Crystallography Open Database

Information card for entry 7716750

Preview

Coordinates	7716750.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H86 Mn2 N6
Calculated formula	C58 H86 Mn2 N6
Title of publication	Manganese catalysed dehydrocoupling of silanes and siloxanes with ammonia to prepare oligosilazanes and polysiloxazanes.
Authors of publication	Mehta, Gautam K.; Nguyen, Thao T.; Flores, Marco; Trovitch, Ryan J.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	34
Pages of publication	14272 - 14277
a	22.875 ± 0.01 Å
b	14.747 ± 0.007 Å
c	16.257 ± 0.007 Å
α	90°
β	91.125 ± 0.008°
γ	90°
Cell volume	5483 ± 4 Å³
Cell temperature	123 ± 0.1 K
Ambient diffraction temperature	123 ± 0.1 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.063
Residual factor for significantly intense reflections	0.049
Weighted residual factors for significantly intense reflections	0.1203
Weighted residual factors for all reflections included in the refinement	0.1273
Goodness-of-fit parameter for all reflections included in the refinement	1.051
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
294588 (current)	2024-09-06	cif/ Updating files of 7716750 Original log message: Adding full bibliography for 7716750.cif.	7716750.cif
293574	2024-07-28	cif/ Adding structures of 7716750 via cif-deposit CGI script.	7716750.cif