Crystallography Open Database

Information card for entry 8104690

Preview

Coordinates	8104690.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Bis(2-<i>tert</i>-butyl-3-phenyl-1-trimethylsilyl-1-azaallyl-κ^2^<i>N</i>,\\ N')Zinc(II)
Formula	C30 H48 N2 Si2 Zn
Calculated formula	C30 H48 N2 Si2 Zn
Title of publication	Crystal structure of bis(3,3-dimethyl-1-phenylbut-1-en-2-yl)(trimethylsilyl)amido-k1 N)zinc(II), Zn(C15H24NSi)2
Authors of publication	Wang, Jun-Hong; Tong, Hong-Bo; Wang, Meng-Liang; Yuan, Hai-Yan
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2021
Journal volume	236
Journal issue	4
Pages of publication	719 - 720
a	8.828 ± 0.003 Å
b	9.458 ± 0.003 Å
c	10.786 ± 0.003 Å
α	74.609 ± 0.004°
β	73.915 ± 0.004°
γ	64.888 ± 0.004°
Cell volume	772.1 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0588
Residual factor for significantly intense reflections	0.0476
Weighted residual factors for significantly intense reflections	0.1166
Weighted residual factors for all reflections included in the refinement	0.1225
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
273533 (current)	2022-03-08	cif/ Adding structures of 8104690 via cif-deposit CGI script.	8104690.cif