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Information card for entry 8102223
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| Coordinates | 8102223.cif |
|---|
| Chemical name | tris(ethylenediamine)nickel(II) diperchlorate 2-(4-pyridyl)-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide solvate monohydrate |
|---|---|
| Formula | C18 H42 Cl2 N9 Ni O11 |
| Calculated formula | C18 H42 Cl2 N9 Ni O11 |
| Title of publication | Crystal structure of tris(ethylenediamine)nickel(II) diperchlorate 2-(4-pyridyl)-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide solvate monohydrate, [Ni(C~2~H~8~N~2~)~3~][ClO~4~]~2~ · C~12~H~16~N~3~O~2~ · H~2~O |
| Authors of publication | Wang, Yu-Fang; Liu, Yuan-Ying |
| Journal of publication | Zeitschrift für Kristallographie - New Crystal Structures |
| Year of publication | 2007 |
| Journal volume | 222 |
| Journal issue | 4 |
| Pages of publication | 439 - 441 |
| a | 9.897 ± 0.002 Å |
| b | 15.461 ± 0.004 Å |
| c | 10.407 ± 0.002 Å |
| α | 90° |
| β | 99.292 ± 0.003° |
| γ | 90° |
| Cell volume | 1571.6 ± 0.6 Å3 |
| Cell temperature | 291 ± 2 K |
| Ambient diffraction temperature | 291 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0933 |
| Residual factor for significantly intense reflections | 0.0728 |
| Weighted residual factors for significantly intense reflections | 0.1819 |
| Weighted residual factors for all reflections included in the refinement | 0.2037 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.995 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176728 (current) | 2016-02-18 | cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8. |
8102223.cif |
| 108390 | 2014-03-31 | cif/8/ (antanas@lokys.ibt.lt) Adding and updating bibliographic information: volume, authors, issue, first page, last page. |
8102223.cif |
| 108108 | 2014-03-27 | cif/8/ (antanas@lokys.ibt.lt) Removing some extra characters introduced while converting CIF's from one encoding into the other. |
8102223.cif |
| 35911 | 2012-02-28 | cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree. |
8102223.cif |
| 12962 | 2011-03-06 | ../uploads/cif-deposit/cod/cif Adding structures of 8102223 via cif-deposit CGI script. |
8102223.cif |
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