Crystallography Open Database

Information card for entry 8106439

Preview

Coordinates	8106439.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H64 Ag2 B20 Cl4 N2 O6 P4
Calculated formula	C54 H64 Ag2 B20 Cl4 N2 O6 P4
Title of publication	Crystal structure of bis(μ-nitrato-κ2 O:O)-bis[1,2-bis(diphenylphosphino)-1,2-dicarba-closo-dodecaborane-κ2 P,P′]disilver(I) dicloromethane monosolvate, C54H64B20Cl4O6P4Ag2
Authors of publication	Yanfei, Wang; Xin, Wang; Qianqian, Gao; Liguo, Yang
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2017
Journal volume	232
Journal issue	1
Pages of publication	81 - 83
a	10.12 ± 0.001 Å
b	11.9101 ± 0.0011 Å
c	14.4999 ± 0.0015 Å
α	86.432 ± 0.002°
β	80.67 ± 0.001°
γ	84.031 ± 0.002°
Cell volume	1713.4 ± 0.3 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0738
Residual factor for significantly intense reflections	0.0535
Weighted residual factors for significantly intense reflections	0.14
Weighted residual factors for all reflections included in the refinement	0.1544
Goodness-of-fit parameter for all reflections included in the refinement	0.981
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
280276 (current)	2023-01-11	cif/ Adding structures of 8106439 via cif-deposit CGI script.	8106439.cif