Crystallography Open Database

Information card for entry 7714805

Preview

Coordinates	7714805.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H52 F2 N4 Ni2 O9
Calculated formula	C34 H52 F2 N4 Ni2 O9
Title of publication	Tetracosanuclear nickel complexes as effective catalysts for cycloaddition of carbon dioxide with epoxides.
Authors of publication	Liu, Guan-Lin; Wu, En-Hsu; Hung, Yu-Ching; Chou, Wei-Chi; Hung, Chia-Hsin; Lin, Chu-Chieh; Ko, Bao-Tsan
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	4
Pages of publication	1425 - 1429
a	14.773 ± 0.0005 Å
b	12.7347 ± 0.0005 Å
c	20.8529 ± 0.0008 Å
α	90°
β	92.829 ± 0.002°
γ	90°
Cell volume	3918.3 ± 0.3 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0363
Residual factor for significantly intense reflections	0.0283
Weighted residual factors for significantly intense reflections	0.0699
Weighted residual factors for all reflections included in the refinement	0.074
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
289505 (current)	2024-02-04	cif/ Updating files of 7714805, 7714806, 7714807, 7714808, 7714809, 7714810 Original log message: Adding full bibliography for 7714805--7714810.cif.	7714805.cif
288494	2023-12-22	cif/ Adding structures of 7714805, 7714806, 7714807, 7714808, 7714809, 7714810 via cif-deposit CGI script.	7714805.cif