Crystallography Open Database

Information card for entry 8102114

Preview

Coordinates	8102114.cif

Structure parameters

Chemical name	dichloro((S)-2-(anilinomethyl)-pyrrolidine)palladium(II)
Formula	C11 H16 Cl2 N2 Pd
Calculated formula	C11 H16 Cl2 N2 Pd
Title of publication	Crystal structure of dichloro((S)-2-(anilinomethyl)pyrrolidine)-palladium (II), Pd(Cl)~2~(C~11~H~16~N~2~)
Authors of publication	El Firdoussi, Larbi; Ait Ali, Mustapha; Karim, Abdallah; Spannenberg, Anke
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2007
Journal volume	222
Journal issue	3
Pages of publication	195 - 196
a	11.246 ± 0.002 Å
b	12.222 ± 0.002 Å
c	19.637 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	2699.1 ± 0.9 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0316
Residual factor for significantly intense reflections	0.0265
Weighted residual factors for significantly intense reflections	0.0587
Weighted residual factors for all reflections included in the refinement	0.0604
Goodness-of-fit parameter for all reflections included in the refinement	0.986
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176728 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8.	8102114.cif
108388	2014-03-31	cif/8/ (antanas@lokys.ibt.lt) Adding and updating bibliographic information: volume, authors, issue, first page, last page.	8102114.cif
35911	2012-02-28	cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree.	8102114.cif
12853	2011-03-06	../uploads/cif-deposit/cod/cif Adding structures of 8102114 via cif-deposit CGI script.	8102114.cif