Crystallography Open Database

Information card for entry 8102577

Preview

Coordinates	8102577.cif

Structure parameters

Chemical name	[[(2-(2-chloro-6-fluorophenyl)-1H-imidazo[4,5-f][1,10]phenanthroline- <i>κ</i>^2^<i>N</i>,<i>N</i>')lead(II)]-μ~2~-adipicato], [Pb(C~19~H~10~N~4~FCl)(C~6~H~8~O~4~)]
Formula	C25 H18 Cl F N4 O4 Pb
Calculated formula	C25 H18 Cl F N4 O4 Pb
Title of publication	Crystal structure of [(2-(2-chloro-6-fluorophenyl)-1H-imidazo-[4,5-f][1,10]phenanthroline-k2N,N')]-(m2-adipato)lead(II), Pb(C19H10N4FCl)(C6H8O4)
Authors of publication	Xiu-Yan Wang; Ming Wang; Wan-Qiu Yu; Ya-Ming Sun
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2010
Journal volume	225
Journal issue	1
Pages of publication	74
a	13.056 ± 0.002 Å
b	9.2897 ± 0.0015 Å
c	19.126 ± 0.003 Å
α	90°
β	100.682 ± 0.002°
γ	90°
Cell volume	2279.5 ± 0.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0464
Residual factor for significantly intense reflections	0.0398
Weighted residual factors for significantly intense reflections	0.1161
Weighted residual factors for all reflections included in the refinement	0.1213
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176728 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8.	8102577.cif
35911	2012-02-28	cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree.	8102577.cif
13316	2011-03-06	../uploads/cif-deposit/cod/cif Adding structures of 8102577 via cif-deposit CGI script.	8102577.cif