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Information card for entry 7716741
Preview
| Coordinates | 7716741.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C40 H49 N4 O2 Pd |
|---|---|
| Calculated formula | C40 H49 N4 O2 Pd |
| Title of publication | Ni(II) and Pd(II) complexes of a new redox-active pentadentate azo-appended 2-aminophenol ligand: Pd(II)-assisted intraligand cyclization forms a phenoxazinyl ring. |
| Authors of publication | Bhowmik, Saumitra; Sengupta, Arunava; Mukherjee, Rabindranath |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2024 |
| Journal volume | 53 |
| Journal issue | 33 |
| Pages of publication | 14046 - 14064 |
| a | 9.6069 ± 0.0009 Å |
| b | 11.3196 ± 0.001 Å |
| c | 17.4614 ± 0.0016 Å |
| α | 72.042 ± 0.003° |
| β | 81.586 ± 0.003° |
| γ | 89.255 ± 0.003° |
| Cell volume | 1785.9 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0472 |
| Residual factor for significantly intense reflections | 0.0376 |
| Weighted residual factors for significantly intense reflections | 0.0824 |
| Weighted residual factors for all reflections included in the refinement | 0.0887 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.074 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 294562 (current) | 2024-09-06 | cif/ Updating files of 7716740, 7716741, 7716742, 7716743 Original log message: Adding full bibliography for 7716740--7716743.cif. |
7716741.cif |
| 293548 | 2024-07-26 | cif/ Adding structures of 7716740, 7716741, 7716742, 7716743 via cif-deposit CGI script. |
7716741.cif |
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Users of the data should acknowledge the original authors of the
structural data.