Crystallography Open Database

Information card for entry 7716963

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Coordinates	7716963.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C4 H18 Li O7 P
Calculated formula	C4 H18 Li O7 P
Title of publication	Facile room-temperature synthesis of layered transition metal phosphonates <i>via</i> hitherto unknown alkali metal <i>tert</i>-butyl phosphonates.
Authors of publication	Kumar, Anuj; Ghatak, Aheli; Murugavel, Ramaswamy
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	34
Pages of publication	14399 - 14410
a	6.2774 ± 0.0003 Å
b	6.5742 ± 0.0004 Å
c	15.5423 ± 0.0008 Å
α	79.599 ± 0.004°
β	88.942 ± 0.004°
γ	63.141 ± 0.005°
Cell volume	561.36 ± 0.06 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0705
Residual factor for significantly intense reflections	0.0632
Weighted residual factors for significantly intense reflections	0.1661
Weighted residual factors for all reflections included in the refinement	0.1742
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
294368 (current)	2024-09-04	cif/ Adding structures of 7716963, 7716964, 7716965 via cif-deposit CGI script.	7716963.cif