Crystallography Open Database

Information card for entry 8103296

Preview

Coordinates	8103296.cif

Structure parameters

Chemical name	catena-poly[[bis(benzo-15-crown-5)ammonium] [silver(I)-di-μ-sulfido-tungstate(VI)(Ag-W)-di-μ-sulfido]]
Formula	C28 H40 Ag N O10 S4 W
Calculated formula	C28 H40 Ag N O10 S4 W
Title of publication	Crystal structure of catena-{[bis(benzo-15-crown-5)ammonium][silver(I)-tetrakis(m-sulfido)tungstate(VI)], [(C14H20O5)2(NH4)][AgWS4]
Authors of publication	Yuan Cao; Guosheng Cheng; Guozhu Shen
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2012
Journal volume	227
Journal issue	1
Pages of publication	50
a	12.915 ± 0.003 Å
b	11.515 ± 0.002 Å
c	24.758 ± 0.005 Å
α	90°
β	92.12 ± 0.03°
γ	90°
Cell volume	3679.4 ± 1.3 Å³
Cell temperature	291 ± 2 K
Ambient diffraction temperature	291 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0742
Residual factor for significantly intense reflections	0.059
Weighted residual factors for significantly intense reflections	0.1518
Weighted residual factors for all reflections included in the refinement	0.1642
Goodness-of-fit parameter for all reflections included in the refinement	0.983
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176728 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 8.	8103296.cif
52261	2012-04-09	../uploads/cif-deposit/cod/cif Adding structures of 8103296 via cif-deposit CGI script.	8103296.cif