Crystallography Open Database

Information card for entry 7715243

Preview

Coordinates	7715243.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C2 H4 K6 N2 Na4 Ni2 O51 Ta10
Calculated formula	C2 H4 K6 N2 Na4 Ni2 O51 Ta10
Title of publication	Two binuclear Ni-inserted polyoxotantalates based on {NiTa10O32} units with catalytic activity
Authors of publication	Zhao, Hui; Chen, Hanhan; yang Zhang, Ming; Yang, Yuanyuan; Yang, Zongfei; Ma, Pengtao; Niu, Jingyang; Wang, Jingping
Journal of publication	Dalton Transactions
Year of publication	2024
Journal volume	53
Journal issue	12
Pages of publication	5562 - 5566
a	43.8013 ± 0.0013 Å
b	14.123 ± 0.0003 Å
c	20.2049 ± 0.0005 Å
α	90°
β	113.429 ± 0.001°
γ	90°
Cell volume	11468.4 ± 0.5 Å³
Cell temperature	149.9 K
Ambient diffraction temperature	150 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0645
Residual factor for significantly intense reflections	0.0423
Weighted residual factors for significantly intense reflections	0.1091
Weighted residual factors for all reflections included in the refinement	0.125
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
290990 (current)	2024-04-05	cif/ Updating files of 7715243, 7715244 Original log message: Adding full bibliography for 7715243--7715244.cif.	7715243.cif
289955	2024-02-25	cif/ Adding structures of 7715243, 7715244 via cif-deposit CGI script.	7715243.cif