Crystallography Open Database

Information card for entry 8105663

Preview

Coordinates	8105663.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H39 N O Si
Calculated formula	C34 H39 N O Si
Title of publication	Crystal structure of 2-(bis(3,5-dimethylphenyl) ((methyldiphenylsilyl)oxy)methyl) pyrrolidine, C34H39NOSi
Authors of publication	Govender, Kimberleigh B.; Samipillai, Marivel; Govender, Thavendran; Kruger, Hendrik G.; Naicker, Tricia
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2019
Journal volume	234
Journal issue	3
Pages of publication	413 - 415
a	10.0901 ± 0.0002 Å
b	11.5016 ± 0.0002 Å
c	14.4098 ± 0.0003 Å
α	69.207 ± 0.001°
β	86.555 ± 0.002°
γ	65.579 ± 0.003°
Cell volume	1416.1 ± 0.06 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100.03 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0503
Residual factor for significantly intense reflections	0.0463
Weighted residual factors for significantly intense reflections	0.1176
Weighted residual factors for all reflections included in the refinement	0.12
Goodness-of-fit parameter for all reflections included in the refinement	1.107
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
276734 (current)	2022-07-08	cif/ Adding structures of 8105663 via cif-deposit CGI script.	8105663.cif