Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 8102153
Preview
| Coordinates | 8102153.cif |
|---|
| Chemical name | bis(μ-bromo)-tetrakis(tert-butyl-(4-methyl-pyridin-2-yl)-amine)-dicopper(I) |
|---|---|
| Formula | C40 H64 Br2 Cu2 N8 |
| Calculated formula | C40 H64 Br2 Cu2 N8 |
| Title of publication | Crystal structure of bis(μ-bromo)-tetrakis(tert-butyl-(4-methyl- pyridin-2-yl)-amine)-dicopper(I), Cu~2~Br~2~(C~10~H~16~N~2~)~4~ |
| Authors of publication | Glatz, Germund; Irrgang, Torsten; Kempe, Rhett |
| Journal of publication | Zeitschrift für Kristallographie - New Crystal Structures |
| Year of publication | 2007 |
| Journal volume | 222 |
| Journal issue | 3 |
| Pages of publication | 287 - 288 |
| a | 11.389 ± 0.0007 Å |
| b | 16.507 ± 0.0008 Å |
| c | 23.728 ± 0.0019 Å |
| α | 90° |
| β | 96.604 ± 0.006° |
| γ | 90° |
| Cell volume | 4431.2 ± 0.5 Å3 |
| Cell temperature | 191 ± 2 K |
| Ambient diffraction temperature | 191 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0776 |
| Residual factor for significantly intense reflections | 0.0393 |
| Weighted residual factors for significantly intense reflections | 0.0728 |
| Weighted residual factors for all reflections included in the refinement | 0.0806 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.854 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176728 (current) | 2016-02-18 | cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8. |
8102153.cif |
| 108388 | 2014-03-31 | cif/8/ (antanas@lokys.ibt.lt) Adding and updating bibliographic information: volume, authors, issue, first page, last page. |
8102153.cif |
| 35911 | 2012-02-28 | cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree. |
8102153.cif |
| 12892 | 2011-03-06 | ../uploads/cif-deposit/cod/cif Adding structures of 8102153 via cif-deposit CGI script. |
8102153.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.