Crystallography Open Database

Information card for entry 7714600

Preview

Coordinates	7714600.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H6 Na6 O58 P4 W14
Calculated formula	Na6 O78.5 P4 W14
Title of publication	Heteroelements in polyoxometalates: a study on the influence of different group 15 elements on polyoxometalate formation.
Authors of publication	Raabe, Jan-Christian; Jameel, Froze; Stein, Matthias; Albert, Jakob; Poller, Maximilian J.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	2
Pages of publication	454 - 466
a	10.8321 ± 0.0002 Å
b	12.6641 ± 0.0003 Å
c	15.4456 ± 0.0003 Å
α	99.1067 ± 0.0016°
β	91.2955 ± 0.0016°
γ	104.338 ± 0.0018°
Cell volume	2022.7 ± 0.08 Å³
Cell temperature	99.92 ± 0.18 K
Ambient diffraction temperature	99.92 ± 0.18 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0296
Residual factor for significantly intense reflections	0.0283
Weighted residual factors for significantly intense reflections	0.0709
Weighted residual factors for all reflections included in the refinement	0.0719
Goodness-of-fit parameter for all reflections included in the refinement	1.076
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
289518 (current)	2024-02-04	cif/ Updating files of 7714599, 7714600, 7714601, 7714602 Original log message: Adding full bibliography for 7714599--7714602.cif.	7714600.cif
288024	2023-12-05	cif/ Adding structures of 7714599, 7714600, 7714601, 7714602 via cif-deposit CGI script.	7714600.cif