Crystallography Open Database

Information card for entry 8106755

Preview

Coordinates	8106755.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	tris(μ2-1,3-bis(4,4,4-Trifluoro-3-oxido-1-(oxo)but-2-en-1-yl)phenyl)- bis(1,2-dimethoxyethane-O,O')-di-Lutetium(iii)
Formula	C50 H38 F18 Lu2 O16
Calculated formula	C50 H38 F18 Lu2 O16
Title of publication	The crystal structure of tris(μ2-1,3-bis(4,4,4-trifluoro-3-oxido-1-(oxo)but-2-en-1-yl)phenyl-κ4 O,O′:O′′,O′′′)-bis(1,2-dimethoxyethane-κ2 O,O′)dilutetium(III), C50H38F18Lu2O16
Authors of publication	Zhao, WeiCan; Shi, Jing; Hou, YanJun
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2017
Journal volume	232
Journal issue	6
Pages of publication	1021 - 1022
a	15.7024 ± 0.0012 Å
b	12.6169 ± 0.001 Å
c	29.715 ± 0.002 Å
α	90°
β	91.919 ± 0.001°
γ	90°
Cell volume	5883.7 ± 0.8 Å³
Cell temperature	273 ± 2 K
Ambient diffraction temperature	273 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0327
Residual factor for significantly intense reflections	0.0273
Weighted residual factors for significantly intense reflections	0.0633
Weighted residual factors for all reflections included in the refinement	0.066
Goodness-of-fit parameter for all reflections included in the refinement	0.959
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
280859 (current)	2023-02-13	cif/ Adding structures of 8106755 via cif-deposit CGI script.	8106755.cif