Crystallography Open Database

Information card for entry 7715313

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Coordinates	7715313.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H46 K O6 P S
Calculated formula	C30 H46 K O6 P S
Title of publication	Coordination chemistry of alkali metal dimesityl-thio- and dimesityl-selenophosphinites [(L)<sub>2</sub>A-EPMes<sub>2</sub>]<sub>2</sub> (A = Li, Na, K; E = S, Se; L = THF, THP) and [(18C6)K-SPMes<sub>2</sub>].
Authors of publication	Dorow, Richard C. C.; Liebing, Phil; Görls, Helmar; Westerhausen, Matthias
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	12
Pages of publication	5711 - 5720
a	11.4806 ± 0.0014 Å
b	14.5572 ± 0.0016 Å
c	19.572 ± 0.002 Å
α	90°
β	97.148 ± 0.003°
γ	90°
Cell volume	3245.6 ± 0.6 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0768
Residual factor for significantly intense reflections	0.0508
Weighted residual factors for significantly intense reflections	0.1167
Weighted residual factors for all reflections included in the refinement	0.1342
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
290977 (current)	2024-04-05	cif/ Updating files of 7715309, 7715310, 7715311, 7715312, 7715313, 7715314, 7715315, 7715316, 7715317, 7715318 Original log message: Adding full bibliography for 7715309--7715318.cif.	7715313.cif
290015	2024-03-01	cif/ Adding structures of 7715309, 7715310, 7715311, 7715312, 7715313, 7715314, 7715315, 7715316, 7715317, 7715318 via cif-deposit CGI script.	7715313.cif