Crystallography Open Database

Information card for entry 7715936

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Coordinates	7715936.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H34 Cu N4 O2
Calculated formula	C38 H34 Cu N4 O2
Title of publication	Dibenzoazepine hydrazine is a building block for <i>N</i>-alkene hybrid ligands: exploratory syntheses of complexes of Cu, Fe, and Li.
Authors of publication	Grasruck, Alexander; Schall, Kristina; Heinemann, Frank W.; Langer, Jens; Herrera, Alberto; Frieß, Sybille; Schmid, Günter; Dorta, Romano
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	20
Pages of publication	8642 - 8656
a	10.6663 ± 0.0001 Å
b	39.1923 ± 0.0005 Å
c	15.0354 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	6285.35 ± 0.13 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	5
Space group number	43
Hermann-Mauguin space group symbol	F d d 2
Hall space group symbol	F 2 -2d
Residual factor for all reflections	0.0224
Residual factor for significantly intense reflections	0.0224
Weighted residual factors for significantly intense reflections	0.0599
Weighted residual factors for all reflections included in the refinement	0.0599
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
293095 (current)	2024-07-05	cif/ Updating files of 7715932, 7715933, 7715934, 7715935, 7715936, 7715937, 7715938, 7715939, 7715940 Original log message: Adding full bibliography for 7715932--7715940.cif.	7715936.cif
291467	2024-05-03	cif/ Adding structures of 7715932, 7715933, 7715934, 7715935, 7715936, 7715937, 7715938, 7715939, 7715940 via cif-deposit CGI script.	7715936.cif