Crystallography Open Database

Information card for entry 7717343

Preview

Coordinates	7717343.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H76 Na2 O6 P2
Calculated formula	C52 H76 Na2 O6 P2
Title of publication	Syntheses and structures of dimesitylphosphinite complexes of alkali metals and their catalytic activity in hydrophosphorylation reactions.
Authors of publication	Fener, Benjamin E.; Schüler, Philipp; Liebing, Phil; Görls, Helmar; Westerhausen, Matthias
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	54
Journal issue	1
Pages of publication	181 - 197
a	20.729 ± 0.002 Å
b	15.1741 ± 0.0017 Å
c	16.7183 ± 0.0017 Å
α	90°
β	102.606 ± 0.004°
γ	90°
Cell volume	5131.9 ± 0.9 Å³
Cell temperature	120 K
Ambient diffraction temperature	120 K
Number of distinct elements	5
Space group number	7
Hermann-Mauguin space group symbol	P 1 c 1
Hall space group symbol	P -2yc
Residual factor for all reflections	0.1137
Residual factor for significantly intense reflections	0.0681
Weighted residual factors for significantly intense reflections	0.1305
Weighted residual factors for all reflections included in the refinement	0.1562
Goodness-of-fit parameter for all reflections included in the refinement	1.106
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
298236 (current)	2025-03-04	cif/ Updating files of 7717331, 7717332, 7717333, 7717334, 7717335, 7717336, 7717337, 7717338, 7717339, 7717340, 7717341, 7717342, 7717343, 7717344, 7717345, 7717346 Original log message: Adding full bibliography for 7717331--7717346.cif.	7717343.cif
295702	2024-11-01	cif/ Adding structures of 7717331, 7717332, 7717333, 7717334, 7717335, 7717336, 7717337, 7717338, 7717339, 7717340, 7717341, 7717342, 7717343, 7717344, 7717345, 7717346 via cif-deposit CGI script.	7717343.cif