Crystallography Open Database

Information card for entry 8103120

Preview

Coordinates	8103120.cif

Structure parameters

Chemical name	pentakis(4,4'-dipyridine)bis(N-Dimethylform amide)copper(II) bis(perchlorate), C~56~H~54~Cl~2~CuN~12~O~10~
Formula	C56 H54 Cl2 Cu N12 O10
Calculated formula	C56 H54 Cl2 Cu N12 O10
Title of publication	Crystal structure of trikis(4,4'-bipyridine)-bis(N-dimethylformamide)copper(II) bis(perchlorate) — pyridine (1:2), [Cu(C10H8N2)3(C3H7O)2][ClO4]2 · 2C10H8N2
Authors of publication	Qin Huang; Zhanqian Song; Xiaoping Rao; Shibin Shang
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2011
Journal volume	226
Journal issue	1
Pages of publication	153
a	29.303 ± 0.013 Å
b	11.041 ± 0.005 Å
c	20.924 ± 0.008 Å
α	90°
β	120.94 ± 0.04°
γ	90°
Cell volume	5806 ± 5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0772
Residual factor for significantly intense reflections	0.0638
Weighted residual factors for significantly intense reflections	0.18
Weighted residual factors for all reflections included in the refinement	0.1947
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176728 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8.	8103120.cif
35911	2012-02-28	cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree.	8103120.cif
29069	2011-11-02	../uploads/cif-deposit/cod/cif Adding structures of 8103120 via cif-deposit CGI script.	8103120.cif