Crystallography Open Database

Information card for entry 8107017

Preview

Coordinates	8107017.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H33 F N2 O7
Calculated formula	C24 H33 F N2 O7
Title of publication	Crystal structure of 2-ethyl-1-tert-butyl-2-((4-fluorophenyl)(tert-butoxycarbonylamino)methyl)-3-oxo-pyrrolidine-1,2-dicarboxylate, C24H33FN2O7
Authors of publication	Makhathini, Sifiso S.; Samipillai, Marivel; Govender, Thavendran; Naicker, Tricia
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2016
Journal volume	231
Journal issue	3
Pages of publication	819 - 821
a	11.0118 ± 0.0007 Å
b	11.5684 ± 0.0007 Å
c	11.7276 ± 0.0007 Å
α	112.294 ± 0.001°
β	100.557 ± 0.001°
γ	105.775 ± 0.002°
Cell volume	1259.57 ± 0.14 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0586
Residual factor for significantly intense reflections	0.0411
Weighted residual factors for significantly intense reflections	0.0956
Weighted residual factors for all reflections included in the refinement	0.105
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
282371 (current)	2023-04-05	cif/ Adding structures of 8107017 via cif-deposit CGI script.	8107017.cif