#------------------------------------------------------------------------------ #$Date: 2023-04-19 12:26:39 +0300 (Wed, 19 Apr 2023) $ #$Revision: 282739 $ #$URL: file:///home/coder/svn-repositories/cod/cif/8/10/70/8107093.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_8107093 loop_ _publ_author_name 'Zhao, Li' 'Zhao, Ji-Xing' 'An, Qin-Qin' 'Wang, Fei' _publ_section_title ; Crystal structure of (E)-1-(4-(((E)-3,5-dibromo-2-hydroxybenzylidene)amino)phenyl)ethan-1-one O-methyl oxime, C17H16Br2N2O2 ; _journal_issue 4 _journal_name_full 'Zeitschrift f\"ur Kristallographie - New Crystal Structures' _journal_page_first 1053 _journal_page_last 1054 _journal_paper_doi 10.1515/ncrs-2016-0047 _journal_volume 231 _journal_year 2016 _chemical_formula_sum 'C17 H16 Br2 N2 O2' _chemical_formula_weight 440.14 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _cell_angle_alpha 90 _cell_angle_beta 105.261(15) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.2648(14) _cell_length_b 13.3034(16) _cell_length_c 14.510(2) _cell_measurement_temperature 293(2) _cell_measurement_theta_max 70.5390 _cell_measurement_theta_min 5.9630 _cell_volume 1725.3(4) _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET) (compiled Feb 1 2013,16:14:44) ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET) (compiled Feb 1 2013,16:14:44) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET) (compiled Feb 1 2013,16:14:44) ; _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution ; Superflip (Palatinus & Chapuis, 2007;Palatinus & van der Lee, 2008; Palatinus et al., 2012) ; _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.977 _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Eos' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0506 _diffrn_reflns_av_unetI/netI 0.0598 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.977 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 6435 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.977 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 70.849 _diffrn_reflns_theta_min 4.585 _exptl_absorpt_coefficient_mu 6.049 _exptl_crystal_colour 'clear light yellow' _exptl_crystal_density_diffrn 1.694 _exptl_crystal_description needle _exptl_crystal_F_000 872 _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.07 _refine_diff_density_max 0.802 _refine_diff_density_min -1.048 _refine_diff_density_rms 0.148 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.605 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 211 _refine_ls_number_reflns 3259 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.605 _refine_ls_R_factor_all 0.0788 _refine_ls_R_factor_gt 0.0679 _refine_ls_shift/su_max 0.139 _refine_ls_shift/su_mean 0.003 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0300P)^2^+0.5000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1564 _refine_ls_wR_factor_ref 0.1657 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 2587 _reflns_number_total 3259 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file suppl_ncrs-2016-0047_suppl.cif _cod_data_source_block C17H17Br2N2O2 _cod_original_cell_volume 1725.4(4) _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 8107093 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; C17H17Br2N2O2.res created by SHELXL-2014/7 TITL D418 in P2(1)/c CELL 1.54184 9.264792 13.303367 14.510257 90 105.2607 90 ZERR 4 0.00138 0.001571 0.002265 0 0.0147 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Br N O UNIT 68 64 8 8 8 LIST 6 ! automatically inserted. Change 6 to 4 for CHECKCIF!! L.S. 10 PLAN 20 MORE -1 BOND $H HTAB CONF fmap 2 53 ACTA SHEL 999 0.81 REM D:/olex2_D418/D418.hkl WGHT 0.030000 0.500000 FVAR 3.68457 BR1 3 -0.331476 0.219906 0.184873 11.00000 0.05762 0.04896 = 0.06085 0.00413 0.00009 0.01053 BR2 3 -0.324951 -0.181116 0.057597 11.00000 0.06917 0.05977 = 0.06083 -0.01652 0.00241 -0.02226 O1 5 -0.057758 0.151123 0.330972 11.00000 0.05940 0.04766 = 0.04968 -0.01133 -0.01098 0.00760 AFIX 147 H1 2 0.002349 0.129110 0.378696 11.00000 -1.50000 AFIX 0 O2 5 0.770498 0.053815 0.887941 11.00000 0.05774 0.06079 = 0.04941 -0.00315 -0.01451 -0.00294 N1 4 0.132243 0.024418 0.425436 11.00000 0.04760 0.04550 = 0.03957 -0.00135 -0.00219 0.00240 N2 4 0.646460 0.063625 0.809197 11.00000 0.05328 0.05570 = 0.04492 0.00264 -0.00601 -0.00804 C1 1 -0.113472 0.075590 0.272344 11.00000 0.04264 0.03857 = 0.03817 -0.00216 0.00417 -0.00446 C2 1 -0.241208 0.090254 0.197752 11.00000 0.04152 0.04377 = 0.03987 0.00390 0.00292 -0.00222 C3 1 -0.304671 0.015045 0.135512 11.00000 0.03469 0.05621 = 0.04112 0.00633 0.00193 -0.00907 AFIX 43 H3 2 -0.391901 0.026459 0.087518 11.00000 -1.20000 AFIX 0 C4 1 -0.236012 -0.078123 0.145748 11.00000 0.04615 0.04297 = 0.04373 -0.00696 0.00600 -0.00924 C5 1 -0.111106 -0.097378 0.218534 11.00000 0.05046 0.03722 = 0.04883 0.00141 0.00685 -0.00117 AFIX 43 H5 2 -0.068034 -0.161010 0.225048 11.00000 -1.20000 AFIX 0 C6 1 -0.048841 -0.021458 0.282703 11.00000 0.04615 0.04073 = 0.04243 0.00097 0.00087 -0.00382 C7 1 0.078526 -0.042901 0.362932 11.00000 0.04572 0.04034 = 0.04973 0.00241 0.00406 0.00355 AFIX 43 H7 2 0.121680 -0.106499 0.368966 11.00000 -1.20000 AFIX 0 C8 1 0.252800 0.007301 0.506474 11.00000 0.04162 0.04280 = 0.03737 0.00122 0.00150 -0.00069 C9 1 0.339315 -0.078730 0.524246 11.00000 0.06049 0.05951 = 0.04860 -0.01408 -0.00629 0.01576 AFIX 43 H9 2 0.318402 -0.131686 0.480924 11.00000 -1.20000 AFIX 0 C10 1 0.457233 -0.087093 0.606091 11.00000 0.05543 0.05383 = 0.04929 -0.00675 -0.00993 0.01209 AFIX 43 H10 2 0.513786 -0.145760 0.616712 11.00000 -1.20000 AFIX 0 C11 1 0.492059 -0.009778 0.672057 11.00000 0.04017 0.04531 = 0.04000 0.00469 0.00332 -0.00248 C12 1 0.401180 0.076087 0.654706 11.00000 0.04629 0.03906 = 0.04139 -0.00270 0.00325 -0.00357 AFIX 43 H12 2 0.419574 0.128093 0.699101 11.00000 -1.20000 AFIX 0 C13 1 0.285453 0.084963 0.573415 11.00000 0.04472 0.03908 = 0.04860 -0.00146 0.00190 -0.00295 AFIX 43 H13 2 0.228280 0.143362 0.562902 11.00000 -1.20000 AFIX 0 C14 1 0.620009 -0.017665 0.757842 11.00000 0.04191 0.05072 = 0.04013 0.00607 0.00233 -0.00674 C15 1 0.712437 -0.110496 0.781169 11.00000 0.05062 0.06488 = 0.06209 -0.00078 -0.00829 0.00611 AFIX 137 H15A 2 0.803714 -0.095303 0.828475 11.00000 -1.50000 H15B 2 0.735305 -0.135286 0.724496 11.00000 -1.50000 H15C 2 0.657838 -0.160706 0.805564 11.00000 -1.50000 AFIX 0 C16 1 0.792224 0.146768 0.937610 11.00000 0.07629 0.07011 = 0.04461 -0.00548 -0.00464 -0.01668 AFIX 23 H16A 2 0.711812 0.158140 0.967761 11.00000 -1.20000 H16B 2 0.792185 0.201432 0.893364 11.00000 -1.20000 AFIX 0 C17 1 0.939768 0.143076 1.012065 11.00000 0.04703 0.10196 = 0.05518 -0.01412 -0.00095 -0.01598 AFIX 137 H17A 2 1.019670 0.141200 0.981315 11.00000 -1.50000 H17B 2 0.943730 0.083954 1.050587 11.00000 -1.50000 H17C 2 0.950107 0.201716 1.051831 11.00000 -1.50000 AFIX 0 HKLF 4 REM D418 in P2(1)/c REM R1 = 0.0679 for 2587 Fo > 4sig(Fo) and 0.0788 for all 3259 data REM 211 parameters refined using 0 restraints END WGHT 0.1327 0.6741 REM Instructions for potential hydrogen bonds HTAB O1 N1 EQIV $1 -x, y-1/2, -z+1/2 HTAB C9 Br1_$1 EQIV $2 x+1, -y+1/2, z+1/2 HTAB C16 Br1_$2 EQIV $3 -x+1, -y, -z+1 HTAB C17 Br2_$3 REM Highest difference peak 0.802, deepest hole -1.048, 1-sigma level 0.148 Q1 1 -0.5149 0.2616 0.0652 11.00000 0.05 0.80 Q2 1 -0.4904 0.1335 0.0631 11.00000 0.05 0.69 Q3 1 -0.1728 -0.1058 0.1630 11.00000 0.05 0.65 Q4 1 0.6698 -0.1957 0.9180 11.00000 0.05 0.65 Q5 1 -0.4452 -0.1796 0.0828 11.00000 0.05 0.64 Q6 1 -0.1660 -0.2526 0.1663 11.00000 0.05 0.64 Q7 1 -0.4789 0.2264 0.2040 11.00000 0.05 0.62 Q8 1 -0.1691 0.2175 0.1627 11.00000 0.05 0.61 Q9 1 -0.2781 0.2242 0.2465 11.00000 0.05 0.59 Q10 1 0.8215 0.2054 0.7877 11.00000 0.05 0.59 Q11 1 -0.3979 0.2398 0.1139 11.00000 0.05 0.58 Q12 1 0.6657 0.2055 1.0447 11.00000 0.05 0.56 Q13 1 -0.2641 -0.1898 0.1234 11.00000 0.05 0.55 Q14 1 -0.3996 -0.1554 -0.0184 11.00000 0.05 0.55 Q15 1 0.6779 0.2847 0.8279 11.00000 0.05 0.53 Q16 1 1.1229 0.1832 0.9558 11.00000 0.05 0.52 Q17 1 -0.1935 -0.1777 0.0346 11.00000 0.05 0.51 Q18 1 0.5313 0.1759 0.9210 11.00000 0.05 0.50 Q19 1 0.4792 -0.1282 0.7682 11.00000 0.05 0.49 Q20 1 -0.4587 0.0982 0.1836 11.00000 0.05 0.49 ; _shelx_res_checksum 87241 _shelx_hkl_file ; 0 0 -2 38835.6 1176.05 3 0 0 -3 49.9339 33.5839 3 0 0 3 60.4037 40.6839 2 0 0 -4 26.9535 33.2347 3 0 0 4 76.8688 54.2976 2 0 0 5 37.5813 57.8088 6 0 0 -5 176.406 65.5347 3 0 0 5 65.1812 64.0126 2 0 0 6 18215.2 1084.17 6 0 0 7 169.608 143.679 5 0 0 8 244150. 7741.06 5 0 0 9 49.1063 124.877 5 0 0 10 1377.60 349.994 5 0 0 11 121.518 84.2118 5 0 0 12 188.100 219.343 8 0 0 12-119.713 118.745 5 0 0 13 197.281 154.276 8 0 0 14 299.566 208.204 8 0 0 15 134.657 156.041 8 0 0 16 7958.69 823.369 8 0 0 16 10200.4 991.740 9 0 -1 0 188.720 36.1950 1 0 -1 1 2751.71 177.255 1 0 -1 2 10341.4 471.898 2 0 -1 3 8335.62 478.489 2 0 1 3 7809.97 356.454 3 0 -1 4 495979. 13701.6 6 0 -1 4 480086. 13671.2 2 0 1 -4 501215. 13641.7 1 0 1 -4 488819. 13554.7 3 0 1 4 514740. 13375.7 3 0 1 5 1946.36 295.216 2 0 -1 5 2051.61 294.141 2 0 1 -5 2054.79 241.709 3 0 1 5 2375.31 311.995 6 0 1 -5 2214.07 278.981 1 0 1 5 1559.34 222.695 7 0 1 6 506.315 161.359 6 0 -1 7 21377.4 1319.65 5 0 1 7 23152.1 1368.64 6 0 1 7 25537.5 1467.44 5 0 1 8 422.879 229.133 5 0 -1 8 528.354 227.556 5 0 1 9 2441.59 476.988 5 0 -1 9 1848.36 411.256 5 0 1 10 3870.00 618.291 5 0 -1 10 2630.39 505.817 5 0 1 11 3532.71 628.328 5 0 -1 11 3135.76 560.594 5 0 1 12 42443.9 2453.63 5 0 -1 12 44253.0 2795.68 8 0 1 12 49438.2 2951.39 8 0 -1 13 7662.60 1063.81 8 0 1 13 8185.61 1114.94 8 0 -1 14 580.237 277.311 8 0 1 14 755.285 289.502 8 0 1 15 1774.33 443.985 8 0 1 15 2144.69 524.726 9 0 -1 15 1436.71 375.203 8 0 -1 16 788.181 258.690 9 0 1 16 930.326 286.691 9 0 1 16 695.908 253.508 8 0 1 17 147.768 104.800 9 0 -2 0 38429.1 1219.80 1 0 -2 1 3337.42 235.746 1 0 2 -2 11305.6 507.494 2 0 2 -3 256062. 7148.62 2 0 2 4 3673.69 261.114 3 0 -2 4 3612.96 352.226 2 0 2 -4 3879.43 365.782 1 0 2 4 3666.21 358.553 7 0 2 4 3786.49 374.226 6 0 -2 5 55947.7 2190.91 2 0 -2 5 61594.8 2233.33 5 0 2 -5 53580.0 2028.86 3 0 2 5 58189.7 2145.32 7 0 2 6 12032.5 839.082 6 0 -2 6 10471.7 775.823 5 0 2 7 24.0894 122.590 5 0 2 7-63.7214 138.898 6 0 -2 7 38.1979 74.4264 5 0 -2 8 183765. 6523.35 5 0 2 8 235363. 6948.99 5 0 2 9 2651.83 527.703 5 0 -2 9 1778.64 373.010 5 0 -2 10 277.698 161.226 5 0 2 10 264.075 117.280 5 0 2 11 14948.8 1355.45 5 0 2 12-148.760 144.291 5 0 2 12-125.906 220.044 8 0 2 13 25916.5 2068.94 8 0 2 14 6294.76 940.835 8 0 2 15 60.7595 149.562 9 0 -2 15 375.732 210.217 9 0 2 15 319.683 184.725 8 0 2 16 5198.66 692.883 9 0 2 16 4455.59 622.534 8 0 -3 0 184.154 65.8073 1 0 -3 1 435484. 11824.0 1 0 3 -2 82542.4 2432.98 2 0 -3 2 78068.9 2534.71 1 0 3 3 26443.0 1225.26 7 0 3 -3 25931.7 1017.19 2 0 3 4 141006. 4312.68 7 0 3 4 129797. 4171.65 6 0 3 5 48442.6 1977.01 7 0 3 5 50741.8 1995.20 6 0 3 6 8601.75 706.406 7 0 3 6 10313.4 848.174 5 0 3 6 10765.3 818.424 6 0 3 7 109798. 4182.93 5 0 3 7 119757. 4171.39 6 0 3 8 217.824 144.435 5 0 3 8-1.17545 116.575 6 0 3 9 57429.3 2806.10 5 0 3 10 2314.49 505.653 5 0 3 11-26.4174 149.059 5 0 3 12 27715.2 2170.73 8 0 3 13-116.141 230.677 8 0 3 14 11.9304 172.498 8 0 3 15 4304.49 703.729 8 0 3 15 4234.22 699.147 9 0 3 16 1419.62 343.964 8 0 3 16 1198.72 308.278 9 0 -4 0 6176.95 439.662 1 0 4 0 4037.75 466.485 7 0 4 -1 49670.8 2121.37 7 0 -4 1 62944.1 2023.18 1 0 -4 -1 64559.5 1996.18 1 0 4 1 51772.0 2231.76 7 0 4 -2 45757.5 1547.29 2 0 -4 2 46532.2 1708.01 1 0 4 2 46343.4 1900.23 7 0 4 -2 43914.0 1722.72 1 0 4 3 101262. 3387.88 6 0 4 -3 104521. 3272.62 2 0 4 4 7150.61 639.995 7 0 4 4 6009.97 524.861 6 0 4 5 379599. 10751.2 7 0 4 5 351896. 10714.0 5 0 4 5 377137. 10638.2 6 0 4 6 17304.9 1176.17 5 0 4 6 16146.4 1091.10 7 0 4 6 18932.8 1163.77 6 0 4 7 4237.76 526.422 7 0 4 7 4960.08 645.758 5 0 4 7 5285.79 634.269 6 0 4 8 4091.68 628.788 5 0 4 8 4480.21 628.620 6 0 4 9 5789.58 771.745 5 0 4 10 8505.44 983.532 5 0 4 11 9394.50 1200.51 8 0 -4 11 8812.05 1065.19 11 0 4 11 9984.12 1090.46 5 0 4 12 3548.80 712.643 8 0 -4 12 2881.60 592.842 11 0 4 13 13590.5 1455.46 8 0 4 14 854.851 321.620 8 0 4 14 890.547 339.796 9 0 4 15 92.4044 76.2210 8 0 4 15 66.1550 132.382 9 0 4 16 2496.21 427.561 9 0 4 16 2594.08 444.194 8 0 5 0 76.7956 69.2671 7 0 -5 0 21.8784 33.5461 1 0 -5 1 116580. 3681.18 1 0 -5 -1 126654. 3699.12 1 0 5 1 119786. 4092.36 7 0 -5 -2 63732.4 2160.09 1 0 5 -2 56785.5 2396.32 7 0 5 -2 57133.4 1996.36 2 0 5 3 2035.21 282.236 6 0 5 -3 2080.02 337.408 7 0 5 3 2267.76 297.902 5 0 5 4 3978.19 440.251 6 0 5 4 3975.83 448.571 5 0 5 4 4876.68 583.717 7 0 5 5 3953.42 475.509 6 0 5 5 4003.56 497.482 5 0 5 5 4710.55 577.517 7 0 5 6 47654.3 2146.31 6 0 5 6 46884.3 2184.03 7 0 5 6 43016.9 2119.22 5 0 5 7 19767.9 1339.32 7 0 5 7 21455.4 1459.05 5 0 5 8 14637.6 1213.69 5 0 5 9 48992.1 2545.73 5 0 5 10 12694.6 1226.03 5 0 5 11 9.82599 53.9751 5 0 -5 11 80.4654 103.655 11 0 -5 12 1507.60 431.878 11 0 5 12 1645.54 475.709 8 0 5 13 2466.02 604.757 8 0 5 13 2230.13 568.663 9 0 -5 13 1914.02 462.953 11 0 5 14 5669.27 851.300 9 0 5 14 5647.58 851.452 8 0 -5 14 4163.64 614.924 11 0 5 15 249.303 133.298 9 0 5 15 42.3882 80.5694 8 0 5 16 363.931 152.830 9 0 6 0 2723.45 475.435 7 0 6 1 9562.04 866.076 7 0 6 -1 6612.58 745.138 7 0 6 -2 93616.1 3964.98 7 0 6 2 137250. 4265.04 7 0 6 -3 31137.6 1797.72 7 0 6 3 51642.8 2205.35 7 0 6 4 10498.7 952.676 7 0 6 5 11822.6 1011.16 7 0 6 5 8998.97 777.480 6 0 6 6 15908.7 1140.85 6 0 6 6 18540.4 1296.09 7 0 6 7 17586.2 1314.15 7 0 6 7 15329.1 1200.27 5 0 6 8 3411.57 557.569 5 0 6 8 2338.13 456.972 7 0 6 9 7858.56 924.239 5 0 6 10 22013.9 1913.89 8 0 6 10 23308.2 1710.10 5 0 -6 10 25042.2 1926.76 11 0 6 11-69.5589 124.736 8 0 -6 11 445.721 266.498 11 0 6 12 73.6522 141.119 9 0 -6 12 12.3711 132.662 11 0 6 12 164.843 166.121 8 0 6 13 7151.89 1002.31 8 0 -6 13 7348.59 907.194 11 0 6 13 6619.79 937.692 9 0 6 14 554.840 221.074 9 0 6 14 516.662 228.767 8 0 -6 14 421.994 190.076 11 0 6 15 739.063 233.624 9 0 -6 15 842.584 214.968 11 0 7 0 23.3226 129.224 7 0 7 1 19648.5 1370.21 7 0 7 -1 14902.9 1262.26 7 0 7 2 77393.1 3052.25 7 0 7 -2 52103.7 2741.82 7 0 7 3 173738. 6071.47 7 0 7 4 46727.0 2428.88 7 0 7 5 67081.8 3053.57 7 0 7 6 62670.0 2950.13 7 0 7 7 6155.29 793.398 7 0 7 8 447.643 231.533 7 0 7 9 6728.35 1009.68 8 0 7 9 9113.28 1054.51 21 0 -7 9 8196.17 1052.46 11 0 7 10 17040.7 1490.84 21 0 7 10 16860.6 1645.10 8 0 -7 10 19291.1 1666.90 11 0 7 11 24206.2 2037.15 8 0 -7 11 28976.0 2066.88 11 0 -7 12 872.482 352.226 11 0 7 12 1063.33 411.030 8 0 7 13 3093.65 613.187 8 0 -7 13 3400.84 600.801 11 0 -7 14 5079.91 641.329 11 0 -7 15 558.641 164.054 11 0 8 0 44773.3 2402.42 7 0 8 -1 42785.0 2424.27 7 0 8 1 52244.6 2608.55 7 0 8 2 31373.9 1937.14 7 0 8 -2 21524.3 1596.47 7 0 8 3 2611.65 547.725 7 0 8 4 6154.07 823.348 7 0 8 5 460.986 220.962 7 0 8 6 12803.5 1220.84 7 0 8 7 34506.1 2143.32 7 0 -8 8 12029.7 1302.93 11 0 8 8 10959.5 1122.92 7 0 8 8 13067.0 1310.36 21 0 8 9 7610.75 988.599 21 0 -8 9 6726.91 973.232 11 0 -8 10 8644.88 1081.13 11 0 8 10 5914.03 947.370 8 0 8 10 7555.28 966.140 21 0 8 11 7367.79 898.818 21 0 -8 11 9050.98 1096.38 11 0 -8 12 812.955 300.709 11 0 -8 13-39.4893 105.607 11 0 -8 14 43.3780 46.3314 11 0 9 0 50.3472 157.184 7 0 9 -1 5930.15 836.399 7 0 9 1 6937.66 917.831 7 0 9 2 5726.33 847.290 7 0 9 -2 4438.44 703.004 7 0 9 3 108219. 4603.93 7 0 9 4 15533.5 1439.93 7 0 9 5 40249.0 2427.80 7 0 9 6 4106.84 692.014 7 0 9 7 108.450 100.312 7 0 9 7-227.576 178.380 21 0 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2049.28 489.367 5 -4 1 9 1151.54 351.092 5 -4 -1 8 2157.66 459.768 5 -4 1 8 1875.23 459.708 5 -4 1 7 1152.04 322.570 5 -4 -1 7 997.935 305.240 5 -4 -1 6 276497. 8611.23 5 -4 1 6 277155. 8631.01 5 -4 -1 5 96990.7 3608.16 5 -4 1 5 96674.0 3582.62 5 -4 -1 4 17612.2 1128.43 5 -4 1 4 17339.7 1115.46 5 -4 -1 3 28135.5 1449.42 5 -4 1 3 28530.5 1457.76 5 4 1 -2 177572. 5383.95 6 4 -1 -2 165863. 5280.64 6 4 1 -1 12666.6 845.496 6 4 -1 -1 12053.5 785.679 6 4 -1 0 3770.65 433.561 6 4 1 0 3876.47 470.402 6 4 -1 1 16581.7 1083.50 6 4 1 1 19417.9 1212.75 6 4 1 2 66291.2 2755.69 6 4 -1 2 59396.3 2609.49 6 4 -1 3 5056.97 596.620 6 4 1 3 5233.89 656.832 6 4 -1 4 23194.5 1393.87 6 4 1 4 24281.0 1529.80 6 4 -1 5 854.994 234.894 6 4 1 5 598.562 218.088 6 4 1 6 67056.6 2853.31 6 4 1 7 11739.5 1008.61 6 4 1 8 779.455 247.401 6 4 -1 9 196.620 81.2754 11 4 1 9 333.700 171.898 10 4 1 9 456.784 200.920 6 4 -1 10 9305.48 1045.63 11 4 1 10 9435.91 1019.89 10 4 -1 11 3824.79 614.635 11 4 1 11 3333.32 565.473 10 4 1 12 14610.6 1353.77 8 4 1 13 155.538 155.277 8 4 -1 13 219.012 152.663 8 4 1 14 3393.24 454.636 8 4 -1 14 3698.54 477.920 8 -4 2 17 707.481 238.339 9 -4 2 16 84.6311 131.621 9 -4 2 15 117.906 117.775 9 -4 2 14 5753.21 978.795 9 -4 2 13 2614.74 662.472 9 -4 2 12-63.2851 109.865 5 -4 2 12 307.555 231.506 9 -4 -2 11 13766.6 1401.56 5 -4 2 11 9860.38 1232.33 5 -4 2 10 5847.17 871.470 5 -4 -2 10 6534.43 927.705 5 -4 2 9 8252.09 990.058 5 -4 -2 9 8153.93 980.174 5 -4 -2 8 8893.94 974.215 5 -4 2 8 9268.56 1015.90 5 -4 -2 7 23735.4 1583.74 5 -4 2 7 25721.3 1643.77 5 -4 -2 6 311626. 9733.98 5 -4 2 6 329540. 9849.11 5 -4 -2 5 5469.57 615.670 5 -4 2 5 5630.63 635.698 5 -4 -2 4 10231.8 839.135 5 -4 2 4 10685.2 860.822 5 -4 2 3 14126.4 971.256 5 4 2 -2 49278.1 1997.66 6 4 -2 -2 43701.9 1845.61 6 4 -2 -1 18400.2 1034.65 6 4 2 -1 23901.0 1255.71 6 4 -2 0 20389.8 1148.12 6 4 2 0 25397.9 1363.98 6 4 2 1 46303.9 2169.67 6 4 2 2 44601.2 2223.49 6 4 2 3 3553.52 573.510 6 4 2 4 290.069 174.183 6 4 2 5 1156.97 278.544 6 4 2 6 32856.5 1815.77 6 4 2 7 2741.85 483.943 6 4 2 8 2962.13 567.786 10 4 -2 8 3008.80 596.860 11 4 2 8 2425.53 458.243 6 4 -2 9 11148.9 1191.80 11 4 2 9 11626.1 1152.77 10 4 -2 10 30445.3 2038.79 11 4 2 10 31649.2 1983.02 10 4 -2 11 10107.1 1049.53 11 4 2 11 9893.61 1017.61 10 4 2 11 11846.0 1264.03 8 4 2 12 688.940 274.041 8 4 -2 12 504.516 207.884 11 4 2 13-8.01107 78.4911 8 4 -2 13 105.542 64.0381 8 4 2 14 201.611 87.7427 8 4 -2 14 378.762 146.375 8 -4 3 17-31.0545 62.2280 9 -4 3 16 249.986 181.838 9 -4 3 15 2859.01 642.419 9 -4 3 14 1210.82 425.876 9 -4 3 13 1648.77 551.077 9 -4 3 12 395.828 265.348 9 -4 3 11 7826.20 1150.23 9 -4 3 11 6979.62 1005.27 5 -4 3 10 23268.3 1848.45 5 -4 3 9 24586.7 1814.61 5 -4 3 8 693.685 251.051 5 -4 -3 8 709.241 261.727 5 -4 -3 7 38427.3 2130.45 5 -4 3 7 43900.6 2284.58 5 -4 -3 6 44048.9 2226.80 5 -4 3 6 50051.6 2383.03 5 -4 3 5 1989.57 393.359 5 -4 3 5 1728.57 397.600 4 -4 -3 5 1825.39 353.334 5 -4 3 4 19896.0 1244.64 5 -4 3 4 19353.9 1402.06 4 -4 3 3 25558.5 1405.29 5 -4 3 3 27755.3 1647.65 4 4 3 -3 25634.5 1429.24 6 -4 3 2 74394.1 3006.97 4 4 3 -2 65063.8 2659.13 6 4 3 -1 110552. 3929.08 6 4 3 0 15057.8 1092.38 6 4 3 1 9402.84 892.108 6 4 3 2 19975.0 1412.05 6 4 3 3 47936.0 2414.36 6 4 3 4 14704.1 1220.05 6 4 3 5 23937.8 1590.12 6 4 3 6 58003.8 2652.18 6 4 3 7 76188.7 3245.20 6 4 -3 8 18987.0 1605.84 11 4 3 8 16591.5 1293.04 6 4 -3 8 17632.6 1681.31 15 4 3 8 20574.4 1560.49 10 4 -3 9-53.4734 121.646 11 4 3 9-12.0671 94.2869 10 4 -3 10 6682.99 890.496 11 4 3 10 5770.31 794.277 10 4 3 10 6601.10 979.222 8 4 -3 11 5818.97 797.417 11 4 3 11 5216.46 716.589 10 4 3 11 6931.19 932.637 8 4 -3 12 918.984 264.176 11 4 3 12 1120.29 327.588 8 4 -3 13-58.3531 98.2837 11 4 3 13 48.4180 92.7043 8 4 -3 13 63.5845 44.8244 8 -4 4 17 514.386 186.292 9 -4 4 16 858.654 297.573 9 -4 4 15 324.880 227.532 9 -4 4 14 449.905 204.534 9 -4 4 13 3208.71 714.809 9 -4 4 12 2819.18 682.107 9 -4 4 11 2103.86 551.327 5 -4 4 11 2564.21 640.258 9 -4 4 11 3067.58 694.678 20 -4 4 10 3285.96 661.175 5 -4 4 9 35846.0 2285.99 5 -4 4 8 183.345 144.804 5 -4 4 7 2824.08 571.582 4 -4 4 7 3422.01 589.466 5 -4 4 6 617.003 263.051 4 -4 4 6 547.326 194.677 5 -4 4 5 125378. 4414.39 5 -4 4 5 114463. 4697.07 4 -4 4 4 84063.2 3256.85 5 -4 4 4 84786.7 3657.32 4 4 4 -4 86105.6 3342.04 6 -4 4 3 2275.50 378.511 5 -4 4 3 2231.72 472.300 4 4 4 -3 2750.30 432.755 6 -4 4 2 8325.78 881.432 4 4 4 -2 6946.85 708.605 6 -4 4 1 58839.3 2662.45 4 4 4 -1 54117.1 2458.48 6 4 4 0 3564.05 546.981 6 -4 4 0 3792.57 550.432 4 4 4 1 8647.83 891.125 6 4 4 2 57637.6 2774.16 6 4 4 3 102745. 4112.88 6 4 4 4 30780.6 1894.90 6 4 4 5 497.872 208.684 6 4 4 6 1658.73 415.878 6 4 4 7 47143.8 2385.24 6 4 -4 8 5044.57 790.633 11 4 4 8 5448.35 760.940 10 4 -4 8 4865.28 862.126 15 4 4 8 3898.41 590.577 6 4 -4 9 1027.74 348.871 11 4 4 9 1003.52 329.188 10 4 4 9 1097.99 374.197 8 4 -4 10 8219.19 999.466 11 4 4 10 8182.92 1053.17 8 4 4 10 7422.52 878.063 10 4 -4 11 17108.1 1381.93 11 4 4 11 17169.1 1325.53 10 4 4 11 15379.7 1392.87 8 4 -4 12 1116.98 308.368 11 4 4 12 1432.56 375.279 8 4 -4 13-67.9439 52.0718 11 4 4 13-82.7184 94.3709 8 4 -4 13 156.847 98.4814 8 -4 5 16 2694.14 483.856 9 -4 5 15 3555.58 645.156 9 -4 5 14-140.646 194.671 9 -4 5 13 2310.55 599.227 9 -4 5 12 788.777 349.311 20 -4 5 12 1125.49 435.053 9 -4 5 11-94.4172 127.142 5 -4 -5 11 48.4649 90.5511 11 -4 5 11 45.7204 140.596 20 -4 5 10 1519.55 455.615 5 -4 5 10 1572.00 508.454 20 -4 5 10 1894.26 551.034 9 -4 5 9 17002.4 1520.31 5 -4 5 8 35803.5 2323.33 4 -4 5 8 35934.7 2231.16 5 -4 5 7 31224.6 1960.45 5 -4 5 7 30461.1 2126.89 4 -4 5 6 4003.48 605.572 5 -4 5 6 3400.50 651.054 4 -4 5 5 48994.6 2324.46 5 -4 5 5 42392.4 2561.08 4 4 5 -5 49810.7 2391.02 6 -4 5 4 199.294 198.099 4 4 5 -4 38.9197 68.2423 6 -4 5 4 54.2925 116.686 5 -4 5 3 1374.90 397.802 4 4 5 -3 968.526 278.443 6 -4 5 2 13468.4 1216.90 4 4 5 -2 12600.0 1039.16 6 -4 5 1 216253. 7081.60 4 4 5 -1 199737. 6769.88 6 -4 5 0 63005.2 2872.77 4 4 5 0 60989.0 2849.60 6 4 5 1 30390.6 1912.85 6 -4 5 -1 31392.0 1787.29 4 4 5 2 5577.78 777.805 6 4 5 3 30590.5 1941.37 6 4 5 4 105.383 126.721 6 4 5 5 11646.2 1086.88 6 4 5 6 103.281 69.5164 6 4 -5 7 18368.0 1618.92 11 4 5 7 17854.6 1480.23 10 4 5 7 14618.3 1228.97 6 4 -5 7 16184.8 1600.38 15 4 -5 8 10938.5 1217.42 11 4 5 8 10994.2 1131.97 10 4 -5 8 8349.17 1134.84 15 4 -5 9 3322.44 633.602 11 4 5 9 4048.98 660.838 10 4 -5 10 3654.59 649.171 11 4 5 10 2302.83 466.984 10 4 5 10 2865.13 590.630 8 4 -5 11 3172.27 557.021 11 4 5 11 2927.71 508.763 10 4 5 11 2725.92 527.733 8 4 -5 12 1462.61 332.816 11 4 5 12 1369.58 333.450 8 4 -5 13 608.151 173.516 11 4 5 13 584.153 175.520 8 -4 6 16 107.144 95.6969 9 -4 6 15 151.262 139.181 9 -4 6 14 436.619 216.767 9 -4 6 13 3453.98 715.572 9 -4 6 13 4704.37 767.859 20 -4 -6 12 7787.48 1064.17 11 -4 6 12 8848.40 1206.89 9 -4 -6 11 1508.27 486.019 11 -4 6 11 3092.51 710.031 20 -4 6 11 2438.41 620.710 9 -4 6 10 495.617 259.449 5 -4 -6 10 118.072 72.0794 11 -4 6 10 582.675 318.348 20 -4 6 10 634.389 289.467 9 -4 6 9 1307.23 401.550 5 -4 6 8 135.046 173.043 4 -4 6 8 238.755 175.998 5 -4 6 7 375.916 212.004 4 -4 6 6 702.046 253.877 4 4 6 -6 958.875 298.042 6 -4 6 5 37471.6 2479.87 4 4 6 -5 43249.9 2214.15 6 -4 6 4 49260.5 2800.32 4 4 6 -4 47559.2 2373.76 6 -4 6 3 43990.1 2562.90 4 4 6 -3 42439.1 2240.56 6 -4 6 2 17609.5 1481.72 4 4 6 -2 15475.5 1247.10 6 -4 6 1 46325.6 2477.63 4 4 6 -1 37649.5 2181.71 6 4 6 0-18.0662 107.799 6 -4 6 0 140.461 85.5080 4 -4 6 -1 13784.7 1167.46 4 4 6 1 11797.1 1196.38 6 4 6 2 2301.00 481.398 7 4 6 2 2537.06 529.702 6 4 6 3 46879.2 2562.82 7 4 6 3 53302.0 2718.67 6 4 6 4 72481.3 3311.89 6 4 6 5 40122.4 2206.14 6 4 -6 6 36168.3 2405.36 11 4 6 6 33136.2 1982.84 6 4 6 6 38248.9 2293.18 10 4 -6 6 35496.1 2456.65 15 4 6 7 163.283 157.307 10 4 -6 7-72.9806 215.953 11 4 -6 7 218.853 176.184 15 4 6 7 113.762 96.3308 6 4 -6 8 4066.03 733.817 11 4 6 8 4469.64 716.102 10 4 -6 8 3402.31 703.029 15 4 -6 9 2003.49 492.670 11 4 6 9 1918.50 440.767 10 4 -6 9 1269.62 411.716 15 4 -6 10 3435.00 619.158 11 4 6 10 3289.83 547.601 10 4 -6 11 8554.27 902.210 11 4 6 11 9072.24 874.172 10 4 -6 12 3889.51 523.116 11 -4 7 15-76.5167 87.6863 9 -4 7 14 136.395 125.908 9 -4 -7 13 23.4348 87.0335 11 -4 7 13 114.782 134.710 20 -4 7 13 41.8871 113.512 9 -4 -7 12 15.6206 115.844 11 -4 7 12 125.049 107.930 20 -4 -7 11 2116.64 582.881 11 -4 7 11 2364.83 602.683 9 -4 -7 10 216.774 141.559 11 -4 7 10 164.572 249.289 20 -4 7 10 321.652 217.395 9 -4 -7 9 16488.1 1632.98 11 -4 7 9 18265.9 1825.40 20 -4 7 9 13780.4 1482.26 9 -4 -7 9 16809.9 1263.13 14 -4 7 8 15741.8 1706.39 20 -4 7 8 28032.7 2117.86 4 -4 7 7 265.809 164.628 4 -4 7 6 3873.42 766.073 4 -4 7 5 291.440 186.409 4 -4 7 4 906.723 367.706 4 -4 7 4 940.516 344.339 7 -4 7 3 6982.58 895.468 7 -4 7 3 7479.88 1007.49 4 4 7 -2 6550.86 837.747 6 -4 7 2 9416.46 1117.56 4 4 7 -1 3146.41 592.141 6 -4 7 1 4214.19 711.806 4 -4 7 0 32912.1 2061.85 4 4 7 0 25442.6 1864.99 6 4 7 1 18140.7 1527.60 7 4 7 1 15350.8 1378.83 6 4 7 2 10978.0 1177.93 7 4 7 2 10738.6 1144.84 6 4 7 3 630.005 282.378 7 4 7 3 467.150 224.336 6 4 7 4 11367.7 1096.28 6 4 -7 5-87.1927 125.785 11 4 -7 5 149.810 69.2438 19 4 7 5 191.768 149.676 6 4 -7 6 638.935 280.980 11 4 -7 6 778.216 357.510 15 4 7 6 917.054 322.384 10 4 7 6 657.205 263.957 6 4 -7 7 20923.2 1768.28 11 4 7 7 21690.8 1647.59 10 4 -7 7 18589.1 1765.74 15 4 -7 8 11473.8 1249.44 11 4 7 8 11506.3 1152.57 10 4 -7 8 10682.2 1264.71 15 4 -7 9 5095.27 797.493 11 4 7 9 5173.05 719.705 10 4 -7 9 5472.21 877.260 15 4 -7 10 9028.19 982.158 11 4 7 10 8756.03 891.743 10 4 -7 11 2483.38 449.574 11 4 -7 12 1154.35 267.198 11 -4 8 14 105.498 79.9079 20 -4 8 14 175.435 92.7358 9 -4 -8 13 3187.64 595.909 11 -4 8 13 2741.09 534.977 9 -4 8 13 3920.68 656.615 20 -4 8 12 2518.42 544.445 9 -4 -8 12 2429.97 586.473 11 -4 8 12 3791.47 721.489 20 -4 -8 11 3822.49 781.226 11 -4 8 11 7457.13 1093.94 20 -4 -8 10 650.034 312.711 11 -4 8 10 972.720 340.138 20 -4 -8 10 885.504 308.435 13 -4 -8 9 8114.46 1133.33 11 -4 -8 9 8568.82 986.868 13 -4 8 9 6691.09 1104.52 20 -4 8 8 953.262 402.679 4 -4 -8 8 465.234 297.960 11 -4 8 8 755.299 392.812 20 -4 -8 8 477.825 235.880 14 -4 -8 7 15219.4 1519.64 11 -4 8 7 12804.9 1529.25 20 -4 8 7 14995.6 1620.25 4 -4 -8 7 15718.5 1273.34 14 -4 8 6 9647.21 1288.00 4 -4 8 5 6823.72 1070.80 4 -4 8 4 29154.5 2223.90 4 -4 8 4 23285.3 1865.42 7 -4 8 3 29510.3 2205.07 4 -4 8 3 25108.3 1865.92 7 -4 8 2 9980.37 1222.56 4 -4 8 1 10356.9 1212.25 4 4 8 0 7959.11 1087.42 7 -4 8 0 8997.49 1073.35 4 4 8 1 24444.8 1956.51 7 4 8 2 5859.76 899.911 7 4 8 3 8453.16 1030.98 7 4 8 3 7591.79 897.884 6 4 8 4 4715.56 676.736 6 -4 -8 -4 5045.71 704.383 18 4 -8 4 5096.17 801.642 19 4 -8 5 1292.89 408.265 19 4 8 5 646.984 240.331 6 4 -8 6-28.9473 119.551 15 4 -8 6 322.036 249.247 11 4 -8 7 2841.98 615.006 11 4 8 7 2740.07 542.543 10 4 -8 7 2536.48 616.136 15 4 -8 8 2224.66 507.808 11 4 8 8 2067.14 445.305 21 4 -8 8 2461.74 577.222 15 4 8 8 2318.99 463.450 10 4 -8 9 12401.7 1185.02 11 4 8 9 12243.5 1087.42 10 4 -8 9 13222.4 1336.31 15 4 -8 10 453.628 176.158 11 4 -8 11 1306.02 299.585 11 -4 9 14 529.634 160.803 20 -4 9 13 1808.01 414.181 20 -4 -9 12-258.117 187.357 11 -4 9 12 33.2637 150.047 20 -4 -9 11 3884.05 737.092 11 -4 9 11 5001.21 877.096 20 -4 -9 10 1664.92 507.557 11 -4 9 10 2188.21 601.665 20 -4 -9 10 2716.43 510.660 13 -4 -9 9 822.903 371.466 11 -4 9 9 757.334 308.905 20 -4 -9 9 972.316 325.161 13 -4 -9 8 234.428 208.942 11 -4 9 8 126.207 150.688 20 -4 -9 8 534.532 269.086 13 -4 -9 7 5827.34 939.524 11 -4 9 7 5399.44 988.475 20 -4 -9 6 10340.4 1257.53 11 -4 9 6 10158.0 1346.53 20 -4 9 6 8073.05 1214.86 4 -4 -9 6 11947.3 1112.26 14 -4 9 5 2680.88 680.125 4 -4 9 5 3470.41 752.639 20 -4 -9 5 3929.53 612.478 14 -4 9 4 1042.30 424.044 4 -4 -9 4 1434.98 384.442 14 -4 9 4 978.382 366.167 7 4 9 -3 40380.5 2719.91 7 -4 9 3 38179.7 2687.58 4 4 9 -2 9342.45 1252.36 7 -4 9 2 10572.0 1305.41 4 4 9 -1 10736.5 1355.60 7 -4 9 1 13474.3 1430.25 4 4 9 0 14909.7 1572.29 7 -4 9 0 13003.2 1353.67 4 4 9 1 6700.70 1035.78 7 -4 -9 -1 7684.09 929.625 18 4 9 2 4674.72 832.300 7 -4 -9 -2 5458.55 780.677 18 4 -9 2 5347.69 843.661 19 4 9 3 594.347 282.759 7 4 -9 3 495.074 227.934 19 -4 -9 -3 423.252 231.271 18 -4 -9 -4 814.173 315.859 18 4 -9 4 660.973 291.612 19 4 -9 5 29067.1 2041.37 19 4 -9 6 535.227 262.253 11 4 -9 6 232.099 210.223 15 4 -9 7 109.145 100.351 11 4 -9 7 130.872 196.754 15 4 -9 8 6030.01 807.760 11 4 9 8 5805.16 739.754 21 4 -9 8 6272.54 911.635 15 4 -9 9 7846.78 852.609 11 4 9 9 5813.41 656.186 21 4 -9 10 299.190 150.047 11 4 -9 11-5.28431 68.4684 11 -4 10 13 1251.14 295.253 20 -4 10 12-49.8152 91.2835 20 -4 10 11 211.172 174.341 20 -4 -10 11 326.502 151.793 13 -4 -10 10 3572.91 691.327 11 -4 10 10 2946.60 647.488 20 -4 -10 10 2727.00 500.176 13 -4 -10 9 977.328 412.782 11 -4 10 9 774.695 349.631 20 -4 -10 9 968.993 325.866 13 -4 -10 8 84.3182 135.238 11 -4 10 8 108.433 197.808 20 -4 -10 8-19.1714 175.466 13 -4 10 7 13887.5 1579.42 20 -4 -10 7 15559.5 1437.04 13 -4 10 6 338.080 247.824 20 4 -10 -5 3324.08 713.616 12 -4 10 5 5300.34 914.006 20 4 -10 -4 76.0964 160.994 12 -4 -10 4 203.190 79.9991 18 -4 -10 4 391.504 217.038 14 4 -10 -3 4646.27 877.256 12 -4 -10 3 6044.16 828.333 18 -4 10 3 5053.47 935.771 4 -4 -10 3 5810.19 800.044 14 4 10 -3 4673.44 894.735 7 4 -10 -2 210.336 151.119 12 -4 10 2 132.676 162.326 4 -4 -10 2 471.632 252.439 18 4 10 -2 554.732 240.597 7 -4 -10 2 372.458 192.641 14 -4 10 1 3552.37 740.766 4 -4 -10 1 4386.57 712.047 18 4 10 -1 3600.69 786.937 7 4 -10 -1 3729.93 790.503 12 4 10 0 12.4228 160.532 7 -4 -10 0 150.823 102.550 18 -4 -10 -1 45965.3 2573.80 18 4 -10 2 8838.20 1131.55 19 -4 -10 -2 9357.54 1056.99 18 4 -10 3 1016.11 369.399 19 -4 -10 -3 1757.67 419.459 18 -4 -10 -4 161.905 114.760 18 4 -10 4-405.022 231.753 19 -4 -10 -5 15319.3 1255.68 18 4 -10 5 13912.5 1337.96 19 4 -10 6 1646.61 478.715 15 4 -10 7-49.5663 82.7961 11 4 10 7 173.510 169.083 21 4 -10 7 33.6910 137.858 15 4 -10 8 103.768 77.3745 11 4 10 8 11.5605 57.8306 21 4 -10 8 216.774 173.973 15 4 -10 9 12935.5 1009.43 11 4 10 9 12347.2 912.555 21 4 -10 10 1888.05 315.390 11 -4 11 12 757.152 234.313 20 -4 11 11 3577.74 613.879 20 -4 -11 11 2243.15 365.320 13 -4 11 10 347.299 258.387 20 -4 -11 10 220.781 142.544 13 -4 11 9 2669.08 603.078 20 -4 -11 9 2664.64 506.959 13 -4 11 8 464.883 276.046 20 -4 -11 8 989.511 337.914 13 -4 11 7 1301.74 448.877 20 -4 -11 7 1932.98 501.725 13 -4 11 6 946.769 424.321 20 -4 -11 6 1312.81 389.062 13 -4 -11 5 6281.21 915.662 13 4 -11 -5 4850.10 880.802 12 4 -11 -4 247.482 247.112 12 -4 -11 4 90.4940 88.2107 18 -4 -11 4 179.330 144.829 13 -4 -11 3 29259.1 1945.68 18 -4 -11 3 28554.1 2039.74 13 4 -11 -3 26554.3 2204.78 12 -4 -11 2 182.877 84.8441 18 -4 -11 2 212.921 106.698 13 4 -11 -2 108.791 193.210 12 -4 -11 1 521.171 285.544 18 -4 -11 0 110.891 128.087 18 -4 -11 -1 9799.18 1084.85 18 4 -11 1 8626.38 1120.77 19 -4 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919.847 10 5 -8 7 8695.35 1103.36 15 5 -8 8 2316.07 474.722 11 5 8 8 2546.70 455.362 10 5 -8 8 2270.48 516.658 15 5 -8 9 1356.69 337.418 11 5 8 9 737.768 219.051 10 5 -8 10 4299.67 524.753 11 -5 9 13 3358.49 536.733 20 -5 9 12 4481.41 714.596 20 -5 9 11 30.4870 122.702 20 -5 9 10 478.706 219.156 20 -5 -9 10 524.430 227.967 13 -5 9 9 7809.33 1167.14 20 -5 -9 9 9971.58 1076.84 13 -5 9 8 102.770 164.020 20 -5 9 7 3957.00 802.967 20 -5 -9 7 3951.73 635.598 14 -5 9 6 7.37157 235.591 20 -5 -9 6-189.699 231.756 14 -5 9 5 25471.0 2106.98 20 -5 -9 5 29944.0 1902.27 14 -5 9 4 2535.90 668.579 4 -5 -9 4 2469.34 517.179 18 -5 -9 4 2838.21 557.429 14 -5 9 3 176.296 141.456 4 -5 -9 3-10.6910 137.381 18 5 9 -3 217.907 119.643 7 -5 -9 3 150.024 137.216 14 5 9 -2 9183.69 1258.06 7 -5 9 2 9262.06 1235.81 4 -5 -9 2 10110.6 1088.81 18 -5 -9 2 8153.40 936.233 14 5 9 -1 3584.66 771.639 7 -5 -9 1 4531.75 724.859 18 -5 9 1 3157.15 668.735 4 -5 -9 0 488.731 191.665 18 5 9 0 498.983 291.652 7 5 -9 0 456.794 328.409 19 5 -9 1 5530.11 904.295 19 -5 -9 -1 5424.47 783.474 18 5 -9 2 1654.36 475.080 19 -5 -9 -2 1506.95 408.530 18 5 -9 3 47345.9 2841.42 19 -5 -9 -3 50252.8 2629.74 18 5 -9 4 1314.90 429.576 19 -5 -9 -4 1179.97 343.769 18 5 -9 5 6444.89 998.109 15 5 -9 6 10906.6 1261.14 15 5 -9 7 2016.23 438.836 11 5 9 7 1926.00 411.631 21 5 -9 7 2717.91 601.384 15 5 -9 8 141.219 86.4515 11 5 9 8 198.504 144.204 21 5 -9 8 1.80423 112.920 15 5 -9 9 947.947 241.632 11 -5 10 13 1378.71 288.410 20 -5 10 12 89.9709 106.675 20 -5 10 11 53.4457 86.2752 20 -5 -10 11-210.963 175.974 13 -5 10 10 105.930 117.576 20 -5 -10 10 279.421 195.244 13 -5 10 9 17657.9 1687.66 20 -5 -10 9 21232.2 1546.05 13 -5 10 8 1097.98 404.718 20 -5 -10 8 2077.72 500.653 13 -5 10 7 160.961 150.396 20 -5 10 6 2696.31 655.624 20 -5 -10 6 2989.68 556.863 14 -5 -10 5 3883.17 648.744 14 -5 -10 4 555.889 262.575 18 -5 -10 4 165.480 161.297 14 -5 -10 3 188.220 100.437 18 -5 -10 3 121.359 73.0798 14 -5 -10 2-70.0498 206.586 18 -5 -10 2 47.1851 164.400 14 5 -10 -1 38531.2 2592.73 19 -5 -10 1 36233.5 2242.08 18 5 -10 0 8256.03 1119.02 19 -5 -10 0 8281.00 977.217 18 5 -10 1 1178.82 419.071 19 -5 -10 -1 1945.05 457.535 18 5 -10 2 3889.99 745.640 19 -5 -10 -2 4336.90 703.480 18 5 -10 3 4509.73 768.727 19 -5 -10 -3 5299.30 746.471 18 5 -10 4 764.979 279.488 19 -5 -10 -4 1169.24 323.082 18 -5 -10 -5-32.7689 99.4561 18 5 -10 5-145.674 195.480 15 5 -10 6 610.610 320.959 15 5 10 7 20225.4 1346.85 21 5 -10 7 23871.8 1688.42 15 5 10 8 2588.97 377.144 21 -5 11 12 110.908 89.8064 20 -5 11 11 430.631 168.825 20 -5 -11 11 285.500 138.430 13 -5 11 10 827.807 282.082 20 -5 -11 10 1132.48 276.223 13 -5 11 9 2001.12 495.862 20 -5 -11 9 2123.39 431.706 13 -5 11 8 45.5530 150.923 20 -5 -11 8 608.424 222.768 13 -5 11 7 37.7009 178.782 20 -5 -11 7-124.345 190.868 13 -5 11 6 368.888 225.663 20 -5 -11 6 444.850 221.730 13 -5 -11 5 28051.5 1982.46 13 -5 -11 4 2210.52 503.361 18 -5 -11 3 145.598 163.576 18 -5 -11 2 296.002 183.816 18 5 -11 -1 9384.61 1208.26 19 -5 -11 1 9522.51 1063.24 18 5 -11 0 5856.37 911.828 19 -5 -11 0 5885.28 815.246 18 5 -11 1 325.663 159.635 19 -5 -11 -1 450.351 233.096 18 -5 -11 -2 429.575 157.249 18 5 -11 2 63.4366 131.449 19 5 -11 3 12544.5 1285.33 19 -5 -11 -3 15628.9 1276.23 18 5 -11 4 2827.49 553.266 19 -5 -11 -4 2840.84 507.521 18 5 -11 4 3253.44 686.782 15 -5 -11 -5 216.892 139.217 18 5 -11 5 893.767 360.849 15 5 11 6 2469.00 440.493 21 5 -11 6 2140.04 482.059 15 5 11 7 152.971 100.725 21 5 -11 7 193.262 134.691 15 -5 12 10 28.8114 46.7782 20 -5 -12 10 171.529 110.197 13 -5 12 9 3659.93 568.736 20 -5 -12 9 4199.49 560.913 13 -5 12 8 64.1163 141.149 20 -5 -12 8 50.8933 99.9606 13 -5 12 7-161.052 136.766 20 -5 -12 7 115.748 131.834 13 -5 -12 6 330.568 185.818 13 -5 -12 5 12634.7 1193.66 13 -5 -12 4 4628.33 654.332 18 -5 -12 4 5227.48 770.241 13 5 -12 -3 1243.11 417.947 19 -5 -12 3 1706.56 415.722 18 -5 -12 3 1159.09 336.246 13 5 -12 -2 1340.96 420.776 19 -5 -12 2 1648.45 437.549 18 -5 -12 2 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1486.78 6 6 3 5 1957.64 510.676 10 6 -3 5 3166.18 712.856 15 6 3 5 2101.79 466.189 6 6 -3 6 12125.6 1277.11 11 6 3 6 11751.7 1186.60 10 6 -3 6 11966.8 1409.85 15 6 -3 7 17250.0 1522.49 11 6 3 7 17089.0 1408.88 10 6 -3 8 226.956 165.854 11 6 3 8 139.669 159.171 10 6 -3 9 11871.8 1123.82 11 6 3 9 10874.0 1009.54 10 6 3 9 11024.8 1111.27 8 6 -3 10 156.129 97.5115 11 6 3 10 163.062 101.561 10 6 3 10 166.189 122.245 8 6 -3 11 569.770 176.232 11 6 3 11 307.537 123.897 8 -6 4 16 276.712 139.458 9 -6 4 15 112.191 156.382 9 -6 4 14 1092.88 382.194 9 -6 4 13 5040.38 876.781 9 -6 4 13 7709.21 1012.15 20 -6 4 12-124.133 148.720 20 -6 4 12 240.460 234.247 9 -6 4 11 2855.10 702.104 20 -6 4 11 3780.51 794.684 9 -6 4 10 3469.65 778.173 20 -6 4 10 4175.49 821.869 9 -6 4 9 31186.7 2292.35 5 -6 4 9 25515.6 2209.50 20 -6 4 9 29661.4 2276.15 9 -6 -4 9 23131.1 1802.63 17 6 4 -9 29342.4 2214.10 6 -6 4 8 24108.5 1965.29 5 6 4 -8 22346.2 1908.42 6 6 4 -7 149.818 204.992 6 -6 4 7-225.456 191.223 5 -6 4 6 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10 6 -5 10 1780.41 351.569 11 6 5 10 1295.69 278.210 10 6 -5 11 1029.42 213.644 11 -6 6 15-25.7862 62.3876 9 -6 6 14 556.628 242.006 9 -6 6 14 637.594 216.837 20 -6 6 13 966.651 337.312 20 -6 6 13 756.728 294.778 9 -6 6 12 7888.39 1079.30 20 -6 6 12 5620.15 929.687 9 -6 6 11 946.846 403.381 20 -6 6 11 969.149 423.821 9 -6 6 10 6777.68 1087.91 20 -6 6 10 8121.04 1168.29 9 -6 6 9 3345.99 750.573 20 -6 6 9 3679.31 767.646 9 -6 -6 9 3620.28 572.934 14 6 6 -8 3371.07 690.774 6 -6 6 8 4752.94 903.139 20 -6 6 8 3529.85 766.151 9 -6 -6 8 5373.25 712.471 14 6 6 -7 2324.54 594.368 6 -6 6 7 2903.68 682.598 20 -6 6 7 2805.95 653.943 9 -6 -6 7 3197.42 557.121 14 -6 6 6 4970.83 912.055 20 6 6 -6 4677.10 827.579 6 -6 -6 6 5232.15 720.433 14 6 6 -5 17705.7 1604.81 6 6 6 -4-221.092 262.650 6 6 6 -3 3002.14 648.138 6 6 6 -2 15032.6 1506.48 6 6 6 -1 24241.3 1985.54 6 6 6 0 5545.95 943.475 6 6 -6 1 12374.5 1359.75 19 6 6 1 9757.61 1225.27 6 6 -6 2 669.462 319.103 19 6 6 2 466.073 269.754 10 6 6 2 230.248 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514.973 178.776 17 -7 6 13 2519.54 528.693 20 -7 6 12 297.389 242.050 20 -7 6 11 1419.92 440.834 20 -7 6 10 6.45203 218.591 20 -7 -6 10-53.1928 119.940 14 -7 6 9 588.369 272.306 20 -7 -6 9 915.211 304.475 14 -7 6 8 477.823 270.288 20 -7 -6 8 63.3883 107.974 14 -7 6 7 468.268 289.475 20 -7 -6 7 850.490 333.435 17 -7 -6 7 658.064 258.875 14 -7 6 6-310.950 230.754 20 -7 -6 6 46.8471 134.272 17 -7 -6 6-113.947 136.689 14 -7 6 5 8377.00 1155.07 20 -7 -6 5 9185.29 1083.48 17 -7 -6 4 26028.8 1907.72 17 7 6 -3 7795.47 1170.26 6 -7 6 3 9318.86 1067.36 16 7 -6 -2 636.235 312.661 19 -7 6 2 897.494 314.948 16 7 -6 -1 3082.64 705.636 19 -7 6 1 1750.51 408.459 16 7 -6 0 2877.71 689.413 19 7 6 1-224.388 194.265 10 7 6 2 103.103 76.1620 10 7 -6 2 391.309 286.520 15 7 6 3 21051.2 1697.32 10 7 -6 3 25939.7 2146.17 15 7 -6 4 10847.1 1175.75 11 7 6 4 12380.8 1213.50 10 -7 -6 -4 9959.29 947.033 18 7 -6 4 12583.7 1419.99 15 7 -6 5 11926.5 1210.63 11 7 6 5 14993.7 1284.05 10 7 -6 5 13709.2 1455.90 15 7 -6 6 3074.17 570.352 11 7 6 6 3423.18 565.455 10 7 -6 7 3237.28 533.438 11 7 6 7 3951.72 546.772 10 7 -6 8 1412.70 312.069 11 7 6 8 1705.37 318.930 10 -7 7 13 53.1810 119.818 20 -7 7 12 1860.26 475.569 20 -7 7 11 2693.33 609.750 20 -7 7 10 225.123 97.4112 20 -7 -7 10 359.587 175.043 14 -7 7 9 5754.22 979.299 20 -7 -7 9 7244.14 810.277 14 -7 7 8 8141.96 1190.37 20 -7 -7 8 8690.62 947.666 14 -7 7 7 4581.64 875.241 20 -7 -7 7 5158.30 737.067 14 -7 7 6 965.902 382.078 20 -7 -7 6 769.885 299.580 14 -7 7 5 1127.70 416.445 20 -7 -7 5 1379.99 339.438 14 -7 7 4 19.5131 127.144 16 -7 -7 4-22.8384 100.472 14 7 -7 -3 10618.7 1325.70 19 -7 7 3 8337.98 997.832 16 -7 -7 3 10729.4 1106.97 14 7 -7 -2 1675.24 528.682 19 -7 7 2 1587.78 411.266 16 -7 -7 2 1691.11 427.781 14 7 -7 -1 1447.64 487.730 19 -7 -7 1 1464.05 390.175 14 7 -7 0 16386.0 1636.36 19 7 7 0 10524.7 1191.89 10 7 7 1 370.595 251.568 10 7 7 2 2685.66 568.087 10 -7 -7 -2 2473.94 502.934 18 7 -7 2 2526.80 651.064 15 7 7 3 21026.1 1643.48 10 -7 -7 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1287.12 19 -7 -9 3 10298.5 1069.93 18 -7 -9 3 9418.80 1017.84 14 7 -9 -2 2377.88 596.101 19 -7 -9 2 3003.18 568.023 18 -7 -9 2 1785.70 384.632 14 7 -9 -1 1237.76 402.859 19 -7 -9 1 2114.13 480.176 18 7 -9 0 3761.51 729.783 19 -7 -9 0 3464.21 610.351 18 -7 -9 -1 7913.08 894.378 18 -7 -9 -2 585.914 239.955 18 7 -9 2 821.572 382.986 15 -7 -9 -3 1396.59 340.031 18 7 -9 3 1341.17 451.724 15 -7 -9 -4 1635.95 309.134 18 7 -9 4 2870.16 580.396 15 7 -9 5 8091.18 930.075 15 7 9 6 1698.68 278.494 21 -7 10 11-72.1466 104.365 20 -7 10 10-36.6221 134.075 20 -7 -10 10-78.8064 58.4506 13 -7 10 9 1821.62 426.567 20 -7 -10 9 1803.46 389.175 13 -7 10 8 20.3298 84.1740 20 -7 -10 8 106.243 139.021 13 -7 10 7 5008.72 730.682 20 -7 10 6 930.685 308.912 16 -7 -10 6 1738.26 403.815 14 -7 10 5 1844.46 407.167 16 -7 -10 5 2829.17 510.578 14 7 -10 -4 122.461 75.8410 19 -7 -10 4 487.186 215.664 18 -7 -10 4 670.481 257.610 14 7 -10 -3 1215.25 372.569 19 -7 -10 3 1298.39 350.610 18 -7 -10 3 1304.70 359.863 14 7 -10 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1 2710.71 481.182 18 -7 -11 0 864.354 249.380 18 -7 -11 -1 3045.09 465.795 18 7 -11 1 2682.41 550.834 15 -7 -11 -2 2084.74 367.334 18 7 -11 2 1969.99 442.657 15 -7 -11 -3 3333.29 408.045 18 7 -11 3 4381.04 622.221 15 7 -11 4 687.528 233.439 15 -7 -12 7 1062.53 254.786 13 -7 -12 6-77.0557 110.496 13 7 -12 -5 264.982 129.370 19 -7 -12 5 361.426 143.740 13 7 -12 -4 2357.61 440.668 19 -7 -12 4 2075.90 341.358 18 -7 -12 4 2347.93 387.431 13 7 -12 -3 33.8918 85.1674 19 -7 -12 3-35.5422 96.6533 18 -7 -12 3-56.4150 101.558 13 7 -12 -2 233.495 163.117 19 -7 -12 2 105.262 80.2689 18 -7 -12 1 2962.31 445.585 18 -7 -12 0 122.686 113.702 18 7 -12 0 146.733 140.806 15 -7 -12 -1 3598.45 448.173 18 7 -12 1 3378.26 537.391 15 -8 0 15 154.556 84.9906 17 -8 0 14 346.586 189.938 17 -8 0 13-41.5216 199.188 17 -8 0 12 155.370 114.470 17 -8 0 11 170.177 144.259 17 -8 0 10 550.501 290.298 17 -8 0 9-449.061 246.271 17 -8 0 8 13644.9 1346.07 17 -8 0 7 85.7045 102.782 17 -8 0 7 276.391 230.575 16 -8 0 6 7154.65 919.334 17 -8 0 6 6605.01 960.104 16 8 0 -6 4782.44 852.418 6 8 0 -5 153.556 172.880 6 -8 0 5 182.874 152.225 17 -8 0 5 157.887 182.716 16 8 0 -4 1275.89 426.681 6 -8 0 4 1745.71 420.102 17 -8 0 4 2326.20 534.348 16 8 0 -3-136.755 190.622 6 -8 0 3 124.963 125.873 17 -8 0 3 112.398 150.406 16 -8 0 2 2742.03 522.208 17 -8 0 2 3897.84 694.473 16 -8 0 1 6.00868 119.637 16 -8 0 0 10361.0 1128.92 16 -8 0 -1 26.2779 132.859 16 8 0 2 13451.7 1311.96 10 -8 0 -2 17148.5 1428.65 16 8 0 3 145.579 75.0262 10 8 0 4 5330.62 771.920 10 8 0 5-7.58320 78.6467 10 8 0 6 12292.1 1143.11 11 8 0 6 10186.3 912.626 10 8 0 7-86.9479 110.182 11 8 0 8 1959.93 352.728 11 -8 -1 15 182.188 117.418 17 -8 1 15 192.113 126.091 17 -8 -1 14 93.4460 99.7399 17 -8 1 14 9.41398 98.9023 17 -8 -1 13 50.4434 66.7712 17 -8 1 13-130.961 181.530 17 -8 -1 12 3265.63 638.603 17 -8 1 12 2838.53 579.613 17 -8 -1 11-16.9385 177.125 17 -8 1 11 105.430 120.663 17 -8 -1 10 5022.45 811.879 17 -8 1 10 4135.39 725.045 17 -8 -1 9 227.729 90.4546 17 -8 1 9 599.626 242.528 17 -8 -1 8 2768.88 590.023 17 -8 1 8 3042.79 597.714 17 -8 1 8 1654.07 494.560 16 -8 -1 7 840.386 338.711 17 -8 1 7 498.955 289.155 17 -8 1 7 465.422 258.708 16 -8 1 6 3832.87 665.429 17 -8 -1 6 3237.21 618.017 17 -8 -1 6 3052.90 643.841 16 -8 1 6 3122.82 671.813 16 8 1 -5 1534.84 482.037 6 -8 -1 5 1333.97 393.389 17 -8 1 5 1809.42 443.330 17 -8 -1 5 1945.49 511.421 16 -8 1 5 2256.10 551.962 16 -8 -1 4 20790.8 1581.16 17 -8 1 4 17107.2 1404.75 17 -8 -1 4 20882.8 1716.75 16 -8 1 4 20016.9 1678.24 16 8 1 -4 15705.5 1611.72 6 8 1 -3 2503.29 616.523 6 -8 -1 3 4357.17 691.620 17 -8 -1 3 4240.10 725.696 16 -8 1 3 4646.28 766.002 16 -8 -1 2 10070.7 1053.86 17 -8 -1 2 10300.9 1158.47 16 -8 1 2 9926.23 1111.80 16 8 1 -1 367.647 254.564 6 -8 -1 1 1180.52 403.694 16 -8 1 1 902.101 299.917 16 -8 -1 0 6934.75 919.026 16 -8 1 0 7417.29 939.272 16 -8 -1 -1 3799.60 661.876 16 -8 1 -1 3473.67 616.643 16 8 -1 2 4750.76 756.156 10 8 1 2 7055.88 929.062 10 -8 -1 -2 7038.10 900.951 16 -8 1 -2 7837.42 931.527 16 8 1 3 412.634 242.599 10 -8 1 -3 617.442 242.797 16 8 1 4 8465.50 974.717 10 8 1 5 1143.42 343.756 10 8 -1 6 4533.61 689.844 11 8 1 6 5374.40 666.676 10 8 -1 7 265.052 148.408 11 8 1 7 344.860 176.533 11 8 1 7 416.741 183.103 10 8 -1 8 322.209 125.647 11 8 1 8 246.669 104.598 11 8 1 8 161.606 84.3156 10 -8 2 15 116.178 81.0963 17 -8 -2 14 216.989 148.489 17 -8 2 14-16.5630 83.2000 17 -8 -2 13-57.8787 116.671 17 -8 2 13-422.902 210.765 17 -8 -2 12 264.886 203.546 17 -8 2 12 157.182 122.374 17 -8 -2 11 5854.55 845.589 17 -8 2 11 3906.45 702.198 17 -8 -2 10 2487.90 579.139 17 -8 2 10 2094.10 497.443 17 -8 -2 9 527.602 272.251 17 -8 2 9 300.033 101.976 17 -8 2 9 113.104 140.584 16 -8 -2 8 11100.1 1207.79 17 -8 2 8 9982.54 1133.81 17 -8 2 8 8497.81 1124.70 16 -8 -2 7 71.2342 128.591 17 -8 2 7 220.284 172.941 17 -8 2 7 93.9536 133.968 16 -8 -2 6 1760.84 455.797 17 -8 2 6 1717.66 440.215 17 -8 2 6 1569.28 452.815 16 -8 -2 5 1204.45 368.802 17 -8 2 5 1382.38 373.631 17 -8 2 5 1307.29 408.623 16 -8 -2 4 6580.48 872.623 17 -8 -2 4 5891.35 884.811 16 -8 2 4 6184.28 904.397 16 8 2 -4 5100.09 908.049 6 -8 -2 3 9556.80 1057.56 17 -8 -2 3 8709.25 1085.64 16 -8 2 3 9548.26 1107.17 16 8 2 -3 7358.86 1104.94 6 -8 -2 2 9567.87 1040.83 17 -8 -2 2 9634.94 1130.72 16 8 2 -2 6727.71 1060.19 6 -8 2 2 8638.78 1033.40 16 -8 -2 1 1783.45 471.090 16 -8 2 1 1397.01 384.351 16 -8 -2 0 31093.6 2103.48 16 -8 2 0 30244.7 2003.28 16 -8 -2 -1 3818.85 676.634 16 -8 2 -1 3698.39 637.178 16 8 2 2 4285.85 727.235 10 -8 2 -2 4414.42 673.842 16 8 2 3 163.150 108.850 10 -8 2 -3 374.882 205.045 16 8 2 4 47.9450 114.304 10 8 -2 5 13452.1 1279.87 11 8 2 5 12911.4 1172.65 10 8 -2 6 5279.72 732.299 11 8 2 6 4380.03 611.005 10 8 -2 7 25.0553 126.450 11 8 2 7 82.9259 107.290 11 8 2 7 71.5907 87.6396 10 8 -2 8 3749.16 486.403 11 8 2 8 2580.83 374.946 11 8 2 8 3032.09 388.700 10 -8 3 15 190.177 121.111 17 -8 -3 14 361.621 165.782 17 -8 3 14 554.703 220.600 17 -8 -3 13 13.7395 58.8256 17 -8 3 13-95.3681 137.838 17 -8 -3 12 3775.59 639.153 17 -8 3 12 2651.49 519.502 17 -8 -3 11 1739.68 457.328 17 -8 3 11 987.612 341.391 17 -8 -3 10 435.838 263.256 17 -8 3 10 229.563 143.287 17 -8 3 10 260.481 209.550 16 -8 -3 9 194.195 191.042 17 -8 3 9-0.58699 147.966 17 -8 3 9 53.8503 168.521 16 -8 -3 8 799.476 341.500 17 -8 3 8 946.521 346.768 17 -8 3 8 746.983 339.516 16 -8 -3 7 16712.2 1491.10 17 -8 3 7 13575.8 1284.78 17 -8 3 7 14295.8 1461.78 16 -8 -3 6 5346.24 807.211 17 -8 3 6 5162.36 858.722 16 -8 -3 5 53.5628 97.7504 17 -8 3 5-35.0374 129.193 16 -8 -3 4 4397.36 710.546 17 -8 3 4 4037.06 715.786 16 -8 -3 3-52.0798 162.705 17 -8 -3 3-131.854 218.631 16 -8 3 3 78.5245 157.138 16 -8 -3 2 2938.40 623.307 16 -8 3 2 2710.25 565.224 16 -8 -3 1 843.094 339.441 16 -8 3 1 809.239 302.373 16 -8 -3 0-97.3598 128.964 16 -8 3 0 137.893 136.633 16 -8 3 -1 15727.8 1346.14 16 8 3 2 1227.63 400.526 10 -8 3 -2 802.831 255.744 16 8 3 3 1582.19 436.571 10 8 -3 4 5267.72 813.486 11 8 3 4 4744.03 745.562 10 8 -3 5 358.014 209.193 11 8 3 5 304.534 203.684 10 8 -3 6 1676.78 394.549 11 8 3 6 1966.59 398.933 10 8 -3 7 367.498 157.128 11 8 3 7 208.026 111.925 11 8 3 7 195.413 144.671 10 8 -3 8 1635.74 307.770 11 8 3 8 1831.99 296.357 10 -8 4 14 83.3078 116.538 17 -8 4 13 772.073 239.581 17 -8 -4 12 4049.75 615.457 17 -8 4 12 3239.15 557.193 17 -8 -4 11 2843.78 552.537 17 -8 4 11 2343.73 502.326 17 -8 4 11 1641.65 420.892 16 -8 4 10 465.601 198.575 17 -8 4 10 227.153 116.288 16 -8 -4 9-32.4392 100.910 17 -8 4 9 340.957 189.418 17 -8 4 9-132.386 245.278 16 -8 -4 9 555.838 237.592 14 -8 -4 8 792.246 350.930 17 -8 4 8 395.562 215.183 16 -8 -4 7 811.191 326.931 17 -8 4 7 238.253 82.7182 16 -8 -4 6-118.963 172.218 17 -8 4 6-183.418 167.670 16 -8 -4 5-145.552 198.433 17 -8 4 5-219.635 180.021 16 -8 -4 4 846.276 293.122 17 -8 4 4 1048.38 359.328 16 -8 4 3 31030.7 2116.04 16 -8 -4 2 5442.49 855.849 16 -8 4 2 5927.50 841.976 16 -8 4 1 1361.45 391.515 16 -8 4 0 264.675 158.342 16 8 4 1 273.229 243.316 10 -8 4 -1-151.100 173.049 16 8 4 2 2609.65 570.350 10 8 -4 3 17.7649 107.350 11 8 4 3 10.7569 97.0919 10 8 -4 4 5863.21 836.253 11 8 4 4 5502.89 803.813 10 8 -4 5 9797.60 1040.72 11 8 4 5 10967.4 1044.09 10 8 -4 6 593.303 230.238 11 8 4 6 459.598 196.486 10 8 -4 7 449.393 171.691 11 8 4 7 206.084 114.066 11 8 4 7 417.465 161.466 10 8 -4 8 694.921 182.534 11 8 4 8 493.615 143.291 10 -8 5 13 275.942 136.854 17 -8 5 12 140.945 97.7372 17 -8 5 12 291.868 162.528 16 -8 -5 11 1788.10 425.155 17 -8 5 11 1890.47 411.348 17 -8 5 11 1469.36 389.820 16 -8 -5 10 475.816 241.929 17 -8 5 10 29.0859 116.133 17 -8 5 10 84.5090 190.636 16 -8 -5 10 466.514 202.131 14 -8 -5 9-132.613 149.699 17 -8 5 9-2.76207 205.595 16 -8 -5 9-86.0924 120.449 14 -8 -5 8 1537.31 432.497 17 -8 5 8 1262.75 418.817 16 -8 -5 8 1001.64 326.878 14 -8 -5 7 15064.8 1411.24 17 -8 5 7 11749.6 1291.56 16 -8 -5 6 3335.96 661.780 17 -8 5 6 2142.32 511.614 16 -8 -5 5 667.000 286.265 17 -8 5 5 694.543 315.385 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1695.63 433.738 10 -8 -7 -1 2459.58 477.234 18 8 7 2 195.270 163.675 10 -8 -7 -2 39.6580 81.3613 18 8 -7 2 47.6483 70.6253 15 8 7 3 5431.55 708.049 10 -8 -7 -3 4691.60 580.257 18 8 -7 3 4323.79 723.472 15 8 7 4 187.848 142.216 10 8 -7 4-320.959 191.768 15 8 7 5-173.561 145.648 10 8 7 6 4135.51 450.829 10 -8 8 11 217.353 145.460 16 -8 -8 11 85.5582 72.3628 13 -8 8 10-314.241 171.161 16 -8 8 9 1800.51 386.800 16 -8 -8 9 2192.95 399.583 14 -8 8 8 3269.30 588.559 16 -8 -8 8 3358.17 557.728 14 -8 8 7 106.412 145.529 16 -8 -8 7-20.9541 170.217 14 -8 8 6 1125.03 358.040 16 -8 -8 6 1502.32 415.568 14 -8 -8 5 3300.10 545.521 18 -8 8 5 2559.56 538.183 16 -8 -8 5 2906.97 563.039 14 -8 -8 4-85.8235 130.701 18 -8 8 4-64.2111 132.159 16 -8 -8 4 221.025 175.847 14 -8 -8 3 2424.10 488.928 18 -8 8 3 2433.44 475.883 16 -8 -8 3 2933.04 539.004 14 -8 -8 2 1159.01 359.957 18 -8 -8 2 548.923 200.234 14 -8 -8 1 9058.90 967.878 18 -8 -8 0 1034.08 302.852 18 8 8 1 95.9650 90.1826 10 -8 -8 -1 367.640 199.262 18 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9003.43 694.009 18 8 -9 3 9610.41 939.068 15 -8 10 9 1860.98 326.618 16 -8 -10 9 1649.28 308.348 13 -8 10 8 83.7186 102.696 16 -8 -10 8-215.077 156.105 13 -8 10 7 137.127 126.651 16 -8 10 6 2159.69 384.787 16 -8 -10 5 944.183 258.274 14 -8 -10 4 193.204 125.319 18 -8 -10 4 172.675 99.9019 14 -8 -10 3 206.072 93.8069 18 -8 -10 3 112.434 75.8250 14 -8 -10 2 51.5109 65.6331 18 8 -10 -2 106.916 142.329 15 -8 -10 1 9002.05 825.174 18 8 -10 -1 6276.01 818.923 15 -8 -10 0 116.884 124.064 18 8 -10 0 31.2204 103.331 15 -8 -10 -1 739.310 199.954 18 8 -10 1 656.618 232.233 15 -8 -10 -2 2385.61 337.869 18 8 -10 2 1915.97 390.190 15 -8 -11 6-5.50310 74.9033 13 -8 -11 5 2790.03 419.053 13 -8 -11 4 350.623 139.454 18 -8 -11 4 127.256 79.7204 13 -8 -11 3 226.616 138.940 18 -8 -11 2 127.098 111.249 18 -8 -11 1 570.534 183.239 18 -8 -11 0 1105.94 233.724 18 -9 0 14 245.739 119.190 17 -9 0 13 125.861 127.329 17 -9 0 12 993.106 323.597 17 -9 0 11 158.348 118.499 17 -9 0 10 786.636 352.722 17 -9 0 9 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236.485 182.576 17 -9 -1 6 753.776 315.697 17 -9 1 6 476.992 211.926 17 -9 -1 6 763.113 320.500 16 -9 1 6 689.567 352.364 16 -9 -1 5 873.352 323.541 17 -9 1 5 1234.48 389.251 17 -9 -1 5 992.668 356.181 16 -9 1 5 946.859 351.908 16 -9 -1 4 22610.7 1692.82 17 -9 1 4 17994.3 1464.35 17 -9 -1 4 19797.9 1694.82 16 -9 1 4 20950.0 1735.45 16 -9 -1 3 1265.60 423.158 16 -9 1 3 656.661 272.540 16 -9 -1 2 486.272 233.248 16 -9 1 2 452.980 248.546 16 -9 -1 1 2994.24 604.337 16 -9 1 1 2729.03 557.156 16 -9 -1 0 781.584 306.972 16 -9 1 0 690.273 278.127 16 9 -1 1 1779.29 433.709 10 9 1 1 1978.89 497.179 10 -9 1 -1 2576.92 516.296 16 9 1 2-220.449 224.258 10 9 1 3 3451.54 569.636 10 9 -1 4 18845.5 1426.40 11 9 1 4 16529.6 1214.16 10 9 -1 5 214.220 131.301 11 9 1 5 52.1876 62.0439 11 9 1 5-5.04656 81.1018 10 9 -1 6 108.734 117.318 11 9 1 6 48.4597 75.2379 11 -9 -2 13 74.7746 77.8545 17 -9 2 13-3.46227 59.2816 17 -9 -2 12 17.3720 82.6557 17 -9 2 12 161.178 115.478 17 -9 -2 11 45.6405 124.445 17 -9 2 11 310.611 208.943 17 -9 -2 10 1634.66 431.451 17 -9 2 10 1216.25 364.371 17 -9 -2 9 915.261 294.389 17 -9 2 9 803.972 317.690 17 -9 2 9 484.440 216.590 16 -9 -2 8 10763.9 1151.39 17 -9 2 8 8323.95 981.601 17 -9 2 8 7967.75 1040.04 16 -9 -2 7 1366.14 420.361 17 -9 2 7 958.580 333.712 17 -9 2 7 1662.59 507.540 16 -9 -2 6 5346.44 822.712 17 -9 2 6 3716.56 614.437 17 -9 2 6 3710.40 718.545 16 -9 -2 5 1522.62 435.216 17 -9 -2 5 1068.04 357.508 16 -9 2 5 1595.48 432.450 16 -9 -2 4 2357.98 531.261 17 -9 -2 4 2062.47 521.036 16 -9 2 4 1395.55 417.639 16 -9 -2 3 2994.87 609.357 16 -9 2 3 2840.39 594.593 16 -9 -2 2 1330.65 439.233 16 -9 2 2 1672.69 439.066 16 -9 -2 1-127.592 134.341 16 -9 2 1 70.4069 113.573 16 -9 2 0 13461.2 1249.31 16 9 2 1-5.30750 101.137 10 -9 2 -1 57.4713 120.145 16 9 2 2 1172.75 356.191 10 9 -2 3 725.339 288.678 11 9 2 3 733.641 299.696 10 9 -2 4 630.145 243.250 11 9 2 4 196.772 178.965 10 9 -2 5 2979.98 488.436 11 9 2 5 3360.66 463.250 10 9 -2 6-26.2995 59.1489 11 9 2 6 63.2092 79.3212 11 9 2 6 92.6907 86.1987 10 -9 -3 13 162.656 123.240 17 -9 3 13-22.4368 54.7150 17 -9 -3 12-24.5328 85.2360 17 -9 3 12-65.2050 112.300 17 -9 -3 11 215.462 194.821 17 -9 3 11-115.208 124.566 17 -9 -3 10 2016.97 457.924 17 -9 3 10 1303.19 360.469 17 -9 3 10 1115.24 343.775 16 -9 -3 9 4323.48 742.356 17 -9 3 9 3280.93 582.299 17 -9 3 9 3366.09 653.633 16 -9 -3 9 3612.50 559.164 14 -9 -3 8 66.3986 195.674 17 -9 3 8 16.3758 87.0853 17 -9 3 8 90.3740 85.0113 16 -9 -3 7 800.229 270.757 17 -9 3 7 1574.43 473.042 16 -9 -3 6 704.225 296.516 17 -9 3 6 954.569 369.375 16 -9 -3 5 824.455 338.147 17 -9 3 5 729.971 373.169 16 -9 -3 4 7498.12 987.295 16 -9 3 4 7559.13 989.031 16 -9 -3 3-27.1279 91.2734 16 -9 3 3-284.232 227.066 16 -9 -3 2 14987.2 1431.56 16 -9 3 2 17260.1 1470.96 16 -9 3 1 3957.43 639.774 16 9 3 0-146.460 155.892 10 -9 3 0-101.679 113.281 16 9 3 1 2718.60 554.990 10 -9 3 -1 3731.33 591.213 16 9 -3 2 2236.45 496.968 11 9 3 2 2241.61 506.122 10 -9 3 -2 1670.41 371.439 16 9 -3 3 331.449 206.748 11 9 3 3 723.812 283.622 10 9 -3 4 3095.80 522.212 11 9 3 4 3942.08 564.198 10 9 -3 5 9.45108 55.3349 11 9 3 5-62.0803 94.6658 10 9 -3 6 2273.04 354.795 11 9 3 6 2761.23 361.968 10 -9 -4 12-81.3020 66.4354 17 -9 4 12-11.3506 46.5910 17 -9 4 11-19.6082 63.9612 17 -9 4 11 76.2509 98.2409 16 -9 -4 10 1516.77 390.686 17 -9 4 10 1089.71 327.239 17 -9 4 10 934.223 329.827 16 -9 4 9 2108.30 514.215 16 -9 -4 9 2555.27 453.904 14 -9 -4 8 742.353 294.013 17 -9 4 8 639.283 289.713 16 -9 -4 8 840.294 314.939 14 -9 -4 7-151.691 188.074 17 -9 4 7-112.175 101.981 16 -9 -4 6 4584.39 775.018 17 -9 4 6 4702.41 777.834 16 -9 4 5 12125.4 1275.59 16 -9 4 4 2609.12 566.846 16 -9 4 3 4673.50 746.807 16 -9 4 2 270.854 167.147 16 -9 4 1 2191.38 464.607 16 9 4 0 123.476 95.3657 10 -9 4 0 206.185 113.274 16 9 4 1-159.045 146.687 10 -9 4 -1-14.8515 82.9497 16 9 4 2 3666.22 633.586 10 9 -4 3 5480.42 698.748 11 9 4 3 6937.24 794.528 10 9 -4 4 168.569 146.967 11 9 4 4 70.6439 101.892 10 9 -4 5 2357.05 380.849 11 9 4 5 3167.50 430.872 10 -9 -5 11 48.9672 91.8013 17 -9 5 11 70.4150 102.607 16 -9 -5 10 273.343 147.965 17 -9 5 10 269.118 179.541 16 -9 -5 10 64.8299 100.740 14 -9 -5 9 1618.72 431.320 17 -9 5 9 1383.30 401.939 16 -9 -5 9 1407.19 345.902 14 -9 -5 8 205.801 191.219 17 -9 5 8-71.6719 148.854 16 -9 -5 8 288.231 133.385 14 -9 -5 7 2152.48 516.257 17 -9 5 7 1052.66 367.473 16 -9 -5 7 1419.08 351.420 14 -9 5 6 2691.28 577.024 16 -9 5 5 8547.40 1034.61 16 -9 5 4 440.689 273.909 16 -9 5 3 108.699 138.325 16 -9 5 2 1037.01 334.089 16 9 5 -1 7097.84 945.808 10 -9 5 1 7353.02 842.916 16 9 5 0 133.299 138.978 10 -9 5 0 339.290 149.655 16 9 5 1 798.097 290.834 10 9 5 2 61.8408 92.7503 10 9 5 3 3513.09 530.078 10 -9 -5 -3 2523.18 373.199 18 9 5 4 109.140 106.826 10 9 5 5 230.437 103.827 10 -9 6 11 181.474 150.061 16 -9 6 10 566.558 229.200 16 -9 -6 10 520.395 183.445 14 -9 6 9 1849.19 423.612 16 -9 -6 9 1498.19 347.791 14 -9 6 8-84.1326 188.153 16 -9 -6 8 18.7311 97.5953 14 -9 6 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548.968 18 -9 -8 -1 5505.74 563.342 18 -9 -9 8 673.851 196.918 13 -9 9 7 74.3100 101.809 16 -9 -9 7 36.7599 87.0366 14 -9 9 6 78.8615 91.1038 16 -9 -9 6-51.2265 72.7289 14 -9 9 5 1529.94 296.001 16 -9 -9 5 401.936 178.375 14 -9 -9 4 351.651 138.436 18 -9 -9 4 80.9969 98.3854 14 -9 -9 3 1972.02 339.378 18 -9 -9 3 432.969 162.645 14 -9 -9 2 285.081 121.314 18 -9 -9 1 350.515 160.318 18 -9 -9 0 6293.42 583.976 18 -10 0 12 64.2128 82.8338 17 -10 0 11-39.5465 76.6762 17 -10 0 10 235.885 149.867 17 -10 0 9-176.574 188.704 17 -10 0 8 234.007 166.650 17 -10 0 7 14.2877 115.853 17 -10 0 7-35.2491 97.1777 16 -10 0 6 16955.1 1361.00 17 -10 0 6 13664.2 1297.87 16 -10 0 5 105.805 122.765 16 -10 0 4-99.9189 192.701 16 -10 0 3 37.0316 119.447 16 -10 0 2 9701.90 1042.02 16 10 0 -1-170.016 181.589 10 -10 0 1-122.587 231.998 16 10 0 0 886.986 273.394 10 10 0 1-11.4414 70.1689 10 10 0 2 3908.66 501.607 10 10 0 3-55.7191 76.1949 11 -10 -1 12 104.893 127.507 17 -10 1 12 12.4491 60.4436 17 -10 -1 11-84.5493 71.2089 17 -10 1 11 135.439 129.143 17 -10 -1 10 2690.88 491.725 17 -10 1 10 2625.50 463.847 17 -10 -1 9 151.204 115.594 17 -10 1 9 184.303 145.805 17 -10 -1 8-103.560 203.118 17 -10 1 8 76.6530 81.4974 17 -10 1 8 79.7595 69.7776 16 -10 -1 7 264.130 178.731 17 -10 1 7 225.120 183.352 17 -10 1 7 102.159 75.3044 16 -10 -1 6 554.076 274.776 17 -10 1 6 376.314 174.348 17 -10 -1 6 245.213 178.979 16 -10 1 6 182.829 161.164 16 -10 -1 5-58.2418 210.193 16 -10 1 5 185.676 158.778 16 -10 -1 4 382.128 237.350 16 -10 1 4 85.8365 125.898 16 -10 -1 3 2804.64 550.453 16 -10 1 3 2449.47 508.895 16 -10 -1 2 6375.58 844.416 16 -10 1 2 5845.85 799.197 16 10 -1 -1 971.391 314.011 10 10 1 -1 1068.15 353.719 10 -10 1 1 751.274 273.833 16 10 1 0-0.66103 123.481 10 10 1 1 798.269 231.462 10 10 -1 2 3303.71 522.925 11 10 1 2 3297.55 481.369 10 10 -1 3 32.0020 50.3624 11 10 1 3 42.3228 61.5580 10 -10 -2 11 324.864 185.879 17 -10 2 11 149.249 118.172 17 -10 -2 10 976.949 290.784 17 -10 2 10 905.339 256.369 17 -10 -2 9 793.417 261.041 17 -10 2 9 776.989 257.966 17 -10 2 9 517.105 220.508 16 -10 -2 9 471.306 170.893 14 -10 -2 8 5.68181 106.681 17 -10 2 8 69.1375 110.210 17 -10 2 8-85.5331 96.2513 16 -10 -2 7 103.300 153.313 17 -10 2 7-2.89529 69.1342 17 -10 2 7 152.524 183.328 16 -10 2 6 4247.69 688.571 16 -10 -2 5 559.584 259.307 16 -10 2 5 513.314 265.976 16 -10 -2 4 2246.93 497.609 16 -10 2 4 2183.55 487.432 16 -10 2 3 3725.11 642.815 16 -10 2 2 508.482 239.539 16 10 2 -1 1402.66 384.558 10 -10 2 1 2171.49 445.978 16 10 2 0-47.6700 120.562 10 -10 2 0 26.9813 132.378 16 10 2 1-131.167 109.238 10 10 -2 2 4169.23 552.218 11 10 2 2 5631.47 639.303 10 10 -2 3 554.841 179.748 11 10 2 3 1362.51 273.925 10 -10 -3 11-9.94262 65.8491 17 -10 -3 10 1063.36 305.168 17 -10 3 10 591.538 196.969 17 -10 3 10 618.952 226.456 16 -10 -3 9 437.147 226.180 17 -10 3 9 180.503 116.275 16 -10 -3 9 82.7243 84.3983 14 -10 -3 8 1784.22 451.889 17 -10 3 8 1494.50 411.081 16 -10 -3 8 1693.45 382.209 14 -10 3 7 2451.23 521.899 16 -10 3 6 4447.60 706.759 16 -10 3 5 2300.07 495.985 16 -10 3 4 420.586 260.899 16 -10 3 3 2009.69 443.555 16 -10 3 2 6390.88 795.806 16 10 3 -1 1842.36 418.497 10 -10 3 1 2676.99 478.708 16 10 3 0 339.050 188.009 10 -10 3 0 617.133 172.317 16 10 3 1 67.2296 64.9069 10 10 3 2 100.411 115.166 10 10 3 3 692.197 192.008 10 -10 4 10-5.53082 96.5661 16 -10 4 9 14.3305 87.5449 16 -10 -4 9 275.997 155.314 14 -10 4 8-31.0198 93.1979 16 -10 -4 8-113.649 150.188 14 -10 4 7-91.2355 186.273 16 -10 -4 7 21.1641 108.913 14 -10 4 6 288.638 144.901 16 -10 4 5 3741.99 612.087 16 -10 4 4 152.541 91.1166 16 -10 4 3 604.019 220.049 16 10 4 -2 137.438 187.590 10 -10 4 2 186.231 152.476 16 10 4 -1 3000.85 531.638 10 -10 4 1 3461.74 516.916 16 10 4 0-17.4799 96.0339 10 -10 4 0 126.832 48.1933 16 10 4 1 12.1898 84.4285 10 10 4 2 1329.63 288.997 10 -10 5 9 494.016 193.784 16 -10 -5 9 245.776 103.937 14 -10 5 8 380.222 188.768 16 -10 -5 8 370.181 171.696 14 -10 5 7 529.432 244.335 16 -10 -5 7 423.325 209.192 14 -10 5 6 357.939 205.407 16 -10 -5 6 171.699 102.016 14 -10 5 5 374.947 207.229 16 -10 -5 5 326.652 171.106 14 -10 5 4 911.617 282.848 16 -10 -5 4 550.234 233.220 14 10 5 -3 250.566 163.945 10 -10 5 3-40.2178 88.1706 16 -10 -5 3-36.2685 129.975 14 -10 5 2-82.1921 110.965 16 -10 -5 2-89.5517 96.4909 14 10 5 -1-101.125 122.890 10 -10 -5 1-35.5801 61.9468 14 10 5 0 3374.25 511.707 10 -10 -5 0 3508.45 469.804 18 10 5 1 2086.90 378.802 10 -10 -5 -1 1922.80 307.557 18 -10 6 9 79.8734 69.4171 16 -10 6 8-43.1136 94.9189 16 -10 -6 8-81.2500 79.2699 14 -10 6 7 97.9061 116.309 16 -10 -6 7 260.384 139.996 14 -10 6 6 12.0149 77.7631 16 -10 -6 6-159.613 108.241 14 10 6 -5 380.939 177.737 10 -10 -6 5 244.133 131.611 18 -10 6 5 307.851 182.748 16 -10 -6 5 185.699 108.630 14 10 6 -4 2727.67 464.783 10 -10 -6 4 5165.60 594.566 18 -10 6 4 4995.82 603.020 16 -10 -6 4 2756.04 462.041 14 -10 -6 3 3590.87 497.223 18 10 6 -3 2028.47 393.022 10 -10 6 3 2856.37 434.989 16 -10 -6 3 1095.99 280.505 14 10 6 -2 122.565 109.303 10 -10 -6 2-91.9416 93.7903 18 -10 6 2 125.959 116.545 16 -10 -6 2 80.8111 111.895 14 10 6 -1-9.10662 77.1395 10 -10 -6 1-56.4030 83.5899 18 10 6 0 27.4594 70.2098 10 -10 -6 0 14.2279 47.0213 18 -10 7 7 2015.82 348.325 16 -10 -7 7 513.889 184.939 14 -10 7 6 25.7682 55.9575 16 -10 -7 6-41.8064 59.9604 14 -10 7 5 170.204 100.954 16 -10 -7 5-30.7320 96.3972 14 -10 -7 4-121.358 97.8495 18 -10 7 4 197.716 85.4505 16 -10 -7 4-37.7497 83.3895 14 -10 -7 3 3964.27 465.876 18 -10 -7 3 414.575 170.501 14 -10 -7 2 284.815 118.329 18 -10 -7 1 3453.71 418.534 18 -11 0 6 354.856 173.568 16 -11 0 5-51.1087 78.0923 16 11 0 -4 64.4252 79.6992 10 11 0 -3-60.5537 73.3053 10 11 0 -2 830.799 248.263 10 -11 1 7 201.059 133.980 16 -11 1 6 882.219 259.040 16 -11 1 5 1374.90 331.178 16 11 -1 -4 819.208 235.977 10 11 1 -4 1444.29 356.327 10 11 1 -3 40.5762 55.8474 10 11 1 -2 532.881 199.347 10 -11 2 7 135.533 112.598 16 -11 -2 7 190.558 121.380 14 -11 2 6 321.937 156.168 16 -11 2 5 543.253 188.258 16 11 2 -4 486.072 204.130 10 -11 2 4 811.466 249.047 16 11 2 -3 804.672 268.794 10 -11 2 3 1669.35 330.659 16 11 2 -2 46.7037 69.6818 10 -11 -3 7 663.680 190.942 14 -11 3 6 211.571 116.146 16 -11 -3 6 48.7616 80.9520 14 11 3 -5 212.944 160.657 10 -11 3 5 557.903 176.726 16 -11 -3 5 282.534 147.805 14 11 3 -4 370.292 164.263 10 -11 3 4 420.528 161.302 16 11 3 -3 0.81107 52.0386 10 -11 3 3-14.7257 48.3801 16 -11 -4 5 108.070 89.1881 14 -11 -4 4 16.1438 79.3674 14 0 0 0 0.00 0.00 0 TITL D418 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 9.264792 13.303367 14.510257 90.0000 105.2607 90.0000 ZERR 7.00 0.001380 0.001571 0.002265 0.0000 0.0147 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 77.00 70.00 7.00 7.00 TREF HKLF 4 END ; _shelx_hkl_checksum 16157 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br1 Br -0.33148(8) 0.21991(5) 0.18487(5) 0.0587(2) Uani 1 1 d . . . . . Br2 Br -0.32495(9) -0.18112(6) 0.05760(5) 0.0660(3) Uani 1 1 d . . . . . O1 O -0.0578(5) 0.1511(3) 0.3310(3) 0.0570(12) Uani 1 1 d . . . . . H1 H 0.0023 0.1291 0.3787 0.086 Uiso 1 1 calc R U . . . O2 O 0.7705(5) 0.0538(4) 0.8879(3) 0.0614(12) Uani 1 1 d . . . . . N1 N 0.1322(6) 0.0244(4) 0.4254(3) 0.0468(11) Uani 1 1 d . . . . . N2 N 0.6465(6) 0.0636(4) 0.8092(4) 0.0549(14) Uani 1 1 d . . . . . C1 C -0.1135(6) 0.0756(4) 0.2723(4) 0.0410(12) Uani 1 1 d . . . . . C2 C -0.2412(6) 0.0903(4) 0.1978(4) 0.0432(12) Uani 1 1 d . . . . . C3 C -0.3047(6) 0.0150(5) 0.1355(4) 0.0455(13) Uani 1 1 d . . . . . H3 H -0.3919 0.0265 0.0875 0.055 Uiso 1 1 calc R U . . . C4 C -0.2360(7) -0.0781(5) 0.1457(4) 0.0454(13) Uani 1 1 d . . . . . C5 C -0.1111(7) -0.0974(4) 0.2185(4) 0.0467(13) Uani 1 1 d . . . . . H5 H -0.0680 -0.1610 0.2250 0.056 Uiso 1 1 calc R U . . . C6 C -0.0488(7) -0.0215(4) 0.2827(4) 0.0451(13) Uani 1 1 d . . . . . C7 C 0.0785(7) -0.0429(4) 0.3629(4) 0.0469(14) Uani 1 1 d . . . . . H7 H 0.1217 -0.1065 0.3690 0.056 Uiso 1 1 calc R U . . . C8 C 0.2528(6) 0.0073(4) 0.5065(4) 0.0423(12) Uani 1 1 d . . . . . C9 C 0.3393(7) -0.0787(5) 0.5242(4) 0.0601(18) Uani 1 1 d . . . . . H9 H 0.3184 -0.1317 0.4809 0.072 Uiso 1 1 calc R U . . . C10 C 0.4572(7) -0.0871(5) 0.6061(4) 0.0573(17) Uani 1 1 d . . . . . H10 H 0.5138 -0.1458 0.6167 0.069 Uiso 1 1 calc R U . . . C11 C 0.4921(6) -0.0098(4) 0.6721(4) 0.0432(13) Uani 1 1 d . . . . . C12 C 0.4012(6) 0.0761(4) 0.6547(4) 0.0438(13) Uani 1 1 d . . . . . H12 H 0.4196 0.1281 0.6991 0.053 Uiso 1 1 calc R U . . . C13 C 0.2855(6) 0.0850(4) 0.5734(4) 0.0461(13) Uani 1 1 d . . . . . H13 H 0.2283 0.1434 0.5629 0.055 Uiso 1 1 calc R U . . . C14 C 0.6200(6) -0.0177(5) 0.7578(4) 0.0459(13) Uani 1 1 d . . . . . C15 C 0.7124(7) -0.1105(5) 0.7812(5) 0.0636(19) Uani 1 1 d . . . . . H15A H 0.8037 -0.0953 0.8285 0.095 Uiso 1 1 calc R U . . . H15B H 0.7353 -0.1353 0.7245 0.095 Uiso 1 1 calc R U . . . H15C H 0.6578 -0.1607 0.8056 0.095 Uiso 1 1 calc R U . . . C16 C 0.7922(9) 0.1468(6) 0.9376(5) 0.068(2) Uani 1 1 d . . . . . H16A H 0.7118 0.1581 0.9678 0.081 Uiso 1 1 calc R U . . . H16B H 0.7922 0.2014 0.8934 0.081 Uiso 1 1 calc R U . . . C17 C 0.9398(7) 0.1431(6) 1.0121(5) 0.071(2) Uani 1 1 d . . . . . H17A H 1.0197 0.1412 0.9813 0.106 Uiso 1 1 calc R U . . . H17B H 0.9437 0.0840 1.0506 0.106 Uiso 1 1 calc R U . . . H17C H 0.9501 0.2017 1.0518 0.106 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.0576(4) 0.0490(4) 0.0608(5) 0.0041(3) 0.0001(3) 0.0105(3) Br2 0.0692(5) 0.0598(5) 0.0608(5) -0.0165(3) 0.0024(3) -0.0223(4) O1 0.059(3) 0.048(2) 0.050(3) -0.0113(19) -0.011(2) 0.008(2) O2 0.058(3) 0.061(3) 0.049(2) -0.003(2) -0.015(2) -0.003(2) N1 0.048(3) 0.045(3) 0.040(3) -0.001(2) -0.002(2) 0.002(2) N2 0.053(3) 0.056(3) 0.045(3) 0.003(2) -0.006(2) -0.008(2) C1 0.043(3) 0.039(3) 0.038(3) -0.002(2) 0.004(2) -0.004(2) C2 0.042(3) 0.044(3) 0.040(3) 0.004(2) 0.003(2) -0.002(2) C3 0.035(3) 0.056(3) 0.041(3) 0.006(3) 0.002(2) -0.009(2) C4 0.046(3) 0.043(3) 0.044(3) -0.007(2) 0.006(2) -0.009(2) C5 0.050(3) 0.037(3) 0.049(3) 0.001(2) 0.007(3) -0.001(2) C6 0.046(3) 0.041(3) 0.042(3) 0.001(2) 0.001(2) -0.004(2) C7 0.046(3) 0.040(3) 0.050(3) 0.002(2) 0.004(3) 0.004(2) C8 0.042(3) 0.043(3) 0.037(3) 0.001(2) 0.002(2) -0.001(2) C9 0.060(4) 0.060(4) 0.049(4) -0.014(3) -0.006(3) 0.016(3) C10 0.055(4) 0.054(4) 0.049(4) -0.007(3) -0.010(3) 0.012(3) C11 0.040(3) 0.045(3) 0.040(3) 0.005(2) 0.003(2) -0.002(2) C12 0.046(3) 0.039(3) 0.041(3) -0.003(2) 0.003(2) -0.004(2) C13 0.045(3) 0.039(3) 0.049(3) -0.001(2) 0.002(2) -0.003(2) C14 0.042(3) 0.051(3) 0.040(3) 0.006(3) 0.002(2) -0.007(3) C15 0.051(4) 0.065(4) 0.062(4) -0.001(3) -0.008(3) 0.006(3) C16 0.076(5) 0.070(5) 0.045(4) -0.005(3) -0.005(3) -0.017(4) C17 0.047(4) 0.102(6) 0.055(4) -0.014(4) -0.001(3) -0.016(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C1 O1 H1 109.5 . . N2 O2 C16 108.1(5) . . C7 N1 C8 123.6(5) . . C14 N2 O2 112.4(5) . . O1 C1 C2 119.9(5) . . O1 C1 C6 122.7(5) . . C2 C1 C6 117.4(5) . . C3 C2 C1 122.6(6) . . C3 C2 Br1 119.7(4) . . C1 C2 Br1 117.7(4) . . C2 C3 C4 118.5(5) . . C2 C3 H3 120.7 . . C4 C3 H3 120.7 . . C3 C4 C5 121.4(5) . . C3 C4 Br2 117.8(4) . . C5 C4 Br2 120.7(5) . . C4 C5 C6 119.8(6) . . C4 C5 H5 120.1 . . C6 C5 H5 120.1 . . C5 C6 C1 120.1(5) . . C5 C6 C7 120.0(5) . . C1 C6 C7 119.8(5) . . N1 C7 C6 120.9(5) . . N1 C7 H7 119.5 . . C6 C7 H7 119.5 . . C9 C8 C13 118.3(5) . . C9 C8 N1 125.6(5) . . C13 C8 N1 116.1(5) . . C8 C9 C10 120.8(6) . . C8 C9 H9 119.6 . . C10 C9 H9 119.6 . . C11 C10 C9 121.3(6) . . C11 C10 H10 119.4 . . C9 C10 H10 119.4 . . C10 C11 C12 117.5(5) . . C10 C11 C14 121.2(5) . . C12 C11 C14 121.3(5) . . C13 C12 C11 121.3(5) . . C13 C12 H12 119.3 . . C11 C12 H12 119.3 . . C12 C13 C8 120.7(6) . . C12 C13 H13 119.6 . . C8 C13 H13 119.6 . . N2 C14 C15 123.3(5) . . N2 C14 C11 114.3(6) . . C15 C14 C11 122.4(5) . . C14 C15 H15A 109.5 . . C14 C15 H15B 109.5 . . H15A C15 H15B 109.5 . . C14 C15 H15C 109.5 . . H15A C15 H15C 109.5 . . H15B C15 H15C 109.5 . . O2 C16 C17 108.5(7) . . O2 C16 H16A 110.0 . . C17 C16 H16A 110.0 . . O2 C16 H16B 110.0 . . C17 C16 H16B 110.0 . . H16A C16 H16B 108.4 . . C16 C17 H17A 109.5 . . C16 C17 H17B 109.5 . . H17A C17 H17B 109.5 . . C16 C17 H17C 109.5 . . H17A C17 H17C 109.5 . . H17B C17 H17C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Br1 C2 1.904(6) . Br2 C4 1.907(6) . O1 C1 1.330(7) . O1 H1 0.8200 . O2 N2 1.397(6) . O2 C16 1.419(8) . N1 C7 1.279(7) . N1 C8 1.411(7) . N2 C14 1.299(8) . C1 C2 1.391(7) . C1 C6 1.414(8) . C2 C3 1.372(8) . C3 C4 1.383(9) . C3 H3 0.9300 . C4 C5 1.370(8) . C5 C6 1.392(8) . C5 H5 0.9300 . C6 C7 1.451(7) . C7 H7 0.9300 . C8 C9 1.382(8) . C8 C13 1.396(8) . C9 C10 1.390(8) . C9 H9 0.9300 . C10 C11 1.384(8) . C10 H10 0.9300 . C11 C12 1.402(8) . C11 C14 1.479(7) . C12 C13 1.374(7) . C12 H12 0.9300 . C13 H13 0.9300 . C14 C15 1.490(9) . C15 H15A 0.9600 . C15 H15B 0.9600 . C15 H15C 0.9600 . C16 C17 1.504(8) . C16 H16A 0.9700 . C16 H16B 0.9700 . C17 H17A 0.9600 . C17 H17B 0.9600 . C17 H17C 0.9600 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C16 O2 N2 C14 178.5(6) . . . . O1 C1 C2 C3 -179.4(6) . . . . C6 C1 C2 C3 0.0(9) . . . . O1 C1 C2 Br1 -0.7(8) . . . . C6 C1 C2 Br1 178.7(4) . . . . C1 C2 C3 C4 -2.0(9) . . . . Br1 C2 C3 C4 179.3(4) . . . . C2 C3 C4 C5 2.8(9) . . . . C2 C3 C4 Br2 -179.3(4) . . . . C3 C4 C5 C6 -1.5(10) . . . . Br2 C4 C5 C6 -179.3(5) . . . . C4 C5 C6 C1 -0.6(9) . . . . C4 C5 C6 C7 176.6(6) . . . . O1 C1 C6 C5 -179.3(6) . . . . C2 C1 C6 C5 1.3(9) . . . . O1 C1 C6 C7 3.5(10) . . . . C2 C1 C6 C7 -175.9(6) . . . . C8 N1 C7 C6 178.0(6) . . . . C5 C6 C7 N1 -176.2(6) . . . . C1 C6 C7 N1 1.0(10) . . . . C7 N1 C8 C9 7.6(11) . . . . C7 N1 C8 C13 -172.4(6) . . . . C13 C8 C9 C10 -0.9(11) . . . . N1 C8 C9 C10 179.1(6) . . . . C8 C9 C10 C11 -0.2(12) . . . . C9 C10 C11 C12 1.9(10) . . . . C9 C10 C11 C14 -178.4(6) . . . . C10 C11 C12 C13 -2.5(9) . . . . C14 C11 C12 C13 177.7(5) . . . . C11 C12 C13 C8 1.5(9) . . . . C9 C8 C13 C12 0.3(10) . . . . N1 C8 C13 C12 -179.7(6) . . . . O2 N2 C14 C15 0.0(9) . . . . O2 N2 C14 C11 -178.4(5) . . . . C10 C11 C14 N2 174.7(6) . . . . C12 C11 C14 N2 -5.5(9) . . . . C10 C11 C14 C15 -3.7(10) . . . . C12 C11 C14 C15 176.1(6) . . . . N2 O2 C16 C17 -170.3(6) . . . .