Crystallography Open Database

Information card for entry 8105015

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Coordinates	8105015.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	tetra-(1,10-phenanthroline-N,N') octa-(azido-N) tetra-zinc(II)
Formula	C48 H32 N32 Zn4
Calculated formula	C48 H32 N32 Zn4
Title of publication	Crystal structure of hexakis(μ2-azido-κ2N:N)-diazido-κ1N-tetrakis(phenanthroline-κ2N,N′)tetrazinc(II), C48H32N32Zn4
Authors of publication	Feng, Yu-Quan; Zhong, Zhi-Guo; Yue, Zi-Long
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2019
Journal volume	235
Journal issue	1
Pages of publication	57 - 58
a	9.9928 ± 0.0014 Å
b	10.1374 ± 0.0014 Å
c	14.2362 ± 0.0019 Å
α	71.71 ± 0.002°
β	76.166 ± 0.002°
γ	71.086 ± 0.002°
Cell volume	1280.1 ± 0.3 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296.15 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0466
Residual factor for significantly intense reflections	0.0314
Weighted residual factors for significantly intense reflections	0.073
Weighted residual factors for all reflections included in the refinement	0.0795
Goodness-of-fit parameter for all reflections included in the refinement	1.0249
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
274317 (current)	2022-04-04	cif/ Adding structures of 8105015 via cif-deposit CGI script.	8105015.cif