Crystallography Open Database

Information card for entry 7717490

Preview

Coordinates	7717490.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H46 Cl3 P Ru2
Calculated formula	C45 H46 Cl3 P Ru2
Title of publication	Phosphanylphosphaalkenes as precursors for metallaphosphaalkene complexes.
Authors of publication	Ziółkowska, Aleksandra; Kruczyński, Tomasz; Gudat, Dietrich; Ponikiewski, Łukasz
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	48
Pages of publication	19107 - 19111
a	16.3325 ± 0.0005 Å
b	16.6265 ± 0.0005 Å
c	16.9118 ± 0.0005 Å
α	74.161 ± 0.002°
β	78.653 ± 0.002°
γ	87.765 ± 0.002°
Cell volume	4331.2 ± 0.2 Å³
Cell temperature	120 K
Ambient diffraction temperature	120 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0655
Residual factor for significantly intense reflections	0.0481
Weighted residual factors for significantly intense reflections	0.1186
Weighted residual factors for all reflections included in the refinement	0.1327
Goodness-of-fit parameter for all reflections included in the refinement	1.015
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
297119 (current)	2025-01-06	cif/ Updating files of 7717484, 7717485, 7717486, 7717487, 7717488, 7717489, 7717490 Original log message: Adding full bibliography for 7717484--7717490.cif.	7717490.cif
295908	2024-11-14	cif/ Adding structures of 7717484, 7717485, 7717486, 7717487, 7717488, 7717489, 7717490 via cif-deposit CGI script.	7717490.cif