Crystallography Open Database

Information card for entry 7717816

Preview

Coordinates	7717816.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H38 N2 O Zn
Calculated formula	C28 H38 N2 O Zn
Title of publication	Alkyl zinc complexes derived from formylfluorenimide ligands: synthesis, characterization and catalysis for hydroboration of aldehydes and ketones.
Authors of publication	Wei, Biao; Qin, Zhibiao; Miao, Hui; Wang, Chaoqun; Huang, Mengna; Liu, Chenxu; Bai, Cuibing; Chen, Zheng
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	8
Pages of publication	3427 - 3436
a	28.7896 ± 0.0019 Å
b	28.7896 ± 0.0019 Å
c	19.0194 ± 0.0009 Å
α	90°
β	90°
γ	120°
Cell volume	13652.1 ± 1.4 Å³
Cell temperature	293.15 K
Ambient diffraction temperature	293.15 K
Number of distinct elements	5
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.0878
Residual factor for significantly intense reflections	0.0488
Weighted residual factors for significantly intense reflections	0.1136
Weighted residual factors for all reflections included in the refinement	0.1272
Goodness-of-fit parameter for all reflections included in the refinement	1.005
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
298259 (current)	2025-03-04	cif/ Updating files of 7717814, 7717815, 7717816, 7717817, 7717818 Original log message: Adding full bibliography for 7717814--7717818.cif.	7717816.cif
297340	2025-01-16	cif/ Adding structures of 7717814, 7717815, 7717816, 7717817, 7717818 via cif-deposit CGI script.	7717816.cif