Crystallography Open Database

Information card for entry 7714798

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Coordinates	7714798.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H72 Fe2 N12
Calculated formula	C32 H72 Fe2 N12
Title of publication	<i>N</i>-Alkyl substituted triazenide-bridged homoleptic iron(II) dimers with an exceptionally short Fe-Fe bond.
Authors of publication	Soussi, Khaled; Jeanneau, Erwann; Maldivi, Pascale; Clémancey, Martin; Latour, Jean-Marc; Khrouz, Lhoussain; Lorentz, Chantal; Daniele, Stéphane; Mishra, Shashank
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	4
Pages of publication	1439 - 1444
a	19.115 ± 0.002 Å
b	11.7866 ± 0.0008 Å
c	21.137 ± 0.002 Å
α	90°
β	120.907 ± 0.016°
γ	90°
Cell volume	4086 ± 0.9 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0701
Residual factor for significantly intense reflections	0.0547
Weighted residual factors for significantly intense reflections	0.1405
Weighted residual factors for all reflections included in the refinement	0.1618
Goodness-of-fit parameter for all reflections included in the refinement	1.111
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
289499 (current)	2024-02-04	cif/ Updating files of 7714797, 7714798 Original log message: Adding full bibliography for 7714797--7714798.cif.	7714798.cif
288491	2023-12-22	cif/ Adding structures of 7714797, 7714798 via cif-deposit CGI script.	7714798.cif