Crystallography Open Database

Information card for entry 7715207

Preview

Coordinates	7715207.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C9 H35 B18 Co I N
Calculated formula	C9 H35 B18 Co I N
Title of publication	Synthetic routes to carbon substituted cobalt bis(dicarbollide) alkyl halides and aromatic amines along with closely related irregular pathways.
Authors of publication	Nekvinda, Jan; Bavol, Dmytro; Litecká, Miroslava; Tüzün, Ece Zeynep; Dušek, Michal; Grüner, Bohumír
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	13
Pages of publication	5816 - 5826
a	11.0665 ± 0.0002 Å
b	10.5685 ± 0.0003 Å
c	10.2132 ± 0.0002 Å
α	90°
β	95.816 ± 0.002°
γ	90°
Cell volume	1188.35 ± 0.05 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	6
Space group number	7
Hermann-Mauguin space group symbol	P 1 c 1
Hall space group symbol	P -2yc
Residual factor for all reflections	0.0518
Residual factor for significantly intense reflections	0.0485
Weighted residual factors for significantly intense reflections	0.1328
Weighted residual factors for all reflections included in the refinement	0.1374
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
290943 (current)	2024-04-05	cif/ Updating files of 7715207, 7715208, 7715209, 7715210, 7715211, 7715212 Original log message: Adding full bibliography for 7715207--7715212.cif.	7715207.cif
289920	2024-02-22	cif/ Adding structures of 7715207, 7715208, 7715209, 7715210, 7715211, 7715212 via cif-deposit CGI script.	7715207.cif