Crystallography Open Database

Information card for entry 7714502

Preview

Coordinates	7714502.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H54 F6 N6 Ni2 O6
Calculated formula	C66 H54 F6 N6 Ni2 O6
Title of publication	Bimetallic nickel complexes containing imidazole-based phenolate ligands as efficient catalysts for the copolymerization of carbon dioxide with epoxides.
Authors of publication	Hsu, Han-Fang; Liu, Guan-Lin; Su, Yu-Chia; Ko, Bao-Tsan
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	53
Journal issue	1
Pages of publication	299 - 314
a	12.6449 ± 0.0017 Å
b	13.4163 ± 0.0019 Å
c	22.2 ± 0.003 Å
α	87.747 ± 0.004°
β	74.48 ± 0.004°
γ	72.929 ± 0.004°
Cell volume	3465.8 ± 0.8 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150.15 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1437
Residual factor for significantly intense reflections	0.0951
Weighted residual factors for significantly intense reflections	0.2434
Weighted residual factors for all reflections included in the refinement	0.2708
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
289463 (current)	2024-02-04	cif/ Updating files of 7714500, 7714501, 7714502, 7714503, 7714504, 7714505, 7714506, 7714507, 7714508, 7714509 Original log message: Adding full bibliography for 7714500--7714509.cif.	7714502.cif
287688	2023-11-19	cif/ Adding structures of 7714500, 7714501, 7714502, 7714503, 7714504, 7714505, 7714506, 7714507, 7714508, 7714509 via cif-deposit CGI script.	7714502.cif