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Information card for entry 7717301
Preview
| Coordinates | 7717301.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C110 H184 B E4 N8 O4 |
|---|---|
| Calculated formula | C100 H160 Be4 N8 O4 |
| Title of publication | Synthesis and structures of molecular beryllium Grignard analogues featuring terminal and bridging pseudohalides. |
| Authors of publication | Czernetzki, Corinna; Arrowsmith, Merle; Jürgensen, Malte; Hagspiel, Stephan; Braunschweig, Holger |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2024 |
| Journal volume | 53 |
| Journal issue | 45 |
| Pages of publication | 18296 - 18303 |
| a | 35.978 ± 0.006 Å |
| b | 25.4382 ± 0.0016 Å |
| c | 36.315 ± 0.003 Å |
| α | 90° |
| β | 92.089 ± 0.01° |
| γ | 90° |
| Cell volume | 33214 ± 7 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | I 1 2/a 1 |
| Hall space group symbol | -I 2ya |
| Residual factor for all reflections | 0.2933 |
| Residual factor for significantly intense reflections | 0.155 |
| Weighted residual factors for significantly intense reflections | 0.4058 |
| Weighted residual factors for all reflections included in the refinement | 0.4805 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.307 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Diffraction radiation X-ray symbol | K-L~2,3~ |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 296603 (current) | 2024-12-06 | cif/ Updating files of 7717294, 7717295, 7717296, 7717297, 7717298, 7717299, 7717300, 7717301 Original log message: Adding full bibliography for 7717294--7717301.cif. |
7717301.cif |
| 295645 | 2024-10-26 | cif/ Adding structures of 7717294, 7717295, 7717296, 7717297, 7717298, 7717299, 7717300, 7717301 via cif-deposit CGI script. |
7717301.cif |
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Users of the data should acknowledge the original authors of the
structural data.