Crystallography Open Database

Information card for entry 8106379

Preview

Coordinates	8106379.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H30 Cu Ge N8 O41 W12
Calculated formula	C30 H30 Cu Ge N8 O41 W12
Title of publication	Crystal structure of catena-poly[bis(4,4′-dipyridylaminium-kN)-(μ2-germanowolframato-κ2 O:O′)-(2,2′-bipyridine-κ2 N,N′)copper(II)] with a Keggin-type heteropolyoxoanion, [Cu(C10H8N2)(C10H10N3)2][GeW12O40] ⋅ H2O
Authors of publication	Wu, Li-Zhou
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2018
Journal volume	233
Journal issue	6
Pages of publication	1007 - 1010
a	12.095 ± 0.002 Å
b	13.488 ± 0.003 Å
c	19.22 ± 0.004 Å
α	90.221 ± 0.003°
β	92.188 ± 0.003°
γ	108.966 ± 0.003°
Cell volume	2962.7 ± 1 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296.15 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0822
Residual factor for significantly intense reflections	0.0624
Weighted residual factors for significantly intense reflections	0.1497
Weighted residual factors for all reflections included in the refinement	0.1622
Goodness-of-fit parameter for all reflections included in the refinement	0.988
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
279854 (current)	2022-12-13	cif/ Adding structures of 8106379 via cif-deposit CGI script.	8106379.cif