Crystallography Open Database

Information card for entry 7719207

7719206 << 7719207 >> 7719208

Preview

Coordinates	7719207.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H52 N5 P2
Calculated formula	C41 H52 N5 P2
Title of publication	A new class of ligand derived from the reactions of bis(dialkylphosphino)amines and 9-diazofluorene: preparation, structure and reactivity.
Authors of publication	Laprade, Matthew J. J.; Robertson, Katherine N.; Clyburne, Jason A. C.; Kozak, Christopher M.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	29
Pages of publication	11382 - 11397
a	9.675 ± 0.003 Å
b	13.444 ± 0.005 Å
c	15.414 ± 0.005 Å
α	69.68 ± 0.004°
β	86.86 ± 0.004°
γ	88.453 ± 0.004°
Cell volume	1877.2 ± 1.1 Å³
Cell temperature	125 ± 2 K
Ambient diffraction temperature	125 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.183
Residual factor for significantly intense reflections	0.0678
Weighted residual factors for significantly intense reflections	0.1225
Weighted residual factors for all reflections included in the refinement	0.1617
Goodness-of-fit parameter for all reflections included in the refinement	0.937
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
301446 (current)	2025-08-04	cif/ Adding structures of 7719207, 7719208, 7719209, 7719210, 7719211, 7719212, 7719213, 7719214 via cif-deposit CGI script.	7719207.cif