Crystallography Open Database

Information card for entry 8102231

Preview

Coordinates	8102231.cif

Structure parameters

Chemical name	tris(2,2'-bipyridine)iron(II) catena-bis((tris-μ-iodo)-plumbate(II))
Formula	C30 H24 Fe I6 N6 Pb2
Calculated formula	C30 H24 Fe I6 N6 Pb2
Title of publication	Crystal structure of tris(2,2'-bipyridine)iron(II) catena-bis((tris-μ-iodo)-plumbate(II)), [Fe(C10H8N2)3][PbI3]2
Authors of publication	Le-Qing Fan; Ji-Huai Wu
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2008
Journal volume	223
Journal issue	1
Pages of publication	72
a	16.906 ± 0.002 Å
b	14.6045 ± 0.0016 Å
c	16.536 ± 0.003 Å
α	90°
β	101.534 ± 0.008°
γ	90°
Cell volume	4000.4 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0911
Residual factor for significantly intense reflections	0.0759
Weighted residual factors for significantly intense reflections	0.1362
Weighted residual factors for all reflections included in the refinement	0.1419
Goodness-of-fit parameter for all reflections included in the refinement	1.245
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MolybdenumKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176728 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8.	8102231.cif
35911	2012-02-28	cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree.	8102231.cif
12970	2011-03-06	../uploads/cif-deposit/cod/cif Adding structures of 8102231 via cif-deposit CGI script.	8102231.cif