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Information card for entry 7714919
Preview
| Coordinates | 7714919.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C56 H57 F6 N7 Ni |
|---|---|
| Calculated formula | C42 H41 F6 N7 Ni |
| Title of publication | A mesoionic carbene stabilized nickel(II) hydroxide complex: a facile precursor for C-H activation chemistry. |
| Authors of publication | Pavun, Anna; Niess, Raffael; Scheibel, Lucas A.; Seidl, Michael; Hohloch, Stephan |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2024 |
| Journal volume | 53 |
| Journal issue | 6 |
| Pages of publication | 2749 - 2761 |
| a | 9.6617 ± 0.0005 Å |
| b | 15.7074 ± 0.0008 Å |
| c | 18.8918 ± 0.001 Å |
| α | 67.512 ± 0.002° |
| β | 75.835 ± 0.002° |
| γ | 77.315 ± 0.002° |
| Cell volume | 2542.9 ± 0.2 Å3 |
| Cell temperature | 153 K |
| Ambient diffraction temperature | 153 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0846 |
| Residual factor for significantly intense reflections | 0.0703 |
| Weighted residual factors for significantly intense reflections | 0.1951 |
| Weighted residual factors for all reflections included in the refinement | 0.2077 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.04 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 290167 (current) | 2024-03-04 | cif/ Updating files of 7714908, 7714909, 7714910, 7714911, 7714912, 7714913, 7714914, 7714915, 7714916, 7714917, 7714918, 7714919, 7714920 Original log message: Adding full bibliography for 7714908--7714920.cif. |
7714919.cif |
| 288690 | 2024-01-05 | cif/ Adding structures of 7714908, 7714909, 7714910, 7714911, 7714912, 7714913, 7714914, 7714915, 7714916, 7714917, 7714918, 7714919, 7714920 via cif-deposit CGI script. |
7714919.cif |
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Users of the data should acknowledge the original authors of the
structural data.