Crystallography Open Database

Information card for entry 8103112

Preview

Coordinates	8103112.cif

Structure parameters

Chemical name	bis[tris(ethylenediamine)cobalt(II)]pentaoxalatocobaltate(III) tetrahydrate
Formula	C22 H56 Co4 N12 O24
Calculated formula	C22 Co4 N12 O24
Title of publication	Crystal structure of bis[tris(ethylenediamine)cobalt(III)] pentaoxalatocobaltate(II) tetrahydrate, [Co(C2H8N2)3]2[Co2(C2O4)5] · 4H2O
Authors of publication	Jaeun Kang; Seungmoon Pyo; Hoseop Yun; Junghwan Do
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2011
Journal volume	226
Journal issue	3
Pages of publication	353
a	7.9875 ± 0.0016 Å
b	10.218 ± 0.002 Å
c	12.873 ± 0.003 Å
α	100.85 ± 0.03°
β	92.14 ± 0.03°
γ	93.57 ± 0.03°
Cell volume	1028.6 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0423
Residual factor for significantly intense reflections	0.0366
Weighted residual factors for significantly intense reflections	0.1131
Weighted residual factors for all reflections included in the refinement	0.1192
Goodness-of-fit parameter for all reflections included in the refinement	1.095
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176728 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8.	8103112.cif
35911	2012-02-28	cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree.	8103112.cif
29053	2011-11-02	../uploads/cif-deposit/cod/cif Adding structures of 8103112 via cif-deposit CGI script.	8103112.cif