Crystallography Open Database

Information card for entry 7717634

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Coordinates	7717634.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	[La(Cp')2(OiPr)]2
Formula	C38 H66 La2 O2 Si4
Calculated formula	C38 H66 La2 O2 Si4
Title of publication	Synthesis and reduction of [(C<sub>5</sub>H<sub>4</sub>SiMe<sub>3</sub>)<sub>2</sub>Ln(μ-OR)]<sub>2</sub> (Ln = La, Ce) complexes: structural effects of bridging alkoxides.
Authors of publication	Brown, Adrian N.; Kelleher, Jack N.; Brown, Alexander M.; Saghy, Peter; Bohl, Joshua J.; Robinson, Jerome R.; Huh, Daniel N.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	47
Pages of publication	18856 - 18864
a	18.0071 ± 0.0007 Å
b	13.843 ± 0.0006 Å
c	18.6821 ± 0.0007 Å
α	90°
β	101.345 ± 0.002°
γ	90°
Cell volume	4565.9 ± 0.3 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	5
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.0259
Residual factor for significantly intense reflections	0.0226
Weighted residual factors for significantly intense reflections	0.0529
Weighted residual factors for all reflections included in the refinement	0.055
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
296219 (current)	2024-12-05	cif/ Adding structures of 7717632, 7717633, 7717634 via cif-deposit CGI script.	7717634.cif