Crystallography Open Database

Information card for entry 7717304

Preview

Coordinates	7717304.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H27 B2 F15 N2 Si
Calculated formula	C36 H27 B2 F15 N2 Si
Title of publication	Reactions of 1,1- and 1,2-bis-boranes with a protic diamine and hydrazine.
Authors of publication	Yeung, Jason; Yeganeh-Salman, Amir; Miao, Linkun; Stephan, Douglas W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	46
Pages of publication	18727 - 18735
a	15.869 ± 0.003 Å
b	10.5026 ± 0.0018 Å
c	21.376 ± 0.004 Å
α	90°
β	96.3 ± 0.006°
γ	90°
Cell volume	3541.1 ± 1.1 Å³
Cell temperature	149.91 K
Ambient diffraction temperature	149.91 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1199
Residual factor for significantly intense reflections	0.087
Weighted residual factors for significantly intense reflections	0.2108
Weighted residual factors for all reflections included in the refinement	0.2494
Goodness-of-fit parameter for all reflections included in the refinement	0.9993
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
296556 (current)	2024-12-06	cif/ Updating files of 7717302, 7717303, 7717304, 7717305, 7717306, 7717307, 7717308 Original log message: Adding full bibliography for 7717302--7717308.cif.	7717304.cif
295646	2024-10-26	cif/ Adding structures of 7717302, 7717303, 7717304, 7717305, 7717306, 7717307, 7717308 via cif-deposit CGI script.	7717304.cif