Crystallography Open Database

Information card for entry 7714591

Preview

Coordinates	7714591.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H30 B2 F20 N2 Si
Calculated formula	C39 H30 B2 F20 N2 Si
Title of publication	Coordination chemistry and FLP reactivity of 1,1- and 1,2-bis-boranes.
Authors of publication	Yeganeh-Salman, Amir; Yeung, Jason; Miao, Linkun; Stephan, Douglas W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	3
Pages of publication	1178 - 1189
a	11.6686 ± 0.0012 Å
b	18.4917 ± 0.0012 Å
c	19.1503 ± 0.0015 Å
α	90°
β	95.857 ± 0.008°
γ	90°
Cell volume	4110.5 ± 0.6 Å³
Cell temperature	149.99 K
Ambient diffraction temperature	149.99 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0766
Residual factor for significantly intense reflections	0.0522
Weighted residual factors for significantly intense reflections	0.12
Weighted residual factors for all reflections included in the refinement	0.1341
Goodness-of-fit parameter for all reflections included in the refinement	1.0232
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
289556 (current)	2024-02-04	cif/ Updating files of 7714584, 7714585, 7714586, 7714587, 7714588, 7714589, 7714590, 7714591, 7714592, 7714593 Original log message: Adding full bibliography for 7714584--7714593.cif.	7714591.cif
287912	2023-12-01	cif/ Adding structures of 7714584, 7714585, 7714586, 7714587, 7714588, 7714589, 7714590, 7714591, 7714592, 7714593 via cif-deposit CGI script.	7714591.cif