Crystallography Open Database

Information card for entry 7719507

7719506 << 7719507 >> 7719508

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Coordinates	7719507.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H58 O4 P4 Rh2
Calculated formula	C64 H58 O4 P4 Rh2
Title of publication	Sodium phosphaethynolate as P-source for the synthesis of molecular rhodium phosphides: an exploratory study.
Authors of publication	Li, Zhongshu; Borger, Jaap E.; Gianetti, Thomas L.; Müller, Fabian; Pribanic, Bruno; Coburger, Peter; Grützmacher, Hansjörg
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	45
Pages of publication	16718 - 16726
a	17.8929 ± 0.0005 Å
b	28.2041 ± 0.0007 Å
c	12.3931 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	6254.2 ± 0.3 Å³
Cell temperature	100 K
Ambient diffraction temperature	100.02 K
Number of distinct elements	5
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0504
Residual factor for significantly intense reflections	0.0438
Weighted residual factors for significantly intense reflections	0.0934
Weighted residual factors for all reflections included in the refinement	0.0964
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
303820 (current)	2025-11-29	cif/ Updating files of 7719506, 7719507, 7719508, 7719509, 7719510 Original log message: Adding full bibliography for 7719506--7719510.cif.	7719507.cif
302297	2025-09-30	cif/ Adding structures of 7719506, 7719507, 7719508, 7719509, 7719510 via cif-deposit CGI script.	7719507.cif