Crystallography Open Database

Information card for entry 8102873

Preview

Coordinates	8102873.cif

Structure parameters

Formula	C48 H46 Cl2 Cu2 N10 O14
Calculated formula	C48 H34 Cl2 Cu2 N10 O14
Title of publication	Crystal structure of tetra(2,2'-bipyridine)oxalatodicopper(II) bisperchlorate — N,N-dimethylformamide (1:2), [Cu2(C10H8N2)4(C2O4)][ClO4]2 · 2C3H7NO
Authors of publication	Qin Huang; Li-Hong Diao; Xian-Hong Yin
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2010
Journal volume	225
Journal issue	4
Pages of publication	781
a	9.7762 ± 0.0003 Å
b	11.2177 ± 0.0004 Å
c	12.3579 ± 0.0004 Å
α	98.675 ± 0.002°
β	99.193 ± 0.002°
γ	92.854 ± 0.002°
Cell volume	1318.74 ± 0.08 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0682
Residual factor for significantly intense reflections	0.0528
Weighted residual factors for significantly intense reflections	0.1601
Weighted residual factors for all reflections included in the refinement	0.1737
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
211175 (current)	2018-09-26	cif/ Removing _chemical_name_systematic and _chemical_name_common data items with placeholder values from 513 entries in range 8.	8102873.cif
176728	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8.	8102873.cif
35911	2012-02-28	cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree.	8102873.cif
13612	2011-03-06	../uploads/cif-deposit/cod/cif Adding structures of 8102873 via cif-deposit CGI script.	8102873.cif