Crystallography Open Database

Information card for entry 8103140

Preview

Coordinates	8103140.cif

Structure parameters

Chemical name	[[dipyrido[7,6 -a:6',7'-c]-3-chloropyrido[2,3-<i>b</i>]quinoxaline)lead(II)]- naphthalene-1,4-dicarboxylato], [Pb(C~17~H~8~N~4~Cl)~2~(C~12~H~6~O~4~)]
Formula	C29 H12 Cl N4 O4 Pb
Calculated formula	C29 H12 Cl N5 O4 Pb
Title of publication	Crystal structure of dipyrido[7,6-a:6',7'-c]-3-chloro-pyrido[2,3-b]-quinoxaline)-(naphthalene-1,4- dicarboxylato)lead(II), Pb(C17H8N4Cl)(C12H6O4)
Authors of publication	Ji-Ku Wang; Hao Chen; Hong-Bin Xu
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2011
Journal volume	226
Journal issue	3
Pages of publication	361
a	10.31 ± 0.005 Å
b	10.521 ± 0.005 Å
c	12.168 ± 0.005 Å
α	80.808 ± 0.005°
β	81.973 ± 0.005°
γ	79.638 ± 0.005°
Cell volume	1273.3 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0595
Residual factor for significantly intense reflections	0.0511
Weighted residual factors for significantly intense reflections	0.1311
Weighted residual factors for all reflections included in the refinement	0.1382
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	8103140.cif
35911	2012-02-28	cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree.	8103140.cif
29109	2011-11-02	../uploads/cif-deposit/cod/cif Adding structures of 8103140 via cif-deposit CGI script.	8103140.cif