume | 3157.77 ± 0.14 Å3 |
| Cell temperature | 120 K |
| Ambient diffraction temperature | 120 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0686 |
| Residual factor for significantly intense reflections | 0.0563 |
| Weighted residual factors for significantly intense reflections | 0.1292 |
| Weighted residual factors for all reflections included in the refinement | 0.1387 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.121 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 286943 (current) | 2023-10-13 | cif/ Adding structures of 7714195, 7714196, 7714197, 7714198 via cif-deposit CGI script. |
7714195.cif |
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Users of the data should acknowledge the original authors of the
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