Crystallography Open Database

Information card for entry 7718131

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Coordinates	7718131.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C76 H87 Cl2 N3 O2 Sn
Calculated formula	C76 H87 Cl2 N3 O2 Sn
Title of publication	Redox-active tin(II) complexes with sterically demanding <i>o</i>-phenylenediamido ligands and their reactivity with organic azides.
Authors of publication	Sugimoto, Hideki; Yoneda, Akira; Yano, Mayuka; Sato, Kazunobu; Shiota, Yoshihito; Miyanishi, Mayuko; Yoshizawa, Kazunari; Itoh, Shinobu
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
a	17.3591 ± 0.0007 Å
b	18.5527 ± 0.0009 Å
c	22.2644 ± 0.0009 Å
α	90°
β	106.496 ± 0.007°
γ	90°
Cell volume	6875.3 ± 0.6 Å³
Cell temperature	115 K
Ambient diffraction temperature	115 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0553
Residual factor for significantly intense reflections	0.045
Weighted residual factors for significantly intense reflections	0.1116
Weighted residual factors for all reflections included in the refinement	0.1162
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
297855 (current)	2025-02-26	cif/ Adding structures of 7718127, 7718128, 7718129, 7718130, 7718131 via cif-deposit CGI script.	7718131.cif