Crystallography Open Database

Information card for entry 8103107

Preview

Coordinates	8103107.cif

Structure parameters

Chemical name	Bis(μ~3~-Oxo)-Bis[μ~2~-2-(2-Formylphenoxy)acetato-O,O'] -Bis[μ~2~-2-(2-Formylphenoxy)acetato-O,O']-Octakis(n-Butyl)-tetra-Tin(IV)
Formula	C34 H50 O9 Sn2
Calculated formula	C34 H50 O9 Sn2
Title of publication	Crystal structure of bis(m3-oxo)-bis[μ2-2-(2-formylphenoxy)acetato-O,O']-bis[m2-2-(2-formylphenoxy)- acetato-O,O']-octakis(n-butyl)tetratin(IV), Sn4O2(C9H7O4)4(C4H9)8
Authors of publication	Rui-Fang Ding; Qi-Bao Wang; Xin-Min Wen
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2011
Journal volume	226
Journal issue	1
Pages of publication	31
a	11.68 ± 0.007 Å
b	12.749 ± 0.008 Å
c	13.991 ± 0.009 Å
α	100.443 ± 0.01°
β	105.201 ± 0.01°
γ	98.874 ± 0.01°
Cell volume	1932 ± 2 Å³
Cell temperature	273 ± 2 K
Ambient diffraction temperature	273 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0904
Residual factor for significantly intense reflections	0.0656
Weighted residual factors for significantly intense reflections	0.1814
Weighted residual factors for all reflections included in the refinement	0.2001
Goodness-of-fit parameter for all reflections included in the refinement	1.16
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176728 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8.	8103107.cif
35911	2012-02-28	cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree.	8103107.cif
29043	2011-11-02	../uploads/cif-deposit/cod/cif Adding structures of 8103107 via cif-deposit CGI script.	8103107.cif