Crystallography Open Database

Information card for entry 8107094

Preview

Coordinates	8107094.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	μ-oxalato-κ^2^O,O:κ^2^O',O'-bis[(bromido)(η^6^-<i>p</i>-cymene)-osmium(II)]
Formula	C22 H28 Br2 O4 Os2
Calculated formula	C22 H28 Br2 O4 Os2
Title of publication	Crystal structure of dibromido μ-oxalato-κ2 O,O′:κ2 O′′,O′′′−η6-p-cymenediosmium(II), C22H28Br2O4Os2
Authors of publication	Clayton, Hadley S.; Tapala, Kgaugelo C.; Lemmerer, Andreas
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2016
Journal volume	231
Journal issue	4
Pages of publication	1055 - 1056
a	10.8433 ± 0.0005 Å
b	11.8395 ± 0.0005 Å
c	18.7871 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	2411.87 ± 0.18 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0555
Residual factor for significantly intense reflections	0.0511
Weighted residual factors for significantly intense reflections	0.1041
Weighted residual factors for all reflections included in the refinement	0.1061
Goodness-of-fit parameter for all reflections included in the refinement	1.381
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
282762 (current)	2023-04-20	cif/ Adding structures of 8107094 via cif-deposit CGI script.	8107094.cif